analytical report amazonaws com
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ANALYTICAL REPORT
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TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Road Nashville, TN 37204 Tel: 800-765-0980
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TestAmerica Job ID: NUC3001 Client Project/Site: Property ID# 908055 Client Project Description: EHS Special Project (PA) - Champdale - 908055
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For: SAIC Energy, Environment & Infrastructure, LLC/CHK 3700 West Robinson, Suite 200 Norman, OK 73072 Attn: Aria Archie
Authorized for release by: 03/24/2011 12:38:16 PM Gail A Lage Program Manager - National Accounts [email protected] Designee for John Smeathers Project Manager [email protected]
Results relate only to the items tested and the sample(s) as received by the laboratory. The test results in this report meet all 2003 NELAC requirements for accredited parameters, exceptions are noted in this report. Pursuant to NELAC, this report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
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Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Table of Contents Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
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Sample Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
NUC3001-01
0316201122801
Ground Water
03/16/11 10:50
03/18/11 08:30
NUC3001-02
Trip Blank
Water
03/16/11 00:01
03/18/11 08:30
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Case Narrative Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
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Job ID: NUC3001
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Laboratory: TestAmerica Nashville
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Narrative
The samples were received in good order and condition in the following cooler(s). Any exception would be noted on the Cooler Receipt Form and/or explained in further detail in the below narrative.
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Cooler ID # & Temperature 6773 0.5 C
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The samples were received the second day after collection potentially providing insufficient holding time for the MBAS and Turbidity analyses. The client requests we proceed as received. The lab expedited these samples as much as possible to secure the holding time. If the holding time was not met, the analysis was flagged with an "HT3" qualifier in the report. No further action was taken.
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Qualifier Definition/Glossary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
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Qualifiers
3
Metals
4
Qualifier
Qualifier Description
M7
The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).
M8
The MS and/or MSD were below the acceptance limits. See Blank Spike (LCS).
MHA
Due to high levels of analyte in the sample, the MS/MSD calculation does not provide useful spike recovery information. See Blank Spike (LCS). No results were reported for the MS/MSD. The sample used for the MS/MSD required dilution due to the sample matrix. Because of this, the spike compounds were diluted below the detection limit.
MNR
5 6 7
WetChem Qualifier
Qualifier Description
HT3
Sample received with insufficient holding time remaining for analysis to be performed within the method's holding time requirements.
MHA
Due to high levels of analyte in the sample, the MS/MSD calculation does not provide useful spike recovery information. See Blank Spike (LCS). Due to the low levels of analyte in the sample, the duplicate RPD calculation does not provide useful information.
R4
1
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TCLP
10
Qualifier
Qualifier Description
HTI
The holding time for this test is immediate. The laboratory measurement, therefore, may not be suitable for compliance purposes.
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Glossary
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Abbreviation
These commonly used abbreviations may or may not be present in this report.
¤
Listed under the "D" column to designate that the result is reported on a dry weight basis.
EPA
United States Environmental Protection Agency
ND
Not Detected above the reporting level.
MDL
Method Detection Limit
RL
Reporting Limit
RE, RE1 (etc.)
Indicates a Re-extraction or Reanalysis of the sample.
%R
Percent Recovery
RPD
Relative Percent Difference, a measure of the relative difference between two points.
TestAmerica Nashville
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Analytical Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Client Sample ID: 0316201122801
Lab Sample ID: NUC3001-01
Date Collected: 03/16/11 10:50 Date Received: 03/18/11 08:30 Sampler Name: Mike Melito 228
Matrix: Ground Water
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Sampler Phone Number: (405) 321-3895
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Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B Analyte
1
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
5
Benzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:18
1.00
Ethylbenzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:18
1.00
1.99
0.500
ug/L
03/21/11 10:05
03/22/11 16:18
1.00
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:18
1.00
7
Dil Fac
8
Toluene Xylenes, total Surrogate
Limits
Prepared
Analyzed
1,2-Dichloroethane-d4
105
63 - 140
03/21/11 10:05
03/22/11 16:18
1.00
Dibromofluoromethane
108
73 - 131
03/21/11 10:05
03/22/11 16:18
1.00
Toluene-d8
118
80 - 120
03/21/11 10:05
03/22/11 16:18
1.00
91
79 - 125
03/21/11 10:05
03/22/11 16:18
1.00
Prepared
Analyzed
4-Bromofluorobenzene
% Recovery Qualifier
Method: RSK 175 - Methane, Ethane, and Ethene by GC - dissolved Analyte
RL
Result Qualifier
MDL Unit
D
Dil Fac
Ethane
ND
0.0260
mg/L
03/21/11 09:00
03/21/11 10:49
1.00
Propane
ND
0.0340
mg/L
03/21/11 09:00
03/21/11 10:49
1.00
Surrogate
Acetylene
% Recovery Qualifier
101
Limits
Prepared
Analyzed
70 - 122
03/21/11 09:00
03/21/11 10:49
Dil Fac
1.00
Method: RSK 175 - Methane, Ethane, and Ethene by GC - dissolved - RE1 Analyte
Methane
RL
Result Qualifier
0.130
2.03
MDL Unit
D
mg/L
Prepared
Analyzed
03/21/11 09:00
03/21/11 10:53
Dil Fac
5.00
Method: SW846 6010C - Total Metals by EPA 6010C Analyte
Arsenic
RL
Result Qualifier
MDL Unit
Prepared
Analyzed
ND
0.0100
mg/L
D
03/19/11 09:13
03/21/11 12:57
Dil Fac
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
0.659
0.0100
Cadmium
ND
0.00100
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Calcium
58.0
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Iron
0.624
0.0500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Lead
0.0375
0.00500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Magnesium
11.7
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Manganese
0.582
0.0150
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Potassium
2.51
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Selenium
ND
0.0100
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Silver
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Sodium
18.6
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Sulfur
7.41
0.500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Barium
Chromium
Method: SW846 7470A - Mercury by EPA Methods 7470A/7471A Analyte
Mercury
Result Qualifier
ND
RL
0.000200
MDL Unit
D
mg/L
Prepared
Analyzed
03/21/11 10:25
03/21/11 13:53
Dil Fac
1.00
Method: EPA 180.1 - General Chemistry Parameters Analyte
Result Qualifier
Turbidity
ND HT3
RL
MDL Unit
1.00
NTU
RL
MDL Unit
D
Prepared
Analyzed
03/18/11 14:31
03/18/11 14:31
Dil Fac
1.00
Method: EPA 300.0 - General Chemistry Parameters Analyte
Chloride
Result Qualifier
21.7
5.00
mg/L
D
Prepared
Analyzed
03/18/11 14:32
03/19/11 16:17
Dil Fac
5.00
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Analytical Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Client Sample ID: 0316201122801
Lab Sample ID: NUC3001-01
Date Collected: 03/16/11 10:50 Date Received: 03/18/11 08:30 Sampler Name: Mike Melito 228
Matrix: Ground Water
3
Sampler Phone Number: (405) 321-3895
4
Method: EPA 300.0 - General Chemistry Parameters (Continued) Analyte
Sulfate
RL
Result Qualifier
5.00
18.7
MDL Unit
D
mg/L
Prepared
Analyzed
03/18/11 14:32
03/19/11 16:17
Prepared
Analyzed
Dil Fac
5.00
Method: SM 2320B - General Chemistry Parameters Analyte
RL
Result Qualifier
MDL Unit
D
Dil Fac
Bicarbonate Alkalinity as CaCO3
192
10.0
mg/L
03/18/11 16:29
03/19/11 02:02
1.00
Carbonate as CaCO3
ND
10.0
mg/L
03/18/11 16:39
03/19/11 02:02
1.00
Prepared
Analyzed
03/22/11 22:24
03/23/11 03:28
Prepared
Analyzed
03/23/11 10:12
03/23/11 13:13
Method: SM 2320B - General Chemistry Parameters - RE1 Analyte
Bicarbonate Alkalinity as CaCO3
RL
Result Qualifier
10.0
181
MDL Unit
D
mg/L
Dil Fac
1.00
Method: SM2510 B - General Chemistry Parameters Analyte
Specific conductance
RL
Result Qualifier
10.0
516
MDL Unit
D
umho/cm
Dil Fac
1.00
Method: SM2540 C - General Chemistry Parameters - dissolved Analyte
Total Dissolved Solids
Result Qualifier
248
RL
10.0
MDL Unit
D
mg/L
Prepared
Analyzed
03/19/11 23:30
03/19/11 23:30
Dil Fac
1.00
Method: SM2540 D - General Chemistry Parameters Analyte
Total Suspended Solids
Result Qualifier
3.43
RL
1.43
MDL Unit
D
mg/L
Prepared
Analyzed
03/21/11 19:04
03/21/11 19:04
Dil Fac
1.43
Method: SM5540 C - General Chemistry Parameters Analyte
MBAS (mol.wt 320)
Result Qualifier
ND HT3
RL
0.0500
MDL Unit
D
mg/L
Prepared
Analyzed
03/18/11 13:05
03/18/11 13:05
Dil Fac
1.00
Method: EPA 1664A - General Chemistry Parameters Analyte
Oil & Grease HEM
Result Qualifier
ND
RL
5.75
MDL Unit
D
mg/L
Prepared
Analyzed
03/23/11 10:00
03/23/11 16:28
Dil Fac
1.00
Method: EPA 170.1 - General Chemistry Parameters Analyte
Temperature of pH determination
Result Qualifier
23.4 HTI
RL
0.00
MDL Unit
D
Deg C
Prepared
Analyzed
03/18/11 15:30
03/18/11 15:30
Dil Fac
1.00
Method: SM 4500 H B - General Chemistry Parameters Analyte
pH
Result Qualifier
7.60 HTI
1
RL
0.100
MDL Unit
pH Units
D
Prepared
Analyzed
03/18/11 15:30
03/18/11 15:30
Dil Fac
1.00
TestAmerica Nashville
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Analytical Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Client Sample ID: Trip Blank
Lab Sample ID: NUC3001-02
Date Collected: 03/16/11 00:01 Date Received: 03/18/11 08:30 Sampler Name:
Matrix: Water
3
Sampler Phone Number: (405) 321-3895
4
Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B Analyte
1
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
5
Benzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:49
1.00
Ethylbenzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:49
1.00
Toluene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:49
1.00
Xylenes, total
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:49
1.00
7
Dil Fac
8
Surrogate
% Recovery Qualifier
Limits
Prepared
Analyzed
1,2-Dichloroethane-d4
99
63 - 140
03/21/11 10:05
03/22/11 16:49
1.00
Dibromofluoromethane
103
73 - 131
03/21/11 10:05
03/22/11 16:49
1.00
Toluene-d8
118
80 - 120
03/21/11 10:05
03/22/11 16:49
1.00
89
79 - 125
03/21/11 10:05
03/22/11 16:49
1.00
4-Bromofluorobenzene
6
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Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B
3
Lab Sample ID: 11C5504-BLK1 Matrix: Water Analysis Batch: U004725
Client Sample ID: 11C5504-BLK1 Prep Type: total Prep Batch: 11C5504_P Blank Blank
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
Benzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 13:14
1.00
Ethylbenzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 13:14
1.00
Toluene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 13:14
1.00
Xylenes, total
ND
0.500
ug/L
03/21/11 10:05
03/22/11 13:14
1.00
Limits
Prepared
Analyzed
Blank Blank Surrogate
% Recovery Qualifier
Dil Fac
1,2-Dichloroethane-d4
100
63 - 140
03/21/11 10:05
03/22/11 13:14
1.00
Dibromofluoromethane
104
73 - 131
03/21/11 10:05
03/22/11 13:14
1.00
Toluene-d8
111
80 - 120
03/21/11 10:05
03/22/11 13:14
1.00
90
79 - 125
03/21/11 10:05
03/22/11 13:14
1.00
4-Bromofluorobenzene
Lab Sample ID: 11C5504-BS1 Matrix: Water Analysis Batch: U004725
Client Sample ID: 11C5504-BS1 Prep Type: total Prep Batch: 11C5504_P Spike
Analyte
Added
LCS LCS Result Qualifier
% Rec. Unit
D
% Rec
Limits
Benzene
50.0
49.2
ug/L
98
80 - 121
Ethylbenzene
50.0
50.9
ug/L
102
78 - 133
Toluene
50.0
56.5
ug/L
113
78 - 125
Xylenes, total
150
153
ug/L
102
78 - 134
LCS LCS % Recovery Qualifier
Limits
1,2-Dichloroethane-d4
97
63 - 140
Dibromofluoromethane
107
73 - 131
Toluene-d8
109
80 - 120
86
79 - 125
Surrogate
4-Bromofluorobenzene
Lab Sample ID: 11C5504-BSD1 Matrix: Water Analysis Batch: U004725
Client Sample ID: 11C5504-BSD1 Prep Type: total Prep Batch: 11C5504_P
Analyte
Spike
LCS Dup LCS Dup
Added
Result Qualifier
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
Benzene
50.0
47.1
ug/L
94
80 - 121
4
12
Ethylbenzene
50.0
50.4
ug/L
101
78 - 133
1
12
Toluene
50.0
56.2
ug/L
112
78 - 125
0.5
35
Xylenes, total
150
152
ug/L
102
78 - 134
0.6
18
LCS Dup LCS Dup % Recovery Qualifier
Limits
1,2-Dichloroethane-d4
93
63 - 140
Dibromofluoromethane
107
73 - 131
Toluene-d8
115
80 - 120
88
79 - 125
Surrogate
4-Bromofluorobenzene
1
TestAmerica Nashville
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Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: RSK 175 - Methane, Ethane, and Ethene by GC
3
Lab Sample ID: 11C4872-BLK1 Matrix: Water Analysis Batch: U004542
Client Sample ID: 11C4872-BLK1 Prep Type: dissolved Prep Batch: 11C4872_P Blank Blank
Analyte
RL
Result Qualifier
MDL Unit
D
Prepared
Analyzed
Dil Fac
Methane
ND
0.0260
mg/L
03/21/11 09:00
03/21/11 09:15
1.00
Ethene
ND
0.0260
mg/L
03/21/11 09:00
03/21/11 09:15
1.00
Ethane
ND
0.0260
mg/L
03/21/11 09:00
03/21/11 09:15
1.00
Propane
ND
0.0340
mg/L
03/21/11 09:00
03/21/11 09:15
1.00
Limits
Prepared
Analyzed
70 - 122
03/21/11 09:00
03/21/11 09:15
Blank Blank Surrogate
% Recovery Qualifier
Acetylene
106
Lab Sample ID: 11C4872-BS1 Matrix: Water Analysis Batch: U004542
Dil Fac
1.00
Client Sample ID: 11C4872-BS1 Prep Type: dissolved Prep Batch: 11C4872_P Spike
LCS LCS
% Rec.
