CERTIFICATE OF ANALYSIS Adrafinil - NewMind


Dec 8, 2015 - S oluble in methanol, slightly soluble in ethyl-acetate. Complies. & methylene chloride, practically insoluble in water. Identification. IR & HPLC ...

NEWMIND 47 W. Polk St. STE 100-241 Chicago, IL 60605

[email protected] www.newmind.com

CERTIFICATE OF ANALYSIS Adrafinil (2-(benzhydrylsulfinyl)acetohydroxamic acid)

Material Lot#

20151208

Manufacture Date:

12/08/2015

Country of Origin:

China

Retesting Date:

12/07/2018

Analysis

Claim

Result

Assay

≥98%

99.35%

Test

Claim

Result

Appearance

Light red to off white crystalline powder

Complies

Solubility

S oluble in methanol, slightly soluble in ethyl-acetate

Complies

& methylene chloride, practically insoluble in water

Identification

IR & HPLC matches standard

Complies

Impurity Test

Claim

Result

Melting Point

148°~150°C

149.0~149.2°C

Is omer

≤1.0%

0.55%

Los s on Drying

≤0.5%

0.2%

Res idue on Ignition

≤0.1%

0.08%

Heavy Metals

≤20ppm

Complies

Conforms to Standard

Adra fi nil s hould be stored a t or below room temperature in a tightly s ealed durable container. Adra fi nil s hould be protected from excess heat, direct s unlight, excess humidity a nd moisture. Adra fi nil has a s table shelf life of 3 yea rs from the date of manufacture when properly s tored.

Recommend Documents
Jan 2, 2019 - Insoluble in water and methanol. Complies. Identification. Reaction positive. Complies. Impurity Test. Claim. Result. Any single Impurity. ≤0.2%.

Oct 13, 2016 - Freely soluble in water, methanol, & dichloromethane. Complies. Identification. IR matches standard & gives reaction to sodium. Complies.

Jan 8, 2018 - Never marketed. Cyclazodone is a centrally acting stimulant drug which is related to other drugs such as pemoline and 4-methylaminorex.

Nov 16, 2016 - Largest Single Impurity. ≤ 0.1%. 0.08%. Total Impurity. ≤ 0.5%. 0.32%. Sunifiram should be stored at or below room temperature in a tightly ...

Mar 6, 2015 - Insoluble in water and methanol. Complies. Identification. Reaction positive. Complies. Impurity Test. Claim. Result. Any single Impurity. ≤0.1%.

Mar 25, 2016 - Acetonitrile. ≤0.041%. Not Detected. Ethanol. ≤0.5%. Not Detected. N, N-dimethylformamide. ≤0.088%. Not Detected. Water. ≤5.0%. 0.43%.

S oluble in glycerol and water. Complies. Impurity Test. Claim. Result. Melting Point. 119-122°C. 120.1-120.7°C. Absorbance. 476-506. 489. Chlorides. 0.014%.

Apr 24, 2017 - Impurity Test. Claim. Result. Impurity A. ≤0.1%. Not Detected. Acetidin. ≤0.5%. Not Detected. Dichloromethane. ≤0.06%. Not Detected.

Nov 7, 2018 - Acetonitrile. ≤0.041%. Not Detected. Ethanol. ≤0.5%. Not Detected. N, N-dimethylformamide. ≤0.088%. Not Detected. Water. ≤5.0%. 1.97%.

Feb 16, 2016 - ≤0.5%. Not Detected. Acetonitrile. ≤0.041%. Not Detected. Ethanol. ≤0.5%. 0.08%. N, N-dimethylformamide. ≤0.088%. Not Detected. Water.