Analyte
Added
Methane
0.273
0.295
mg/L
108
80 - 120
Ethene
0.479
0.465
mg/L
97
80 - 120
Ethane
0.512
0.569
mg/L
111
80 - 120
Propane
0.754
0.824
mg/L
109
80 - 120
Result Qualifier
Unit
D
% Rec
Limits
% Recovery Qualifier
Limits
Acetylene
99
70 - 122
Lab Sample ID: 11C4872-BSD1 Matrix: Water Analysis Batch: U004542
Client Sample ID: 11C4872-BSD1 Prep Type: dissolved Prep Batch: 11C4872_P Spike
LCS Dup LCS Dup
Analyte
Added
Result Qualifier
Methane
0.273
0.293
mg/L
107
Ethene
0.479
0.458
mg/L
96
Ethane
0.512
0.566
mg/L
Propane
0.754
0.821
mg/L
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
80 - 120
0.7
33
80 - 120
1
29
110
80 - 120
0.6
30
109
80 - 120
0.4
33
LCS Dup LCS Dup Surrogate
% Recovery Qualifier
Limits
Acetylene
88
70 - 122
Lab Sample ID: 11C4872-MS1 Matrix: Water Analysis Batch: U004542
Client Sample ID: NUC2978-01 Prep Type: dissolved Prep Batch: 11C4872_P Spike
Matrix Spike Matrix Spike
% Rec.
Analyte
Result Qualifier
Methane
0.0252
0.273
0.308
mg/L
Ethene
ND
0.479
0.441
Ethane
ND
0.512
0.542
Propane
ND
0.754
0.786
Added
Result Qualifier
Unit
D
% Rec
Limits
103
46 - 142
mg/L
92
71 - 120
mg/L
106
71 - 120
mg/L
104
46 - 142
Matrix Spike Matrix Spike Surrogate
% Recovery Qualifier
Limits
Acetylene
87
70 - 122
TestAmerica Nashville
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LCS LCS Surrogate
Sample Sample
1
03/24/2011
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: RSK 175 - Methane, Ethane, and Ethene by GC (Continued)
3
Lab Sample ID: 11C4872-MSD1 Matrix: Water Analysis Batch: U004542
Client Sample ID: NUC2978-01 Prep Type: dissolved Prep Batch: 11C4872_P Spike Matrix Spike Dup Matrix Spike Dup
Sample Sample Analyte
Result Qualifier
Methane
Added
Result Qualifier
% Rec.
Unit
D
% Rec
RPD
Limits
RPD
Limit
0.0252
0.273
0.304
mg/L
102
46 - 142
1
33
Ethene
ND
0.479
0.431
mg/L
90
71 - 120
2
29
Ethane
ND
0.512
0.534
mg/L
104
71 - 120
2
30
Propane
ND
0.754
0.775
mg/L
103
46 - 142
1
33
% Recovery Qualifier
Limits
Acetylene
78
70 - 122
Client Sample ID: 11C4553-BLK1 Prep Type: total Prep Batch: 11C4553_P Blank Blank RL
Result Qualifier
MDL Unit
Prepared
Analyzed
Arsenic
ND
0.0100
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Barium
ND
0.0100
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Cadmium
ND
0.00100
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Calcium
ND
1.00
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Chromium
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Iron
ND
0.0500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Lead
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Magnesium
ND
1.00
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Manganese
ND
0.0150
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Potassium
ND
1.00
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Selenium
ND
0.0100
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Silver
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Sodium
ND
1.00
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Sulfur
ND
0.500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
D
Lab Sample ID: 11C4553-BS1 Matrix: Water Analysis Batch: 11C4553 Spike
LCS LCS
% Rec.
Added
Result Qualifier
Unit
Arsenic
0.0500
0.0514
mg/L
103
80 - 120
D
% Rec
Limits
2.00
2.02
mg/L
101
80 - 120
0.0500
0.0484
mg/L
97
80 - 120
5.00
4.69
mg/L
94
80 - 120
0.200
0.189
mg/L
95
80 - 120
1.00
0.951
mg/L
95
80 - 120
0.0500
0.0505
mg/L
101
80 - 120
Magnesium
5.00
4.62
mg/L
92
80 - 120
Manganese
0.500
0.479
mg/L
96
80 - 120
Potassium
5.00
4.51
mg/L
90
80 - 120
Selenium
0.0500
0.0498
mg/L
100
80 - 120
Silver
0.0500
0.0496
mg/L
99
80 - 120
Chromium Iron Lead
Dil Fac
Client Sample ID: 11C4553-BS1 Prep Type: total Prep Batch: 11C4553_P
Analyte
Calcium
6 7
10
Lab Sample ID: 11C4553-BLK1 Matrix: Water Analysis Batch: 11C4553
Cadmium
5
9
Method: SW846 6010C - Total Metals by EPA 6010C
Barium
4
8
Matrix Spike Dup Matrix Spike Dup Surrogate
Analyte
1
Sodium
5.00
4.82 MNR
mg/L
96
80 - 120
Sulfur
1.00
1.03
mg/L
103
80 - 120
TestAmerica Nashville
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03/24/2011
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Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SW846 6010C - Total Metals by EPA 6010C (Continued)
3
Lab Sample ID: 11C4553-BSD1 Matrix: Water Analysis Batch: 11C4553
Client Sample ID: 11C4553-BSD1 Prep Type: total Prep Batch: 11C4553_P Spike
LCS Dup LCS Dup
Analyte
Added
Result Qualifier
Unit
Arsenic
0.0500
0.0519
mg/L
104
Barium
2.00
2.09
mg/L
104
0.0500
0.0493
mg/L
5.00
4.89
mg/L
0.200
0.193
1.00
0.975
Cadmium Calcium Chromium Iron Lead
% Rec. D
% Rec
Limits
RPD RPD
Limit
80 - 120
1
20
80 - 120
3
20
99
80 - 120
2
20
98
80 - 120
4
20
mg/L
96
80 - 120
2
20
mg/L
98
80 - 120
3
20
0.0500
0.0525
mg/L
105
80 - 120
4
20
Magnesium
5.00
4.73
mg/L
95
80 - 120
2
20
Manganese
0.500
0.492
mg/L
98
80 - 120
3
20
Potassium
5.00
4.67
mg/L
93
80 - 120
4
20
Selenium
0.0500
0.0533
mg/L
107
80 - 120
7
20
Silver
0.0500
0.0494
mg/L
99
80 - 120
0.4
20
Sodium
5.00
4.97
mg/L
99
80 - 120
3
20
Sulfur
1.00
1.04
mg/L
104
80 - 120
0.6
20
Lab Sample ID: 11C4553-MS1 Matrix: Water Analysis Batch: 11C4553
Client Sample ID: NUC2783-02 Prep Type: total Prep Batch: 11C4553_P Sample Sample
Analyte
Arsenic Barium
Result Qualifier
0.274
Spike Added
0.0500
Matrix Spike Matrix Spike Result Qualifier
% Rec. Unit
D
% Rec
Limits
0.270 MHA
mg/L
-8
75 - 125
11.3 MHA
mg/L
-142
75 - 125
mg/L
65
75 - 125
2480 MHA
mg/L
75 - 125
0.233 M8
mg/L
-3910 0 55
mg/L
-3450
75 - 125
mg/L
307
75 - 125
14.1
2.00
0.00600
0.0500
Calcium
4440
5.00
Chromium
0.123
0.200
172
1.00
0.171
0.0500
Magnesium
525
5.00
398 MHA
mg/L
-2550
75 - 125
Manganese
4.53
0.500
3.55 MHA
mg/L
-196
75 - 125
Potassium
184
5.00
173 MHA
mg/L
-214
75 - 125
Selenium
ND
0.0500
0.0544
mg/L
109
75 - 125
Silver
ND
0.0500
0.0510
mg/L
102
75 - 125
Sulfur
156
1.00
mg/L
-2140
75 - 125
Cadmium
Iron Lead
0.0386 M8
138 MHA 0.324 M7
134 MHA
Lab Sample ID: 11C4553-MSD1 Matrix: Water Analysis Batch: 11C4553
75 - 125
Client Sample ID: NUC2783-02 Prep Type: total Prep Batch: 11C4553_P Sample Sample
Analyte
Result Qualifier
Spike Matrix Spike Dup Matrix Spike Dup Added
Result Qualifier
Unit
% Rec. D
% Rec
Limits
RPD RPD
Limit
Arsenic
0.274
0.0500
0.286 MHA
mg/L
24
75 - 125
6
20
Barium
14.1
2.00
11.5 MHA
mg/L
-132
75 - 125
2
20
0.00600
0.0500
mg/L
66
75 - 125
0.8
20
Calcium
4440
5.00
2520 MHA
mg/L
75 - 125
1
20
Chromium
0.123
0.200
0.236 M8
mg/L
-3840 0 56
75 - 125
1
20
172
1.00
mg/L
-3280
75 - 125
1
20
0.171
0.0500
mg/L
333
75 - 125
4
20
Magnesium
525
5.00
406 MHA
mg/L
-2390
75 - 125
2
20
Manganese
4.53
0.500
3.61 MHA
mg/L
-184
75 - 125
2
20
Potassium
184
5.00
176 MHA
mg/L
-150
75 - 125
2
20
Cadmium
Iron Lead
1
0.0389 M8
139 MHA 0.338 M7
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Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SW846 6010C - Total Metals by EPA 6010C (Continued) Lab Sample ID: 11C4553-MSD1 Matrix: Water Analysis Batch: 11C4553
Client Sample ID: NUC2783-02 Prep Type: total Prep Batch: 11C4553_P Sample Sample
Analyte
Result Qualifier
Spike Matrix Spike Dup Matrix Spike Dup Added
Result Qualifier
Unit
% Rec. D
% Rec
RPD
Limits
RPD
Limit
Selenium
ND
0.0500
0.0525
mg/L
105
75 - 125
4
20
Silver
ND
0.0500
0.0522
mg/L
104
75 - 125
2
20
Sulfur
156
1.00
mg/L
-1960
75 - 125
1
20
136 MHA
Method: SW846 7470A - Mercury by EPA Methods 7470A/7471A Client Sample ID: 11C4512-BLK1 Prep Type: total Prep Batch: 11C4512_P Blank Blank RL
Result Qualifier
Mercury
ND
MDL Unit
0.000200
D
mg/L
Prepared
Analyzed
03/21/11 10:25
03/21/11 13:01
Lab Sample ID: 11C4512-BS1 Matrix: Water Analysis Batch: 11C4512 LCS LCS
Spike Added
Mercury
0.00100
Result Qualifier
0.000916
D
mg/L
Spike
LCS Dup LCS Dup
Added
Result Qualifier
Mercury
0.00100
92
0.000908
D
mg/L
% Rec
91
RPD
Limits
80 - 120
RPD
Limit
0.9
20
Client Sample ID: NUC2982-01 Prep Type: total Prep Batch: 11C4512_P Sample Sample Result Qualifier
ND
Spike
Matrix Spike Matrix Spike
Added
Result Qualifier
0.00100
0.000975
% Rec. Unit
D
mg/L
% Rec
97
Lab Sample ID: 11C4512-MSD1 Matrix: Water Analysis Batch: 11C4512
Limits
75 - 125
Client Sample ID: NUC2982-01 Prep Type: total Prep Batch: 11C4512_P Sample Sample
Mercury
Limits
80 - 120
% Rec. Unit
Lab Sample ID: 11C4512-MS1 Matrix: Water Analysis Batch: 11C4512
Analyte
% Rec
Client Sample ID: 11C4512-BSD1 Prep Type: total Prep Batch: 11C4512_P
Analyte
Mercury
1.00
% Rec. Unit
Lab Sample ID: 11C4512-BSD1 Matrix: Water Analysis Batch: 11C4512
Analyte
Dil Fac
Client Sample ID: 11C4512-BS1 Prep Type: total Prep Batch: 11C4512_P
Analyte
Result Qualifier
ND
Spike Matrix Spike Dup Matrix Spike Dup Added
Result Qualifier
0.00100
0.000943
% Rec.
Unit
D
mg/L
% Rec
94
RPD
Limits
RPD
Limit
3
20
75 - 125
Method: EPA 180.1 - General Chemistry Parameters Lab Sample ID: 11C4582-BLK1 Matrix: Water Analysis Batch: 11C4582
Client Sample ID: 11C4582-BLK1 Prep Type: total Prep Batch: 11C4582_P Blank Blank
Analyte
Turbidity
Result Qualifier
ND
3 4 5 6 7 8
Lab Sample ID: 11C4512-BLK1 Matrix: Water Analysis Batch: 11C4512 Analyte
1
RL
MDL Unit
1.00
NTU
D
Prepared
Analyzed
03/18/11 14:31
03/18/11 14:31
Dil Fac
1.00
TestAmerica Nashville
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03/24/2011
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Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: EPA 180.1 - General Chemistry Parameters (Continued)
3
Lab Sample ID: 11C4582-BS1 Matrix: Water Analysis Batch: 11C4582
Client Sample ID: 11C4582-BS1 Prep Type: total Prep Batch: 11C4582_P LCS LCS
Spike Analyte
Added
Turbidity
Result Qualifier
5.00
5.00
D
NTU
100
Spike
LCS Dup LCS Dup
Added
Result Qualifier
5.00
5.00
D
NTU
% Rec
100
RPD
Limits
RPD
Limit
0
15
90 - 110
Duplicate Duplicate
Result Qualifier
Result Qualifier
ND
ND
RPD Unit
D
RPD
NTU
Limit
15
Lab Sample ID: 11C4582-DUP2 Matrix: Water Analysis Batch: 11C4582
Client Sample ID: NUC3009-01 Prep Type: total Prep Batch: 11C4582_P Duplicate Duplicate
Sample Sample
Turbidity
6
Client Sample ID: NUC2987-01 Prep Type: total Prep Batch: 11C4582_P Sample Sample
Analyte
90 - 110
% Rec. Unit
Lab Sample ID: 11C4582-DUP1 Matrix: Water Analysis Batch: 11C4582
Turbidity
Limits
Client Sample ID: 11C4582-BSD1 Prep Type: total Prep Batch: 11C4582_P
Turbidity
Analyte
% Rec
Result Qualifier
Result Qualifier
0.400
0.400
RPD Unit
D
RPD
Limit
0
15
NTU
Method: EPA 300.0 - General Chemistry Parameters Lab Sample ID: 11C4583-BLK1 Matrix: Water Analysis Batch: U004576
Client Sample ID: 11C4583-BLK1 Prep Type: total Prep Batch: 11C4583_P Blank Blank
Analyte
RL
Result Qualifier
MDL Unit
D
Prepared
Analyzed
Chloride
ND
1.00
mg/L
03/18/11 14:32
03/19/11 14:16
1.00
Sulfate
ND
1.00
mg/L
03/18/11 14:32
03/19/11 14:16
1.00
Lab Sample ID: 11C4583-BS1 Matrix: Water Analysis Batch: U004576 Spike
LCS LCS
% Rec.
Added
Chloride
3.00
2.85
mg/L
95
90 - 110
Sulfate
15.0
14.6
mg/L
97
90 - 110
Result Qualifier
Unit
D
Lab Sample ID: 11C4583-MS1 Matrix: Water Analysis Batch: U004576
% Rec
Limits
Client Sample ID: NUC2986-01 Prep Type: total Prep Batch: 11C4583_P Sample Sample
Analyte
Dil Fac
Client Sample ID: 11C4583-BS1 Prep Type: total Prep Batch: 11C4583_P
Analyte
Result Qualifier
Spike Added
Matrix Spike Matrix Spike
% Rec.
Result Qualifier
Unit
D
% Rec
Limits
Chloride
140
15.0
317 MHA
mg/L
1180
80 - 120
Sulfate
3.38
75.0
72.6
mg/L
92
80 - 120
TestAmerica Nashville
Page 14 of 29
4 5
% Rec. Unit
Lab Sample ID: 11C4582-BSD1 Matrix: Water Analysis Batch: 11C4582 Analyte
1
03/24/2011
7 8 9 10 11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: EPA 300.0 - General Chemistry Parameters (Continued)
3
Lab Sample ID: 11C4583-DUP1 Matrix: Water Analysis Batch: U004576
Client Sample ID: NUC3019-01 Prep Type: total Prep Batch: 11C4583_P
4
RPD
5
Duplicate Duplicate
Sample Sample Analyte
Result Qualifier
Result Qualifier
Unit
D
RPD
Limit
Chloride
115
115
mg/L
0.4
20
Sulfate
5.50
6.70
mg/L
20
20
Lab Sample ID: 11C4645-BLK1 Matrix: Water Analysis Batch: 11C4645
Client Sample ID: 11C4645-BLK1 Prep Type: total Prep Batch: 11C4645_P Blank Blank Result Qualifier
Bicarbonate Alkalinity as CaCO3
ND
RL
MDL Unit
10.0
D
mg/L
Prepared
Analyzed
03/18/11 16:29
03/19/11 00:51
Lab Sample ID: 11C4645-DUP1 Matrix: Water Analysis Batch: 11C4645
Bicarbonate Alkalinity as CaCO3
Result Qualifier
190
187
RPD Unit
D
Limit
2
20
Client Sample ID: NUC2954-01 Prep Type: total Prep Batch: 11C4645_P Duplicate Duplicate
Sample Sample
Bicarbonate Alkalinity as CaCO3
RPD
mg/L
Result Qualifier
Result Qualifier
39.2
38.5
RPD Unit
D
RPD
Limit
2
20
mg/L
Lab Sample ID: 11C4657-BLK1 Matrix: Water Analysis Batch: 11C4657
Client Sample ID: 11C4657-BLK1 Prep Type: total Prep Batch: 11C4657_P Blank Blank
Analyte
Result Qualifier
Carbonate as CaCO3
ND
RL
MDL Unit
10.0
D
mg/L
Prepared
Analyzed
03/18/11 16:39
03/19/11 00:51
Lab Sample ID: 11C4657-DUP1 Matrix: Water Analysis Batch: 11C4657
Carbonate as CaCO3
Dil Fac
1.00
Client Sample ID: NUC2952-01 Prep Type: total Prep Batch: 11C4657_P Duplicate Duplicate
Sample Sample Analyte
Result Qualifier
Result Qualifier
ND
ND
RPD Unit
D
RPD
mg/L
Limit
20
Lab Sample ID: 11C5551-BLK1 Matrix: Water Analysis Batch: 11C5551
Client Sample ID: 11C5551-BLK1 Prep Type: total Prep Batch: 11C5551_P Blank Blank
Analyte
Bicarbonate Alkalinity as CaCO3
Result Qualifier
ND
RL
10.0
MDL Unit
mg/L
D
Prepared
Analyzed
03/22/11 22:25
03/23/11 02:16
Dil Fac
1.00
TestAmerica Nashville
Page 15 of 29
8 9 10
1.00
Duplicate Duplicate
Result Qualifier
Lab Sample ID: 11C4645-DUP2 Matrix: Water Analysis Batch: 11C4645 Analyte
Dil Fac
Client Sample ID: NUC2952-01 Prep Type: total Prep Batch: 11C4645_P Sample Sample
Analyte
6 7
Method: SM 2320B - General Chemistry Parameters
Analyte
1
03/24/2011
11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SM 2320B - General Chemistry Parameters (Continued)
3
Lab Sample ID: 11C5551-DUP1 Matrix: Water Analysis Batch: 11C5551
Bicarbonate Alkalinity as CaCO3
Client Sample ID: NUC2956-01RE1 Prep Type: total Prep Batch: 11C5551_P
4
RPD
5
Duplicate Duplicate
Sample Sample Analyte
Result Qualifier
Result Qualifier
98.5
99.9
Unit
D
RPD
Limit
1
20
mg/L
Method: SM2510 B - General Chemistry Parameters Client Sample ID: 11C5627-BLK1 Prep Type: total Prep Batch: 11C5627_P Blank Blank RL
Result Qualifier
Specific conductance
ND
MDL Unit
10.0
D
umho/cm
Prepared
Analyzed
03/23/11 10:12
03/23/11 13:13
Lab Sample ID: 11C5627-BS1 Matrix: Water Analysis Batch: 11C5627 LCS LCS
Spike Added
Specific conductance
Result Qualifier
1410
1430
Unit
D
umho/cm
% Rec
101
Limits
90 - 110
Client Sample ID: NUC0332-01RE1 Prep Type: total Prep Batch: 11C5627_P Duplicate Duplicate
Sample Sample
Specific conductance
1.00
% Rec.
Lab Sample ID: 11C5627-DUP1 Matrix: Water Analysis Batch: 11C5627 Analyte
Dil Fac
Client Sample ID: 11C5627-BS1 Prep Type: total Prep Batch: 11C5627_P
Analyte
Result Qualifier
Result Qualifier
93.2
94.2
RPD Unit
D
RPD
Limit
1
10
umho/cm
Method: SM2540 C - General Chemistry Parameters Lab Sample ID: 11C4897-BLK1 Matrix: Water Analysis Batch: 11C4897
Client Sample ID: 11C4897-BLK1 Prep Type: dissolved Prep Batch: 11C4897_P Blank Blank
Analyte
RL
Result Qualifier
Total Dissolved Solids
ND
MDL Unit
10.0
D
mg/L
Prepared
Analyzed
03/19/11 23:30
03/19/11 23:30
Lab Sample ID: 11C4897-BS1 Matrix: Water Analysis Batch: 11C4897 Spike Added
Total Dissolved Solids
100
LCS LCS Result Qualifier
90.0
D
ug/mL
% Rec
90
Limits
90 - 110
Client Sample ID: NUC3009-01 Prep Type: dissolved Prep Batch: 11C4897_P Sample Sample
Total Dissolved Solids
1.00
% Rec. Unit
Lab Sample ID: 11C4897-DUP1 Matrix: Water Analysis Batch: 11C4897 Analyte
Dil Fac
Client Sample ID: 11C4897-BS1 Prep Type: dissolved Prep Batch: 11C4897_P
Analyte
Result Qualifier
304
6 7
Lab Sample ID: 11C5627-BLK1 Matrix: Water Analysis Batch: 11C5627 Analyte
1
Duplicate Duplicate Result Qualifier
306
RPD Unit
mg/L
D
RPD
Limit
0.7
5
TestAmerica Nashville
Page 16 of 29
03/24/2011
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Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SM2540 D - General Chemistry Parameters
3
Lab Sample ID: 11C5102-BLK1 Matrix: Water Analysis Batch: 11C5102
Client Sample ID: 11C5102-BLK1 Prep Type: total Prep Batch: 11C5102_P Blank Blank
Analyte
RL
Result Qualifier
Total Suspended Solids
ND
MDL Unit
1.00
D
mg/L
Prepared
Analyzed
03/21/11 19:04
03/21/11 19:04
Lab Sample ID: 11C5102-BS1 Matrix: Water Analysis Batch: 11C5102 LCS LCS
Spike Added
Total Suspended Solids
Result Qualifier
100
97.7
D
mg/L
98
Result Qualifier
Result Qualifier
70.4
68.8
D
Total Suspended Solids
RPD
Limit
2
5
mg/L
Client Sample ID: 0316201122801 Prep Type: total Prep Batch: 11C5102_P Duplicate Duplicate
Sample Sample Result Qualifier
Result Qualifier
3.43
5.43 R4
RPD Unit
D
RPD
Limit
45
5
mg/L
Method: SM5540 C - General Chemistry Parameters Lab Sample ID: 11C4511-BLK1 Matrix: Water Analysis Batch: 11C4511
Client Sample ID: 11C4511-BLK1 Prep Type: total Prep Batch: 11C4511_P Blank Blank
Analyte
RL
Result Qualifier
MBAS (mol.wt 320)
ND
MDL Unit
0.0500
D
mg/L
Prepared
Analyzed
03/18/11 13:05
03/18/11 13:05
Lab Sample ID: 11C4511-BS1 Matrix: Water Analysis Batch: 11C4511
Dil Fac
1.00
Client Sample ID: 11C4511-BS1 Prep Type: total Prep Batch: 11C4511_P Spike
Analyte
Added
MBAS (mol.wt 320)
0.750
LCS LCS Result Qualifier
0.746
% Rec. Unit
D
mg/L
% Rec
99
Lab Sample ID: 11C4511-MS1 Matrix: Water Analysis Batch: 11C4511
Limits
80 - 120
Client Sample ID: NUC2953-01 Prep Type: total Prep Batch: 11C4511_P Sample Sample
Analyte
Result Qualifier
MBAS (mol.wt 320)
0.0313
Spike Added
0.750
Matrix Spike Matrix Spike Result Qualifier
0.768
% Rec. Unit
mg/L
D
% Rec
98
Limits
80 - 120
TestAmerica Nashville
Page 17 of 29
5 6 7 8 9
90 - 110
RPD Unit
4
Limits
Duplicate Duplicate
Lab Sample ID: 11C5102-DUP2 Matrix: Water Analysis Batch: 11C5102 Analyte
% Rec
Client Sample ID: NUC2446-01 Prep Type: total Prep Batch: 11C5102_P Sample Sample
Total Suspended Solids
1.00
% Rec. Unit
Lab Sample ID: 11C5102-DUP1 Matrix: Water Analysis Batch: 11C5102 Analyte
Dil Fac
Client Sample ID: 11C5102-BS1 Prep Type: total Prep Batch: 11C5102_P
Analyte
1
03/24/2011
10 11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SM5540 C - General Chemistry Parameters (Continued)
3
Lab Sample ID: 11C4511-MSD1 Matrix: Water Analysis Batch: 11C4511
Client Sample ID: NUC2953-01 Prep Type: total Prep Batch: 11C4511_P Sample Sample
Analyte
Result Qualifier
MBAS (mol.wt 320)
0.0313
Spike Matrix Spike Dup Matrix Spike Dup Added
Result Qualifier
0.750
0.772
% Rec.
Unit
D
mg/L
% Rec
99
RPD
Limits
80 - 120
RPD
Limit
0.6
20
Method: EPA 1664A - General Chemistry Parameters Client Sample ID: 11C5376-BLK1 Prep Type: total Prep Batch: 11C5376_P Blank Blank RL
Result Qualifier
Oil & Grease HEM
ND
MDL Unit
5.21
D
mg/L
Prepared
Analyzed
03/22/11 12:43
03/23/11 16:28
Lab Sample ID: 11C5376-BS1 Matrix: Water Analysis Batch: 11C5376 Analyte
Added
Oil & Grease HEM
40.0
LCS LCS Result Qualifier
36.9
Unit
D
mg/L
% Rec
92
Limits
78 - 114
Client Sample ID: 11C5376-BSD1 Prep Type: total Prep Batch: 11C5376_P
Analyte
Oil & Grease HEM
Spike
LCS Dup LCS Dup
Added
Result Qualifier
40.0
39.5
% Rec. Unit
D
mg/L
% Rec
99
Lab Sample ID: 11C5376-MS1 Matrix: Water Analysis Batch: 11C5376
Limits
78 - 114
RPD RPD
Limit
7
18
Client Sample ID: NUC1440-01 Prep Type: total Prep Batch: 11C5376_P Sample Sample
Oil & Grease HEM
1.00
% Rec.
Lab Sample ID: 11C5376-BSD1 Matrix: Water Analysis Batch: 11C5376
Analyte
Dil Fac
Client Sample ID: 11C5376-BS1 Prep Type: total Prep Batch: 11C5376_P Spike
Result Qualifier
1.15
Spike Added
40.0
Matrix Spike Matrix Spike Result Qualifier
41.8
% Rec. Unit
D
mg/L
% Rec
102
Limits
78 - 114
Method: EPA 170.1 - General Chemistry Parameters Lab Sample ID: 11C4508-DUP1 Matrix: Water Analysis Batch: 11C4508
Client Sample ID: NUC2986-01 Prep Type: total Prep Batch: 11C4508_P Sample Sample
Analyte
Temperature of pH determination
Result Qualifier
23.4
Duplicate Duplicate Result Qualifier
23.4
RPD Unit
D
Deg C
Lab Sample ID: 11C4508-DUP2 Matrix: Water Analysis Batch: 11C4508
Temperature of pH determination
RPD
Limit
0
200
Client Sample ID: NUC3008-01 Prep Type: total Prep Batch: 11C4508_P Sample Sample
Analyte
Result Qualifier
23.4
4 5 6 7
Lab Sample ID: 11C5376-BLK1 Matrix: Water Analysis Batch: 11C5376 Analyte
1
Duplicate Duplicate Result Qualifier
23.4
RPD Unit
Deg C
D
RPD
Limit
0
200
TestAmerica Nashville
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03/24/2011
8 9 10 11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SM 4500 H B - General Chemistry Parameters
3
Lab Sample ID: 11C4508-BS1 Matrix: Water Analysis Batch: 11C4508
Client Sample ID: 11C4508-BS1 Prep Type: total Prep Batch: 11C4508_P Spike
Analyte
Added
pH
7.00
LCS LCS Result Qualifier
6.97
D
pH Units
100
Added
pH
7.00
LCS LCS Result Qualifier
7.04
D
pH Units
% Rec
101
Result Qualifier
6.30
Result Qualifier
6.30
D
pH Units
RPD
Limit
0
10
Client Sample ID: NUC3008-01 Prep Type: total Prep Batch: 11C4508_P Sample Sample Result Qualifier
7.80
Duplicate Duplicate Result Qualifier
7.80
RPD Unit
pH Units
D
RPD
Limit
0
10
TestAmerica Nashville
Page 19 of 29
8 9
95 - 105
RPD Unit
7
Limits
Duplicate Duplicate
Lab Sample ID: 11C4508-DUP2 Matrix: Water Analysis Batch: 11C4508
pH
6
Client Sample ID: NUC2986-01 Prep Type: total Prep Batch: 11C4508_P Sample Sample
Analyte
95 - 105
% Rec. Unit
Lab Sample ID: 11C4508-DUP1 Matrix: Water Analysis Batch: 11C4508
pH
Limits
Client Sample ID: 11C4508-BS2 Prep Type: total Prep Batch: 11C4508_P Spike
Analyte
% Rec
4 5
% Rec. Unit
Lab Sample ID: 11C4508-BS2 Matrix: Water Analysis Batch: 11C4508 Analyte
1
03/24/2011
10 11 12
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
GCMS Volatiles
3
Prep Batch: 11C5504_P Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C5504-BS1
11C5504-BS1
total
Water
EPA 5030B
Prep Batch
11C5504-BSD1
11C5504-BSD1
total
Water
EPA 5030B
11C5504-BLK1
11C5504-BLK1
total
Water
EPA 5030B
NUC3001-01
0316201122801
total
Ground Water
EPA 5030B
NUC3001-02
Trip Blank
total
Water
EPA 5030B
4 5 6 7
Analysis Batch: U004725 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5504-BS1
11C5504-BS1
total
Water
SW846 8260B
11C5504_P
11C5504-BSD1
11C5504-BSD1
total
Water
SW846 8260B
11C5504_P
11C5504-BLK1
11C5504-BLK1
total
Water
SW846 8260B
11C5504_P
NUC3001-01
0316201122801
total
Ground Water
SW846 8260B
11C5504_P
NUC3001-02
Trip Blank
total
Water
SW846 8260B
11C5504_P
8 9 10
Pesticides
11
Prep Batch: 11C4872_P
12
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4872-BLK1
11C4872-BLK1
Dissolved
Water
RSK 175/3810
Prep Batch
11C4872-BS1
11C4872-BS1
Dissolved
Water
RSK 175/3810
11C4872-BSD1
11C4872-BSD1
Dissolved
Water
RSK 175/3810
11C4872-MS1
NUC2978-01
Dissolved
Water
RSK 175/3810
11C4872-MSD1
NUC2978-01
Dissolved
Water
RSK 175/3810
NUC3001-01
0316201122801
Dissolved
Ground Water
RSK 175/3810
NUC3001-01 - RE1
0316201122801
Dissolved
Ground Water
RSK 175/3810
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4872-BLK1
11C4872-BLK1
Dissolved
Water
RSK 175
11C4872_P
11C4872-BS1
11C4872-BS1
Dissolved
Water
RSK 175
11C4872_P
11C4872-BSD1
11C4872-BSD1
Dissolved
Water
RSK 175
11C4872_P
11C4872-MS1
NUC2978-01
Dissolved
Water
RSK 175
11C4872_P
11C4872-MSD1
NUC2978-01
Dissolved
Water
RSK 175
11C4872_P
NUC3001-01
0316201122801
Dissolved
Ground Water
RSK 175
11C4872_P
NUC3001-01 - RE1
0316201122801
Dissolved
Ground Water
RSK 175
11C4872_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4512-BLK1
11C4512-BLK1
total
Water
SW846 7470A
11C4512_P
11C4512-BS1
11C4512-BS1
total
Water
SW846 7470A
11C4512_P
11C4512-BSD1
11C4512-BSD1
total
Water
SW846 7470A
11C4512_P
11C4512-MS1
NUC2982-01
total
Water
SW846 7470A
11C4512_P
11C4512-MSD1
NUC2982-01
total
Water
SW846 7470A
11C4512_P
NUC3001-01
0316201122801
total
Ground Water
SW846 7470A
11C4512_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4512-BLK1
11C4512-BLK1
total
Water
EPA 7470
11C4512-BS1
11C4512-BS1
total
Water
EPA 7470
11C4512-BSD1
11C4512-BSD1
total
Water
EPA 7470
Analysis Batch: U004542
Metals Analysis Batch: 11C4512
Prep Batch: 11C4512_P
TestAmerica Nashville
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03/24/2011
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
Metals (Continued)
3
Prep Batch: 11C4512_P (Continued) Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4512-MS1
NUC2982-01
total
Water
EPA 7470
Prep Batch
11C4512-MSD1
NUC2982-01
total
Water
EPA 7470
NUC3001-01
0316201122801
total
Ground Water
EPA 7470
4 5 6
Analysis Batch: 11C4553 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4553-BLK1
11C4553-BLK1
total
Water
SW846 6010C
11C4553_P
11C4553-BS1
11C4553-BS1
total
Water
SW846 6010C
11C4553_P
11C4553-BSD1
11C4553-BSD1
total
Water
SW846 6010C
11C4553_P
11C4553-MS1
NUC2783-02
total
Water
SW846 6010C
11C4553_P
11C4553-MSD1
NUC2783-02
total
Water
SW846 6010C
11C4553_P
NUC3001-01
0316201122801
total
Ground Water
SW846 6010C
11C4553_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4553-BLK1
11C4553-BLK1
total
Water
11C4553-BS1
11C4553-BS1
total
Water
11C4553-BSD1
11C4553-BSD1
total
Water
11C4553-MS1
NUC2783-02
total
Water
11C4553-MSD1
NUC2783-02
total
Water
NUC3001-01
0316201122801
total
Ground Water
EPA 3010A / 6010 EPA 3010A / 6010 EPA 3010A / 6010 EPA 3010A / 6010 EPA 3010A / 6010 EPA 3010A / 6010
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4511-BLK1
11C4511-BLK1
total
Water
SM5540 C
11C4511_P
11C4511-BS1
11C4511-BS1
total
Water
SM5540 C
11C4511_P
11C4511-MS1
NUC2953-01
total
Water
SM5540 C
11C4511_P
11C4511-MSD1
NUC2953-01
total
Water
SM5540 C
11C4511_P
NUC3001-01
0316201122801
total
Ground Water
SM5540 C
11C4511_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4511-BLK1
11C4511-BLK1
total
Water
SM5540C
11C4511-BS1
11C4511-BS1
total
Water
SM5540C
11C4511-MS1
NUC2953-01
total
Water
SM5540C
11C4511-MSD1
NUC2953-01
total
Water
SM5540C
NUC3001-01
0316201122801
total
Ground Water
SM5540C
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4582-BLK1
11C4582-BLK1
total
Water
EPA 180.1
11C4582_P
11C4582-BS1
11C4582-BS1
total
Water
EPA 180.1
11C4582_P
11C4582-BSD1
11C4582-BSD1
total
Water
EPA 180.1
11C4582_P
11C4582-DUP1
NUC2987-01
total
Water
EPA 180.1
11C4582_P
11C4582-DUP2
NUC3009-01
total
Water
EPA 180.1
11C4582_P
NUC3001-01
0316201122801
total
Ground Water
EPA 180.1
11C4582_P
Prep Batch: 11C4553_P
8 9 10 11 12
WetChem Analysis Batch: 11C4511
Prep Batch: 11C4511_P
Analysis Batch: 11C4582
TestAmerica Nashville
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03/24/2011
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
WetChem (Continued)
3
Prep Batch: 11C4582_P Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4582-BLK1
11C4582-BLK1
total
Water
NO PREP
Prep Batch
11C4582-BS1
11C4582-BS1
total
Water
NO PREP
11C4582-BSD1
11C4582-BSD1
total
Water
NO PREP
11C4582-DUP1
NUC2987-01
total
Water
NO PREP
11C4582-DUP2
NUC3009-01
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4583-BLK1
11C4583-BLK1
total
Water
NO PREP
11C4583-BS1
11C4583-BS1
total
Water
NO PREP
11C4583-MS1
NUC2986-01
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
11C4583-DUP1
NUC3019-01
total
Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4645-BLK1
11C4645-BLK1
total
Water
SM 2320B
11C4645_P
11C4645-DUP1
NUC2952-01
total
Water
SM 2320B
11C4645_P
11C4645-DUP2
NUC2954-01
total
Water
SM 2320B
11C4645_P
NUC3001-01
0316201122801
total
Ground Water
SM 2320B
11C4645_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4645-BLK1
11C4645-BLK1
total
Water
NO PREP
11C4645-DUP1
NUC2952-01
total
Water
NO PREP
11C4645-DUP2
NUC2954-01
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4657-BLK1
11C4657-BLK1
total
Water
SM 2320B
11C4657_P
11C4657-DUP1
NUC2952-01
total
Water
SM 2320B
11C4657_P
NUC3001-01
0316201122801
total
Ground Water
SM 2320B
11C4657_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4657-BLK1
11C4657-BLK1
total
Water
NO PREP
11C4657-DUP1
NUC2952-01
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4897-BLK1
11C4897-BLK1
Dissolved
Water
SM2540 C
11C4897_P
11C4897-BS1
11C4897-BS1
Dissolved
Water
SM2540 C
11C4897_P
11C4897-DUP1
NUC3009-01
Dissolved
Water
SM2540 C
11C4897_P
NUC3001-01
0316201122801
Dissolved
Ground Water
SM2540 C
11C4897_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4897-BLK1
11C4897-BLK1
Dissolved
Water
SOLIDS
11C4897-BS1
11C4897-BS1
Dissolved
Water
SOLIDS
5 6 7
Prep Batch: 11C4583_P Prep Batch
8 9 10 11
Analysis Batch: 11C4645
Prep Batch: 11C4645_P
Analysis Batch: 11C4657
Prep Batch: 11C4657_P
Analysis Batch: 11C4897
Prep Batch: 11C4897_P
TestAmerica Nashville
Page 22 of 29
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03/24/2011
12
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
WetChem (Continued)
3
Prep Batch: 11C4897_P (Continued) Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4897-DUP1
NUC3009-01
Dissolved
Water
SOLIDS
Prep Batch
NUC3001-01
0316201122801
Dissolved
Ground Water
SOLIDS
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5102-BLK1
11C5102-BLK1
total
Water
SM2540 D
11C5102_P
11C5102-BS1
11C5102-BS1
total
Water
SM2540 D
11C5102_P
11C5102-DUP1
NUC2446-01
total
Water
SM2540 D
11C5102_P
11C5102-DUP2
0316201122801
total
Water
SM2540 D
11C5102_P
NUC3001-01
0316201122801
total
Ground Water
SM2540 D
11C5102_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5102-BLK1
11C5102-BLK1
total
Water
SOLIDS
11C5102-BS1
11C5102-BS1
total
Water
SOLIDS
11C5102-DUP1
NUC2446-01
total
Water
SOLIDS
11C5102-DUP2
0316201122801
total
Water
SOLIDS
NUC3001-01
0316201122801
total
Ground Water
SOLIDS
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5551-BLK1
11C5551-BLK1
total
Water
SM 2320B
11C5551_P
11C5551-DUP1
NUC2956-01RE1
total
Water
SM 2320B
11C5551_P
NUC3001-01 - RE1
0316201122801
total
Ground Water
SM 2320B
11C5551_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5551-BLK1
11C5551-BLK1
total
Water
NO PREP
11C5551-DUP1
NUC2956-01RE1
total
Water
NO PREP
NUC3001-01 - RE1
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5627-BLK1
11C5627-BLK1
total
Water
SM2510 B
11C5627_P
11C5627-BS1
11C5627-BS1
total
Water
SM2510 B
11C5627_P
11C5627-DUP1
NUC0332-01RE1
total
Water
SM2510 B
11C5627_P
NUC3001-01
0316201122801
total
Ground Water
SM2510 B
11C5627_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5627-BLK1
11C5627-BLK1
total
Water
NO PREP
11C5627-BS1
11C5627-BS1
total
Water
NO PREP
11C5627-DUP1
NUC0332-01RE1
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4583-BLK1
11C4583-BLK1
total
Water
EPA 300.0
11C4583_P
11C4583-BS1
11C4583-BS1
total
Water
EPA 300.0
11C4583_P
11C4583-MS1
NUC2986-01
total
Water
EPA 300.0
11C4583_P
NUC3001-01
0316201122801
total
Ground Water
EPA 300.0
11C4583_P
11C4583-DUP1
NUC3019-01
total
Water
EPA 300.0
11C4583_P
4 5
Analysis Batch: 11C5102
6 7 8 9
Prep Batch: 11C5102_P
11 12
Analysis Batch: 11C5551
Prep Batch: 11C5551_P
Analysis Batch: 11C5627
Prep Batch: 11C5627_P
Analysis Batch: U004576
TestAmerica Nashville
Page 23 of 29
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03/24/2011
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
Extractions
3
Analysis Batch: 11C5376 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5376-BLK1
11C5376-BLK1
total
Water
EPA 1664A
11C5376_P
11C5376-BS1
11C5376-BS1
total
Water
EPA 1664A
11C5376_P
11C5376-BSD1
11C5376-BSD1
total
Water
EPA 1664A
11C5376_P
11C5376-MS1
NUC1440-01
total
Water
EPA 1664A
11C5376_P
NUC3001-01
0316201122801
total
Ground Water
EPA 1664A
11C5376_P
4 5 6 7
Prep Batch: 11C5376_P Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C5376-BLK1
11C5376-BLK1
total
Water
11C5376-BS1
11C5376-BS1
total
Water
11C5376-BSD1
11C5376-BSD1
total
Water
11C5376-MS1
NUC1440-01
total
Water
NUC3001-01
0316201122801
total
Ground Water
1664 HEM/SGTHEM 1664 HEM/SGTHEM 1664 HEM/SGTHEM 1664 HEM/SGTHEM 1664 HEM/SGTHEM
Prep Batch
8 9 10 11 12
TCLP Analysis Batch: 11C4508 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4508-BS1
11C4508-BS1
total
Water
SM 4500 H B
11C4508_P
11C4508-BS2
11C4508-BS2
total
Water
SM 4500 H B
11C4508_P
11C4508-DUP1
NUC2986-01
total
Water
SM 4500 H B
11C4508_P
11C4508-DUP1
NUC2986-01
total
Water
EPA 170.1
11C4508_P
11C4508-DUP2
NUC3008-01
total
Water
SM 4500 H B
11C4508_P
11C4508-DUP2
NUC3008-01
total
Water
EPA 170.1
11C4508_P
NUC3001-01
0316201122801
total
Ground Water
SM 4500 H B
11C4508_P
NUC3001-01
0316201122801
total
Ground Water
EPA 170.1
11C4508_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4508-BS1
11C4508-BS1
total
Water
METHOD PREP
11C4508-BS2
11C4508-BS2
total
Water
METHOD PREP
11C4508-DUP1
NUC2986-01
total
Water
METHOD PREP
11C4508-DUP2
NUC3008-01
total
Water
METHOD PREP
NUC3001-01
0316201122801
total
Ground Water
METHOD PREP
Prep Batch: 11C4508_P
TestAmerica Nashville
Page 24 of 29
03/24/2011
Lab Chronicle Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Client Sample ID: 0316201122801
Lab Sample ID: NUC3001-01
Date Collected: 03/16/11 10:50 Date Received: 03/18/11 08:30
Matrix: Ground Water
Dilution
Batch
Batch
Prepared
Prep Type
Type
Method
Factor
Number
Analyst
Lab
total
Prep
EPA 5030B
1.00
11C5504_P
03/21/11 10:05
TSP
TestAmerica Nashville
total
Analysis
SW846 8260B
1.00
U004725
03/22/11 16:18
FE
TestAmerica Nashville
Dissolved
Prep
RSK 175/3810
1.00
11C4872_P
03/21/11 09:00
WAM
TestAmerica Nashville
Dissolved
Analysis
RSK 175
1.00
U004542
03/21/11 10:49
ljt
TestAmerica Nashville
Dissolved
Prep
RSK 175/3810
RE1
1.00
11C4872_P
03/21/11 09:00
WAM
TestAmerica Nashville
Dissolved
Analysis
RSK 175
RE1
5.00
U004542
03/21/11 10:53
ljt
TestAmerica Nashville
total
Prep
1.00
11C4553_P
03/19/11 09:13
MET
TestAmerica Nashville
total
Analysis
EPA 3010A / 6010 SW846 6010C
1.00
11C4553
03/21/11 12:57
LTB
TestAmerica Nashville
total
Prep
EPA 7470
1.00
11C4512_P
03/21/11 10:25
DEB
TestAmerica Nashville
total
Analysis
SW846 7470A
1.00
11C4512
03/21/11 13:53
DEB
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C4645_P
03/18/11 16:29
JAG2
TestAmerica Nashville
total
Analysis
SM 2320B
1.00
11C4645
03/19/11 02:02
JAG2
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C4657_P
03/18/11 16:39
JAG2
TestAmerica Nashville
total
Analysis
SM 2320B
1.00
11C4657
03/19/11 02:02
JAG2
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C4583_P
03/18/11 14:32
amc
TestAmerica Nashville
total
Analysis
EPA 300.0
5.00
U004576
03/19/11 16:17
amc
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C5627_P
03/23/11 10:12
TEM
TestAmerica Nashville
total
Analysis
SM2510 B
1.00
11C5627
03/23/11 13:13
TEM
TestAmerica Nashville
total
Analysis
SM5540 C
1.00
11C4511
03/18/11 13:05
JJR
TestAmerica Nashville
total
Prep
SM5540C
1.00
11C4511_P
03/18/11 13:05
AMJ
TestAmerica Nashville
Dissolved
Analysis
SM2540 C
1.00
11C4897
03/19/11 23:30
cob
TestAmerica Nashville
Dissolved
Prep
SOLIDS
1.00
11C4897_P
03/19/11 23:30
cob
TestAmerica Nashville
total
Analysis
SM2540 D
1.43
11C5102
03/21/11 19:04
bmc
TestAmerica Nashville
total
Prep
SOLIDS
1.43
11C5102_P
03/21/11 19:04
bmc
TestAmerica Nashville
total
Analysis
EPA 180.1
1.00
11C4582
03/18/11 14:31
KJA
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C4582_P
03/18/11 14:31
KJA
TestAmerica Nashville
total
Prep
NO PREP
RE1
1.00
11C5551_P
03/22/11 22:24
JAG2
TestAmerica Nashville
total
Analysis
SM 2320B
RE1
1.00
11C5551
03/23/11 03:28
JAG2
TestAmerica Nashville
total
Prep
1.00
11C5376_P
03/23/11 10:00
BJM
TestAmerica Nashville
total
Analysis
1664 HEM/SGTHEM EPA 1664A
1.00
11C5376
03/23/11 16:28
MSR
TestAmerica Nashville
total
Analysis
SM 4500 H B
1.00
11C4508
03/18/11 15:30
SJM
TestAmerica Nashville
total
Prep
METHOD PREP
1.00
11C4508_P
03/18/11 15:30
SJM
TestAmerica Nashville
total
Analysis
EPA 170.1
1.00
11C4508
03/18/11 15:30
SJM
TestAmerica Nashville
Or Analyzed
Client Sample ID: Trip Blank
5 6 7 8 9 10 11 12
Lab Sample ID: NUC3001-02
Date Collected: 03/16/11 00:01 Date Received: 03/18/11 08:30
Matrix: Water
Batch
Batch
Prep Type
Type
Method
Dilution
Batch
Factor
Number
total
Prep
Analyst
Lab
EPA 5030B
1.00
11C5504_P
03/21/11 10:05
TSP
total
Analysis
TestAmerica Nashville
SW846 8260B
1.00
U004725
03/22/11 16:49
FE
TestAmerica Nashville
Run
Prepared Or Analyzed
TestAmerica Nashville
Page 25 of 29
3 4
Batch
Run
1
03/24/2011
Method Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
Method
Method Description
EPA 1664A
General Chemistry Parameters
Protocol
Laboratory
TAL NSH
EPA 170.1
General Chemistry Parameters
TAL NSH
SM 4500 H B
General Chemistry Parameters
TAL NSH
SW846 8260B
Volatile Organic Compounds by EPA Method 8260B
TAL NSH
RSK 175
Methane, Ethane, and Ethene by GC
TAL NSH
SW846 6010C
Total Metals by EPA 6010C
TAL NSH
SW846 7470A
Mercury by EPA Methods 7470A/7471A
TAL NSH
EPA 180.1
General Chemistry Parameters
TAL NSH
EPA 300.0
General Chemistry Parameters
TAL NSH
SM 2320B
General Chemistry Parameters
TAL NSH
SM2510 B
General Chemistry Parameters
TAL NSH
SM2540 C
General Chemistry Parameters
TAL NSH
SM2540 D
General Chemistry Parameters
TAL NSH
SM5540 C
General Chemistry Parameters
TAL NSH
3 4 5 6 7 8 9 10
Protocol References:
11 12
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Road, Nashville, TN 37204, TEL 800-765-0980
TestAmerica Nashville
Page 26 of 29
03/24/2011
Certification Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
Laboratory
Authority
TestAmerica Nashville
TestAmerica Job ID: NUC3001
2
Program
EPA Region
AIHA
TestAmerica Nashville
1
USDA
Certification ID
* Expiration Date
100790
09/01/11
S-48469
11/02/13
TestAmerica Nashville
A2LA
A2LA
0
0453.07
12/31/11
TestAmerica Nashville
A2LA
WY UST
0
453.07
12/31/11
TestAmerica Nashville
Alabama
State Program
4
41150
03/19/11
TestAmerica Nashville
Alaska
Alaska UST
10
UST-087
07/24/11
TestAmerica Nashville
Arizona
State Program
9
AZ0473
05/05/11
TestAmerica Nashville
Arkansas
State Program
6
88-0737
04/25/11
TestAmerica Nashville
CALA
CALA
0
3744
03/08/14
TestAmerica Nashville
California
NELAC
9
1168CA
10/31/11
TestAmerica Nashville
Colorado
State Program
8
N/A
02/28/12
TestAmerica Nashville
Connecticut
State Program
1
PH-0220
12/31/11
TestAmerica Nashville
Florida
NELAC
4
E87358
06/30/11
TestAmerica Nashville
Illinois
NELAC
5
200010
12/09/11
TestAmerica Nashville
Iowa
State Program
7
131
05/01/12
TestAmerica Nashville
Kansas
NELAC
7
E-10229
10/31/11
TestAmerica Nashville
Kentucky
Kentucky UST
4
19
07/13/12
TestAmerica Nashville
Kentucky
State Program
4
90038
12/31/11
TestAmerica Nashville
Louisiana
NELAC
6
LA100011
12/31/11
TestAmerica Nashville
Louisiana
NELAC
6
30613
06/30/11
TestAmerica Nashville
Maryland
State Program
3
316
03/31/11
TestAmerica Nashville
Massachusetts
State Program
1
M-TN032
06/30/11
TestAmerica Nashville
Minnesota
NELAC
5
047-999-345
12/31/11
TestAmerica Nashville
Mississippi
State Program
4
N/A
06/30/11
TestAmerica Nashville
Montana
MT DEQ UST
8
NA
01/01/15
TestAmerica Nashville
Nevada
State Program
9
TN00032
07/31/11
TestAmerica Nashville
New Hampshire
NELAC
1
2963
10/09/11
TestAmerica Nashville
New Jersey
NELAC
2
TN965
06/30/11
TestAmerica Nashville
New York
NELAC
2
11342
04/01/11
TestAmerica Nashville
North Carolina
North Carolina DENR
4
387
12/31/11
TestAmerica Nashville
North Dakota
State Program
8
R-146
06/30/11
TestAmerica Nashville
Ohio
OVAP
5
CL0033
04/01/12
TestAmerica Nashville
Oklahoma
State Program
6
9412
08/31/11
TestAmerica Nashville
Oregon
NELAC
10
TN200001
04/30/11
TestAmerica Nashville
Pennsylvania
NELAC
3
68-00585
06/30/11
TestAmerica Nashville
Rhode Island
State Program
1
LAO00268
12/30/11
TestAmerica Nashville
South Carolina
State Program
4
84009
03/19/11
TestAmerica Nashville
South Carolina
State Program
4
84009
04/30/11
TestAmerica Nashville
Tennessee
State Program
4
2008
03/19/11
TestAmerica Nashville
Texas
NELAC
6
T104704077-09-TX
08/31/11
TestAmerica Nashville
Utah
NELAC
8
TAN
06/30/11
TestAmerica Nashville
Virginia
State Program
3
00323
06/30/11
TestAmerica Nashville
Washington
State Program
10
C789
07/19/11
TestAmerica Nashville
West Virginia
West Virginia DEP
3
219
04/30/11
TestAmerica Nashville
Wisconsin
State Program
5
998020430
08/31/11
Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s current list of certified methods and analytes. * Any expired certifications in this list are currently pending renewal and are considered valid.
TestAmerica Nashville
Page 27 of 29
03/24/2011
3 4 5 6 7 8 9 10 11 12
1 2 3 4 5 6 7 8 9 10 11 12
Page 28 of 29
03/24/2011
1 2 3 4 5 6 7 8 9 10 11 12
Page 29 of 29
03/24/2011
ANALYTICAL REPORT
6
TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Road Nashville, TN 37204 Tel: 800-765-0980
7 8 9
TestAmerica Job ID: NUC3001 Client Project/Site: Property ID# 908055 Client Project Description: EHS Special Project (PA) - Champdale - 908055
10 11
For: SAIC Energy, Environment & Infrastructure, LLC/CHK 3700 West Robinson, Suite 200 Norman, OK 73072 Attn: Aria Archie
Authorized for release by: 03/24/2011 12:38:16 PM Gail A Lage Program Manager - National Accounts [email protected] Designee for John Smeathers Project Manager [email protected]
Results relate only to the items tested and the sample(s) as received by the laboratory. The test results in this report meet all 2003 NELAC requirements for accredited parameters, exceptions are noted in this report. Pursuant to NELAC, this report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Page 1 of 29
03/24/2011
12
Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Table of Contents Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
1 3
1 2 3 4 5 6 9 20 25 26 27
4 5 6 7 8 9 10 11
28
12
TestAmerica Nashville
Page 2 of 29
03/24/2011
Sample Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
NUC3001-01
0316201122801
Ground Water
03/16/11 10:50
03/18/11 08:30
NUC3001-02
Trip Blank
Water
03/16/11 00:01
03/18/11 08:30
3 4 5 6 7 8 9 10 11 12
TestAmerica Nashville
Page 3 of 29
03/24/2011
Case Narrative Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
Job ID: NUC3001
3
Laboratory: TestAmerica Nashville
4
Narrative
The samples were received in good order and condition in the following cooler(s). Any exception would be noted on the Cooler Receipt Form and/or explained in further detail in the below narrative.
5 6
Cooler ID # & Temperature 6773 0.5 C
7 8
The samples were received the second day after collection potentially providing insufficient holding time for the MBAS and Turbidity analyses. The client requests we proceed as received. The lab expedited these samples as much as possible to secure the holding time. If the holding time was not met, the analysis was flagged with an "HT3" qualifier in the report. No further action was taken.
9 10 11 12
TestAmerica Nashville
Page 4 of 29
03/24/2011
Qualifier Definition/Glossary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Qualifiers
3
Metals
4
Qualifier
Qualifier Description
M7
The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).
M8
The MS and/or MSD were below the acceptance limits. See Blank Spike (LCS).
MHA
Due to high levels of analyte in the sample, the MS/MSD calculation does not provide useful spike recovery information. See Blank Spike (LCS). No results were reported for the MS/MSD. The sample used for the MS/MSD required dilution due to the sample matrix. Because of this, the spike compounds were diluted below the detection limit.
MNR
5 6 7
WetChem Qualifier
Qualifier Description
HT3
Sample received with insufficient holding time remaining for analysis to be performed within the method's holding time requirements.
MHA
Due to high levels of analyte in the sample, the MS/MSD calculation does not provide useful spike recovery information. See Blank Spike (LCS). Due to the low levels of analyte in the sample, the duplicate RPD calculation does not provide useful information.
R4
1
8 9
TCLP
10
Qualifier
Qualifier Description
HTI
The holding time for this test is immediate. The laboratory measurement, therefore, may not be suitable for compliance purposes.
11
Glossary
12
Abbreviation
These commonly used abbreviations may or may not be present in this report.
¤
Listed under the "D" column to designate that the result is reported on a dry weight basis.
EPA
United States Environmental Protection Agency
ND
Not Detected above the reporting level.
MDL
Method Detection Limit
RL
Reporting Limit
RE, RE1 (etc.)
Indicates a Re-extraction or Reanalysis of the sample.
%R
Percent Recovery
RPD
Relative Percent Difference, a measure of the relative difference between two points.
TestAmerica Nashville
Page 5 of 29
03/24/2011
Analytical Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Client Sample ID: 0316201122801
Lab Sample ID: NUC3001-01
Date Collected: 03/16/11 10:50 Date Received: 03/18/11 08:30 Sampler Name: Mike Melito 228
Matrix: Ground Water
3
Sampler Phone Number: (405) 321-3895
4
Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B Analyte
1
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
5
Benzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:18
1.00
Ethylbenzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:18
1.00
1.99
0.500
ug/L
03/21/11 10:05
03/22/11 16:18
1.00
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:18
1.00
7
Dil Fac
8
Toluene Xylenes, total Surrogate
Limits
Prepared
Analyzed
1,2-Dichloroethane-d4
105
63 - 140
03/21/11 10:05
03/22/11 16:18
1.00
Dibromofluoromethane
108
73 - 131
03/21/11 10:05
03/22/11 16:18
1.00
Toluene-d8
118
80 - 120
03/21/11 10:05
03/22/11 16:18
1.00
91
79 - 125
03/21/11 10:05
03/22/11 16:18
1.00
Prepared
Analyzed
4-Bromofluorobenzene
% Recovery Qualifier
Method: RSK 175 - Methane, Ethane, and Ethene by GC - dissolved Analyte
RL
Result Qualifier
MDL Unit
D
Dil Fac
Ethane
ND
0.0260
mg/L
03/21/11 09:00
03/21/11 10:49
1.00
Propane
ND
0.0340
mg/L
03/21/11 09:00
03/21/11 10:49
1.00
Surrogate
Acetylene
% Recovery Qualifier
101
Limits
Prepared
Analyzed
70 - 122
03/21/11 09:00
03/21/11 10:49
Dil Fac
1.00
Method: RSK 175 - Methane, Ethane, and Ethene by GC - dissolved - RE1 Analyte
Methane
RL
Result Qualifier
0.130
2.03
MDL Unit
D
mg/L
Prepared
Analyzed
03/21/11 09:00
03/21/11 10:53
Dil Fac
5.00
Method: SW846 6010C - Total Metals by EPA 6010C Analyte
Arsenic
RL
Result Qualifier
MDL Unit
Prepared
Analyzed
ND
0.0100
mg/L
D
03/19/11 09:13
03/21/11 12:57
Dil Fac
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
0.659
0.0100
Cadmium
ND
0.00100
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Calcium
58.0
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Iron
0.624
0.0500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Lead
0.0375
0.00500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Magnesium
11.7
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Manganese
0.582
0.0150
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Potassium
2.51
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Selenium
ND
0.0100
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Silver
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Sodium
18.6
1.00
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Sulfur
7.41
0.500
mg/L
03/19/11 09:13
03/21/11 12:57
1.00
Barium
Chromium
Method: SW846 7470A - Mercury by EPA Methods 7470A/7471A Analyte
Mercury
Result Qualifier
ND
RL
0.000200
MDL Unit
D
mg/L
Prepared
Analyzed
03/21/11 10:25
03/21/11 13:53
Dil Fac
1.00
Method: EPA 180.1 - General Chemistry Parameters Analyte
Result Qualifier
Turbidity
ND HT3
RL
MDL Unit
1.00
NTU
RL
MDL Unit
D
Prepared
Analyzed
03/18/11 14:31
03/18/11 14:31
Dil Fac
1.00
Method: EPA 300.0 - General Chemistry Parameters Analyte
Chloride
Result Qualifier
21.7
5.00
mg/L
D
Prepared
Analyzed
03/18/11 14:32
03/19/11 16:17
Dil Fac
5.00
TestAmerica Nashville
Page 6 of 29
03/24/2011
6
9 10 11 12
Analytical Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Client Sample ID: 0316201122801
Lab Sample ID: NUC3001-01
Date Collected: 03/16/11 10:50 Date Received: 03/18/11 08:30 Sampler Name: Mike Melito 228
Matrix: Ground Water
3
Sampler Phone Number: (405) 321-3895
4
Method: EPA 300.0 - General Chemistry Parameters (Continued) Analyte
Sulfate
RL
Result Qualifier
5.00
18.7
MDL Unit
D
mg/L
Prepared
Analyzed
03/18/11 14:32
03/19/11 16:17
Prepared
Analyzed
Dil Fac
5.00
Method: SM 2320B - General Chemistry Parameters Analyte
RL
Result Qualifier
MDL Unit
D
Dil Fac
Bicarbonate Alkalinity as CaCO3
192
10.0
mg/L
03/18/11 16:29
03/19/11 02:02
1.00
Carbonate as CaCO3
ND
10.0
mg/L
03/18/11 16:39
03/19/11 02:02
1.00
Prepared
Analyzed
03/22/11 22:24
03/23/11 03:28
Prepared
Analyzed
03/23/11 10:12
03/23/11 13:13
Method: SM 2320B - General Chemistry Parameters - RE1 Analyte
Bicarbonate Alkalinity as CaCO3
RL
Result Qualifier
10.0
181
MDL Unit
D
mg/L
Dil Fac
1.00
Method: SM2510 B - General Chemistry Parameters Analyte
Specific conductance
RL
Result Qualifier
10.0
516
MDL Unit
D
umho/cm
Dil Fac
1.00
Method: SM2540 C - General Chemistry Parameters - dissolved Analyte
Total Dissolved Solids
Result Qualifier
248
RL
10.0
MDL Unit
D
mg/L
Prepared
Analyzed
03/19/11 23:30
03/19/11 23:30
Dil Fac
1.00
Method: SM2540 D - General Chemistry Parameters Analyte
Total Suspended Solids
Result Qualifier
3.43
RL
1.43
MDL Unit
D
mg/L
Prepared
Analyzed
03/21/11 19:04
03/21/11 19:04
Dil Fac
1.43
Method: SM5540 C - General Chemistry Parameters Analyte
MBAS (mol.wt 320)
Result Qualifier
ND HT3
RL
0.0500
MDL Unit
D
mg/L
Prepared
Analyzed
03/18/11 13:05
03/18/11 13:05
Dil Fac
1.00
Method: EPA 1664A - General Chemistry Parameters Analyte
Oil & Grease HEM
Result Qualifier
ND
RL
5.75
MDL Unit
D
mg/L
Prepared
Analyzed
03/23/11 10:00
03/23/11 16:28
Dil Fac
1.00
Method: EPA 170.1 - General Chemistry Parameters Analyte
Temperature of pH determination
Result Qualifier
23.4 HTI
RL
0.00
MDL Unit
D
Deg C
Prepared
Analyzed
03/18/11 15:30
03/18/11 15:30
Dil Fac
1.00
Method: SM 4500 H B - General Chemistry Parameters Analyte
pH
Result Qualifier
7.60 HTI
1
RL
0.100
MDL Unit
pH Units
D
Prepared
Analyzed
03/18/11 15:30
03/18/11 15:30
Dil Fac
1.00
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Analytical Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Client Sample ID: Trip Blank
Lab Sample ID: NUC3001-02
Date Collected: 03/16/11 00:01 Date Received: 03/18/11 08:30 Sampler Name:
Matrix: Water
3
Sampler Phone Number: (405) 321-3895
4
Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B Analyte
1
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
5
Benzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:49
1.00
Ethylbenzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:49
1.00
Toluene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:49
1.00
Xylenes, total
ND
0.500
ug/L
03/21/11 10:05
03/22/11 16:49
1.00
7
Dil Fac
8
Surrogate
% Recovery Qualifier
Limits
Prepared
Analyzed
1,2-Dichloroethane-d4
99
63 - 140
03/21/11 10:05
03/22/11 16:49
1.00
Dibromofluoromethane
103
73 - 131
03/21/11 10:05
03/22/11 16:49
1.00
Toluene-d8
118
80 - 120
03/21/11 10:05
03/22/11 16:49
1.00
89
79 - 125
03/21/11 10:05
03/22/11 16:49
1.00
4-Bromofluorobenzene
6
9 10 11 12
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Page 8 of 29
03/24/2011
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B
3
Lab Sample ID: 11C5504-BLK1 Matrix: Water Analysis Batch: U004725
Client Sample ID: 11C5504-BLK1 Prep Type: total Prep Batch: 11C5504_P Blank Blank
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
Benzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 13:14
1.00
Ethylbenzene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 13:14
1.00
Toluene
ND
0.500
ug/L
03/21/11 10:05
03/22/11 13:14
1.00
Xylenes, total
ND
0.500
ug/L
03/21/11 10:05
03/22/11 13:14
1.00
Limits
Prepared
Analyzed
Blank Blank Surrogate
% Recovery Qualifier
Dil Fac
1,2-Dichloroethane-d4
100
63 - 140
03/21/11 10:05
03/22/11 13:14
1.00
Dibromofluoromethane
104
73 - 131
03/21/11 10:05
03/22/11 13:14
1.00
Toluene-d8
111
80 - 120
03/21/11 10:05
03/22/11 13:14
1.00
90
79 - 125
03/21/11 10:05
03/22/11 13:14
1.00
4-Bromofluorobenzene
Lab Sample ID: 11C5504-BS1 Matrix: Water Analysis Batch: U004725
Client Sample ID: 11C5504-BS1 Prep Type: total Prep Batch: 11C5504_P Spike
Analyte
Added
LCS LCS Result Qualifier
% Rec. Unit
D
% Rec
Limits
Benzene
50.0
49.2
ug/L
98
80 - 121
Ethylbenzene
50.0
50.9
ug/L
102
78 - 133
Toluene
50.0
56.5
ug/L
113
78 - 125
Xylenes, total
150
153
ug/L
102
78 - 134
LCS LCS % Recovery Qualifier
Limits
1,2-Dichloroethane-d4
97
63 - 140
Dibromofluoromethane
107
73 - 131
Toluene-d8
109
80 - 120
86
79 - 125
Surrogate
4-Bromofluorobenzene
Lab Sample ID: 11C5504-BSD1 Matrix: Water Analysis Batch: U004725
Client Sample ID: 11C5504-BSD1 Prep Type: total Prep Batch: 11C5504_P
Analyte
Spike
LCS Dup LCS Dup
Added
Result Qualifier
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
Benzene
50.0
47.1
ug/L
94
80 - 121
4
12
Ethylbenzene
50.0
50.4
ug/L
101
78 - 133
1
12
Toluene
50.0
56.2
ug/L
112
78 - 125
0.5
35
Xylenes, total
150
152
ug/L
102
78 - 134
0.6
18
LCS Dup LCS Dup % Recovery Qualifier
Limits
1,2-Dichloroethane-d4
93
63 - 140
Dibromofluoromethane
107
73 - 131
Toluene-d8
115
80 - 120
88
79 - 125
Surrogate
4-Bromofluorobenzene
1
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Page 9 of 29
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Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: RSK 175 - Methane, Ethane, and Ethene by GC
3
Lab Sample ID: 11C4872-BLK1 Matrix: Water Analysis Batch: U004542
Client Sample ID: 11C4872-BLK1 Prep Type: dissolved Prep Batch: 11C4872_P Blank Blank
Analyte
RL
Result Qualifier
MDL Unit
D
Prepared
Analyzed
Dil Fac
Methane
ND
0.0260
mg/L
03/21/11 09:00
03/21/11 09:15
1.00
Ethene
ND
0.0260
mg/L
03/21/11 09:00
03/21/11 09:15
1.00
Ethane
ND
0.0260
mg/L
03/21/11 09:00
03/21/11 09:15
1.00
Propane
ND
0.0340
mg/L
03/21/11 09:00
03/21/11 09:15
1.00
Limits
Prepared
Analyzed
70 - 122
03/21/11 09:00
03/21/11 09:15
Blank Blank Surrogate
% Recovery Qualifier
Acetylene
106
Lab Sample ID: 11C4872-BS1 Matrix: Water Analysis Batch: U004542
Dil Fac
1.00
Client Sample ID: 11C4872-BS1 Prep Type: dissolved Prep Batch: 11C4872_P Spike
LCS LCS
% Rec.
Analyte
Added
Methane
0.273
0.295
mg/L
108
80 - 120
Ethene
0.479
0.465
mg/L
97
80 - 120
Ethane
0.512
0.569
mg/L
111
80 - 120
Propane
0.754
0.824
mg/L
109
80 - 120
Result Qualifier
Unit
D
% Rec
Limits
% Recovery Qualifier
Limits
Acetylene
99
70 - 122
Lab Sample ID: 11C4872-BSD1 Matrix: Water Analysis Batch: U004542
Client Sample ID: 11C4872-BSD1 Prep Type: dissolved Prep Batch: 11C4872_P Spike
LCS Dup LCS Dup
Analyte
Added
Result Qualifier
Methane
0.273
0.293
mg/L
107
Ethene
0.479
0.458
mg/L
96
Ethane
0.512
0.566
mg/L
Propane
0.754
0.821
mg/L
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
80 - 120
0.7
33
80 - 120
1
29
110
80 - 120
0.6
30
109
80 - 120
0.4
33
LCS Dup LCS Dup Surrogate
% Recovery Qualifier
Limits
Acetylene
88
70 - 122
Lab Sample ID: 11C4872-MS1 Matrix: Water Analysis Batch: U004542
Client Sample ID: NUC2978-01 Prep Type: dissolved Prep Batch: 11C4872_P Spike
Matrix Spike Matrix Spike
% Rec.
Analyte
Result Qualifier
Methane
0.0252
0.273
0.308
mg/L
Ethene
ND
0.479
0.441
Ethane
ND
0.512
0.542
Propane
ND
0.754
0.786
Added
Result Qualifier
Unit
D
% Rec
Limits
103
46 - 142
mg/L
92
71 - 120
mg/L
106
71 - 120
mg/L
104
46 - 142
Matrix Spike Matrix Spike Surrogate
% Recovery Qualifier
Limits
Acetylene
87
70 - 122
TestAmerica Nashville
Page 10 of 29
4 5 6 7 8 9 10 11 12
LCS LCS Surrogate
Sample Sample
1
03/24/2011
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: RSK 175 - Methane, Ethane, and Ethene by GC (Continued)
3
Lab Sample ID: 11C4872-MSD1 Matrix: Water Analysis Batch: U004542
Client Sample ID: NUC2978-01 Prep Type: dissolved Prep Batch: 11C4872_P Spike Matrix Spike Dup Matrix Spike Dup
Sample Sample Analyte
Result Qualifier
Methane
Added
Result Qualifier
% Rec.
Unit
D
% Rec
RPD
Limits
RPD
Limit
0.0252
0.273
0.304
mg/L
102
46 - 142
1
33
Ethene
ND
0.479
0.431
mg/L
90
71 - 120
2
29
Ethane
ND
0.512
0.534
mg/L
104
71 - 120
2
30
Propane
ND
0.754
0.775
mg/L
103
46 - 142
1
33
% Recovery Qualifier
Limits
Acetylene
78
70 - 122
Client Sample ID: 11C4553-BLK1 Prep Type: total Prep Batch: 11C4553_P Blank Blank RL
Result Qualifier
MDL Unit
Prepared
Analyzed
Arsenic
ND
0.0100
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Barium
ND
0.0100
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Cadmium
ND
0.00100
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Calcium
ND
1.00
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Chromium
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Iron
ND
0.0500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Lead
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Magnesium
ND
1.00
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Manganese
ND
0.0150
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Potassium
ND
1.00
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Selenium
ND
0.0100
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Silver
ND
0.00500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Sodium
ND
1.00
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
Sulfur
ND
0.500
mg/L
03/19/11 09:13
03/21/11 11:32
1.00
D
Lab Sample ID: 11C4553-BS1 Matrix: Water Analysis Batch: 11C4553 Spike
LCS LCS
% Rec.
Added
Result Qualifier
Unit
Arsenic
0.0500
0.0514
mg/L
103
80 - 120
D
% Rec
Limits
2.00
2.02
mg/L
101
80 - 120
0.0500
0.0484
mg/L
97
80 - 120
5.00
4.69
mg/L
94
80 - 120
0.200
0.189
mg/L
95
80 - 120
1.00
0.951
mg/L
95
80 - 120
0.0500
0.0505
mg/L
101
80 - 120
Magnesium
5.00
4.62
mg/L
92
80 - 120
Manganese
0.500
0.479
mg/L
96
80 - 120
Potassium
5.00
4.51
mg/L
90
80 - 120
Selenium
0.0500
0.0498
mg/L
100
80 - 120
Silver
0.0500
0.0496
mg/L
99
80 - 120
Chromium Iron Lead
Dil Fac
Client Sample ID: 11C4553-BS1 Prep Type: total Prep Batch: 11C4553_P
Analyte
Calcium
6 7
10
Lab Sample ID: 11C4553-BLK1 Matrix: Water Analysis Batch: 11C4553
Cadmium
5
9
Method: SW846 6010C - Total Metals by EPA 6010C
Barium
4
8
Matrix Spike Dup Matrix Spike Dup Surrogate
Analyte
1
Sodium
5.00
4.82 MNR
mg/L
96
80 - 120
Sulfur
1.00
1.03
mg/L
103
80 - 120
TestAmerica Nashville
Page 11 of 29
03/24/2011
11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SW846 6010C - Total Metals by EPA 6010C (Continued)
3
Lab Sample ID: 11C4553-BSD1 Matrix: Water Analysis Batch: 11C4553
Client Sample ID: 11C4553-BSD1 Prep Type: total Prep Batch: 11C4553_P Spike
LCS Dup LCS Dup
Analyte
Added
Result Qualifier
Unit
Arsenic
0.0500
0.0519
mg/L
104
Barium
2.00
2.09
mg/L
104
0.0500
0.0493
mg/L
5.00
4.89
mg/L
0.200
0.193
1.00
0.975
Cadmium Calcium Chromium Iron Lead
% Rec. D
% Rec
Limits
RPD RPD
Limit
80 - 120
1
20
80 - 120
3
20
99
80 - 120
2
20
98
80 - 120
4
20
mg/L
96
80 - 120
2
20
mg/L
98
80 - 120
3
20
0.0500
0.0525
mg/L
105
80 - 120
4
20
Magnesium
5.00
4.73
mg/L
95
80 - 120
2
20
Manganese
0.500
0.492
mg/L
98
80 - 120
3
20
Potassium
5.00
4.67
mg/L
93
80 - 120
4
20
Selenium
0.0500
0.0533
mg/L
107
80 - 120
7
20
Silver
0.0500
0.0494
mg/L
99
80 - 120
0.4
20
Sodium
5.00
4.97
mg/L
99
80 - 120
3
20
Sulfur
1.00
1.04
mg/L
104
80 - 120
0.6
20
Lab Sample ID: 11C4553-MS1 Matrix: Water Analysis Batch: 11C4553
Client Sample ID: NUC2783-02 Prep Type: total Prep Batch: 11C4553_P Sample Sample
Analyte
Arsenic Barium
Result Qualifier
0.274
Spike Added
0.0500
Matrix Spike Matrix Spike Result Qualifier
% Rec. Unit
D
% Rec
Limits
0.270 MHA
mg/L
-8
75 - 125
11.3 MHA
mg/L
-142
75 - 125
mg/L
65
75 - 125
2480 MHA
mg/L
75 - 125
0.233 M8
mg/L
-3910 0 55
mg/L
-3450
75 - 125
mg/L
307
75 - 125
14.1
2.00
0.00600
0.0500
Calcium
4440
5.00
Chromium
0.123
0.200
172
1.00
0.171
0.0500
Magnesium
525
5.00
398 MHA
mg/L
-2550
75 - 125
Manganese
4.53
0.500
3.55 MHA
mg/L
-196
75 - 125
Potassium
184
5.00
173 MHA
mg/L
-214
75 - 125
Selenium
ND
0.0500
0.0544
mg/L
109
75 - 125
Silver
ND
0.0500
0.0510
mg/L
102
75 - 125
Sulfur
156
1.00
mg/L
-2140
75 - 125
Cadmium
Iron Lead
0.0386 M8
138 MHA 0.324 M7
134 MHA
Lab Sample ID: 11C4553-MSD1 Matrix: Water Analysis Batch: 11C4553
75 - 125
Client Sample ID: NUC2783-02 Prep Type: total Prep Batch: 11C4553_P Sample Sample
Analyte
Result Qualifier
Spike Matrix Spike Dup Matrix Spike Dup Added
Result Qualifier
Unit
% Rec. D
% Rec
Limits
RPD RPD
Limit
Arsenic
0.274
0.0500
0.286 MHA
mg/L
24
75 - 125
6
20
Barium
14.1
2.00
11.5 MHA
mg/L
-132
75 - 125
2
20
0.00600
0.0500
mg/L
66
75 - 125
0.8
20
Calcium
4440
5.00
2520 MHA
mg/L
75 - 125
1
20
Chromium
0.123
0.200
0.236 M8
mg/L
-3840 0 56
75 - 125
1
20
172
1.00
mg/L
-3280
75 - 125
1
20
0.171
0.0500
mg/L
333
75 - 125
4
20
Magnesium
525
5.00
406 MHA
mg/L
-2390
75 - 125
2
20
Manganese
4.53
0.500
3.61 MHA
mg/L
-184
75 - 125
2
20
Potassium
184
5.00
176 MHA
mg/L
-150
75 - 125
2
20
Cadmium
Iron Lead
1
0.0389 M8
139 MHA 0.338 M7
TestAmerica Nashville
Page 12 of 29
03/24/2011
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Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SW846 6010C - Total Metals by EPA 6010C (Continued) Lab Sample ID: 11C4553-MSD1 Matrix: Water Analysis Batch: 11C4553
Client Sample ID: NUC2783-02 Prep Type: total Prep Batch: 11C4553_P Sample Sample
Analyte
Result Qualifier
Spike Matrix Spike Dup Matrix Spike Dup Added
Result Qualifier
Unit
% Rec. D
% Rec
RPD
Limits
RPD
Limit
Selenium
ND
0.0500
0.0525
mg/L
105
75 - 125
4
20
Silver
ND
0.0500
0.0522
mg/L
104
75 - 125
2
20
Sulfur
156
1.00
mg/L
-1960
75 - 125
1
20
136 MHA
Method: SW846 7470A - Mercury by EPA Methods 7470A/7471A Client Sample ID: 11C4512-BLK1 Prep Type: total Prep Batch: 11C4512_P Blank Blank RL
Result Qualifier
Mercury
ND
MDL Unit
0.000200
D
mg/L
Prepared
Analyzed
03/21/11 10:25
03/21/11 13:01
Lab Sample ID: 11C4512-BS1 Matrix: Water Analysis Batch: 11C4512 LCS LCS
Spike Added
Mercury
0.00100
Result Qualifier
0.000916
D
mg/L
Spike
LCS Dup LCS Dup
Added
Result Qualifier
Mercury
0.00100
92
0.000908
D
mg/L
% Rec
91
RPD
Limits
80 - 120
RPD
Limit
0.9
20
Client Sample ID: NUC2982-01 Prep Type: total Prep Batch: 11C4512_P Sample Sample Result Qualifier
ND
Spike
Matrix Spike Matrix Spike
Added
Result Qualifier
0.00100
0.000975
% Rec. Unit
D
mg/L
% Rec
97
Lab Sample ID: 11C4512-MSD1 Matrix: Water Analysis Batch: 11C4512
Limits
75 - 125
Client Sample ID: NUC2982-01 Prep Type: total Prep Batch: 11C4512_P Sample Sample
Mercury
Limits
80 - 120
% Rec. Unit
Lab Sample ID: 11C4512-MS1 Matrix: Water Analysis Batch: 11C4512
Analyte
% Rec
Client Sample ID: 11C4512-BSD1 Prep Type: total Prep Batch: 11C4512_P
Analyte
Mercury
1.00
% Rec. Unit
Lab Sample ID: 11C4512-BSD1 Matrix: Water Analysis Batch: 11C4512
Analyte
Dil Fac
Client Sample ID: 11C4512-BS1 Prep Type: total Prep Batch: 11C4512_P
Analyte
Result Qualifier
ND
Spike Matrix Spike Dup Matrix Spike Dup Added
Result Qualifier
0.00100
0.000943
% Rec.
Unit
D
mg/L
% Rec
94
RPD
Limits
RPD
Limit
3
20
75 - 125
Method: EPA 180.1 - General Chemistry Parameters Lab Sample ID: 11C4582-BLK1 Matrix: Water Analysis Batch: 11C4582
Client Sample ID: 11C4582-BLK1 Prep Type: total Prep Batch: 11C4582_P Blank Blank
Analyte
Turbidity
Result Qualifier
ND
3 4 5 6 7 8
Lab Sample ID: 11C4512-BLK1 Matrix: Water Analysis Batch: 11C4512 Analyte
1
RL
MDL Unit
1.00
NTU
D
Prepared
Analyzed
03/18/11 14:31
03/18/11 14:31
Dil Fac
1.00
TestAmerica Nashville
Page 13 of 29
03/24/2011
9 10 11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: EPA 180.1 - General Chemistry Parameters (Continued)
3
Lab Sample ID: 11C4582-BS1 Matrix: Water Analysis Batch: 11C4582
Client Sample ID: 11C4582-BS1 Prep Type: total Prep Batch: 11C4582_P LCS LCS
Spike Analyte
Added
Turbidity
Result Qualifier
5.00
5.00
D
NTU
100
Spike
LCS Dup LCS Dup
Added
Result Qualifier
5.00
5.00
D
NTU
% Rec
100
RPD
Limits
RPD
Limit
0
15
90 - 110
Duplicate Duplicate
Result Qualifier
Result Qualifier
ND
ND
RPD Unit
D
RPD
NTU
Limit
15
Lab Sample ID: 11C4582-DUP2 Matrix: Water Analysis Batch: 11C4582
Client Sample ID: NUC3009-01 Prep Type: total Prep Batch: 11C4582_P Duplicate Duplicate
Sample Sample
Turbidity
6
Client Sample ID: NUC2987-01 Prep Type: total Prep Batch: 11C4582_P Sample Sample
Analyte
90 - 110
% Rec. Unit
Lab Sample ID: 11C4582-DUP1 Matrix: Water Analysis Batch: 11C4582
Turbidity
Limits
Client Sample ID: 11C4582-BSD1 Prep Type: total Prep Batch: 11C4582_P
Turbidity
Analyte
% Rec
Result Qualifier
Result Qualifier
0.400
0.400
RPD Unit
D
RPD
Limit
0
15
NTU
Method: EPA 300.0 - General Chemistry Parameters Lab Sample ID: 11C4583-BLK1 Matrix: Water Analysis Batch: U004576
Client Sample ID: 11C4583-BLK1 Prep Type: total Prep Batch: 11C4583_P Blank Blank
Analyte
RL
Result Qualifier
MDL Unit
D
Prepared
Analyzed
Chloride
ND
1.00
mg/L
03/18/11 14:32
03/19/11 14:16
1.00
Sulfate
ND
1.00
mg/L
03/18/11 14:32
03/19/11 14:16
1.00
Lab Sample ID: 11C4583-BS1 Matrix: Water Analysis Batch: U004576 Spike
LCS LCS
% Rec.
Added
Chloride
3.00
2.85
mg/L
95
90 - 110
Sulfate
15.0
14.6
mg/L
97
90 - 110
Result Qualifier
Unit
D
Lab Sample ID: 11C4583-MS1 Matrix: Water Analysis Batch: U004576
% Rec
Limits
Client Sample ID: NUC2986-01 Prep Type: total Prep Batch: 11C4583_P Sample Sample
Analyte
Dil Fac
Client Sample ID: 11C4583-BS1 Prep Type: total Prep Batch: 11C4583_P
Analyte
Result Qualifier
Spike Added
Matrix Spike Matrix Spike
% Rec.
Result Qualifier
Unit
D
% Rec
Limits
Chloride
140
15.0
317 MHA
mg/L
1180
80 - 120
Sulfate
3.38
75.0
72.6
mg/L
92
80 - 120
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4 5
% Rec. Unit
Lab Sample ID: 11C4582-BSD1 Matrix: Water Analysis Batch: 11C4582 Analyte
1
03/24/2011
7 8 9 10 11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: EPA 300.0 - General Chemistry Parameters (Continued)
3
Lab Sample ID: 11C4583-DUP1 Matrix: Water Analysis Batch: U004576
Client Sample ID: NUC3019-01 Prep Type: total Prep Batch: 11C4583_P
4
RPD
5
Duplicate Duplicate
Sample Sample Analyte
Result Qualifier
Result Qualifier
Unit
D
RPD
Limit
Chloride
115
115
mg/L
0.4
20
Sulfate
5.50
6.70
mg/L
20
20
Lab Sample ID: 11C4645-BLK1 Matrix: Water Analysis Batch: 11C4645
Client Sample ID: 11C4645-BLK1 Prep Type: total Prep Batch: 11C4645_P Blank Blank Result Qualifier
Bicarbonate Alkalinity as CaCO3
ND
RL
MDL Unit
10.0
D
mg/L
Prepared
Analyzed
03/18/11 16:29
03/19/11 00:51
Lab Sample ID: 11C4645-DUP1 Matrix: Water Analysis Batch: 11C4645
Bicarbonate Alkalinity as CaCO3
Result Qualifier
190
187
RPD Unit
D
Limit
2
20
Client Sample ID: NUC2954-01 Prep Type: total Prep Batch: 11C4645_P Duplicate Duplicate
Sample Sample
Bicarbonate Alkalinity as CaCO3
RPD
mg/L
Result Qualifier
Result Qualifier
39.2
38.5
RPD Unit
D
RPD
Limit
2
20
mg/L
Lab Sample ID: 11C4657-BLK1 Matrix: Water Analysis Batch: 11C4657
Client Sample ID: 11C4657-BLK1 Prep Type: total Prep Batch: 11C4657_P Blank Blank
Analyte
Result Qualifier
Carbonate as CaCO3
ND
RL
MDL Unit
10.0
D
mg/L
Prepared
Analyzed
03/18/11 16:39
03/19/11 00:51
Lab Sample ID: 11C4657-DUP1 Matrix: Water Analysis Batch: 11C4657
Carbonate as CaCO3
Dil Fac
1.00
Client Sample ID: NUC2952-01 Prep Type: total Prep Batch: 11C4657_P Duplicate Duplicate
Sample Sample Analyte
Result Qualifier
Result Qualifier
ND
ND
RPD Unit
D
RPD
mg/L
Limit
20
Lab Sample ID: 11C5551-BLK1 Matrix: Water Analysis Batch: 11C5551
Client Sample ID: 11C5551-BLK1 Prep Type: total Prep Batch: 11C5551_P Blank Blank
Analyte
Bicarbonate Alkalinity as CaCO3
Result Qualifier
ND
RL
10.0
MDL Unit
mg/L
D
Prepared
Analyzed
03/22/11 22:25
03/23/11 02:16
Dil Fac
1.00
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Page 15 of 29
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1.00
Duplicate Duplicate
Result Qualifier
Lab Sample ID: 11C4645-DUP2 Matrix: Water Analysis Batch: 11C4645 Analyte
Dil Fac
Client Sample ID: NUC2952-01 Prep Type: total Prep Batch: 11C4645_P Sample Sample
Analyte
6 7
Method: SM 2320B - General Chemistry Parameters
Analyte
1
03/24/2011
11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SM 2320B - General Chemistry Parameters (Continued)
3
Lab Sample ID: 11C5551-DUP1 Matrix: Water Analysis Batch: 11C5551
Bicarbonate Alkalinity as CaCO3
Client Sample ID: NUC2956-01RE1 Prep Type: total Prep Batch: 11C5551_P
4
RPD
5
Duplicate Duplicate
Sample Sample Analyte
Result Qualifier
Result Qualifier
98.5
99.9
Unit
D
RPD
Limit
1
20
mg/L
Method: SM2510 B - General Chemistry Parameters Client Sample ID: 11C5627-BLK1 Prep Type: total Prep Batch: 11C5627_P Blank Blank RL
Result Qualifier
Specific conductance
ND
MDL Unit
10.0
D
umho/cm
Prepared
Analyzed
03/23/11 10:12
03/23/11 13:13
Lab Sample ID: 11C5627-BS1 Matrix: Water Analysis Batch: 11C5627 LCS LCS
Spike Added
Specific conductance
Result Qualifier
1410
1430
Unit
D
umho/cm
% Rec
101
Limits
90 - 110
Client Sample ID: NUC0332-01RE1 Prep Type: total Prep Batch: 11C5627_P Duplicate Duplicate
Sample Sample
Specific conductance
1.00
% Rec.
Lab Sample ID: 11C5627-DUP1 Matrix: Water Analysis Batch: 11C5627 Analyte
Dil Fac
Client Sample ID: 11C5627-BS1 Prep Type: total Prep Batch: 11C5627_P
Analyte
Result Qualifier
Result Qualifier
93.2
94.2
RPD Unit
D
RPD
Limit
1
10
umho/cm
Method: SM2540 C - General Chemistry Parameters Lab Sample ID: 11C4897-BLK1 Matrix: Water Analysis Batch: 11C4897
Client Sample ID: 11C4897-BLK1 Prep Type: dissolved Prep Batch: 11C4897_P Blank Blank
Analyte
RL
Result Qualifier
Total Dissolved Solids
ND
MDL Unit
10.0
D
mg/L
Prepared
Analyzed
03/19/11 23:30
03/19/11 23:30
Lab Sample ID: 11C4897-BS1 Matrix: Water Analysis Batch: 11C4897 Spike Added
Total Dissolved Solids
100
LCS LCS Result Qualifier
90.0
D
ug/mL
% Rec
90
Limits
90 - 110
Client Sample ID: NUC3009-01 Prep Type: dissolved Prep Batch: 11C4897_P Sample Sample
Total Dissolved Solids
1.00
% Rec. Unit
Lab Sample ID: 11C4897-DUP1 Matrix: Water Analysis Batch: 11C4897 Analyte
Dil Fac
Client Sample ID: 11C4897-BS1 Prep Type: dissolved Prep Batch: 11C4897_P
Analyte
Result Qualifier
304
6 7
Lab Sample ID: 11C5627-BLK1 Matrix: Water Analysis Batch: 11C5627 Analyte
1
Duplicate Duplicate Result Qualifier
306
RPD Unit
mg/L
D
RPD
Limit
0.7
5
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8 9 10 11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SM2540 D - General Chemistry Parameters
3
Lab Sample ID: 11C5102-BLK1 Matrix: Water Analysis Batch: 11C5102
Client Sample ID: 11C5102-BLK1 Prep Type: total Prep Batch: 11C5102_P Blank Blank
Analyte
RL
Result Qualifier
Total Suspended Solids
ND
MDL Unit
1.00
D
mg/L
Prepared
Analyzed
03/21/11 19:04
03/21/11 19:04
Lab Sample ID: 11C5102-BS1 Matrix: Water Analysis Batch: 11C5102 LCS LCS
Spike Added
Total Suspended Solids
Result Qualifier
100
97.7
D
mg/L
98
Result Qualifier
Result Qualifier
70.4
68.8
D
Total Suspended Solids
RPD
Limit
2
5
mg/L
Client Sample ID: 0316201122801 Prep Type: total Prep Batch: 11C5102_P Duplicate Duplicate
Sample Sample Result Qualifier
Result Qualifier
3.43
5.43 R4
RPD Unit
D
RPD
Limit
45
5
mg/L
Method: SM5540 C - General Chemistry Parameters Lab Sample ID: 11C4511-BLK1 Matrix: Water Analysis Batch: 11C4511
Client Sample ID: 11C4511-BLK1 Prep Type: total Prep Batch: 11C4511_P Blank Blank
Analyte
RL
Result Qualifier
MBAS (mol.wt 320)
ND
MDL Unit
0.0500
D
mg/L
Prepared
Analyzed
03/18/11 13:05
03/18/11 13:05
Lab Sample ID: 11C4511-BS1 Matrix: Water Analysis Batch: 11C4511
Dil Fac
1.00
Client Sample ID: 11C4511-BS1 Prep Type: total Prep Batch: 11C4511_P Spike
Analyte
Added
MBAS (mol.wt 320)
0.750
LCS LCS Result Qualifier
0.746
% Rec. Unit
D
mg/L
% Rec
99
Lab Sample ID: 11C4511-MS1 Matrix: Water Analysis Batch: 11C4511
Limits
80 - 120
Client Sample ID: NUC2953-01 Prep Type: total Prep Batch: 11C4511_P Sample Sample
Analyte
Result Qualifier
MBAS (mol.wt 320)
0.0313
Spike Added
0.750
Matrix Spike Matrix Spike Result Qualifier
0.768
% Rec. Unit
mg/L
D
% Rec
98
Limits
80 - 120
TestAmerica Nashville
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90 - 110
RPD Unit
4
Limits
Duplicate Duplicate
Lab Sample ID: 11C5102-DUP2 Matrix: Water Analysis Batch: 11C5102 Analyte
% Rec
Client Sample ID: NUC2446-01 Prep Type: total Prep Batch: 11C5102_P Sample Sample
Total Suspended Solids
1.00
% Rec. Unit
Lab Sample ID: 11C5102-DUP1 Matrix: Water Analysis Batch: 11C5102 Analyte
Dil Fac
Client Sample ID: 11C5102-BS1 Prep Type: total Prep Batch: 11C5102_P
Analyte
1
03/24/2011
10 11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SM5540 C - General Chemistry Parameters (Continued)
3
Lab Sample ID: 11C4511-MSD1 Matrix: Water Analysis Batch: 11C4511
Client Sample ID: NUC2953-01 Prep Type: total Prep Batch: 11C4511_P Sample Sample
Analyte
Result Qualifier
MBAS (mol.wt 320)
0.0313
Spike Matrix Spike Dup Matrix Spike Dup Added
Result Qualifier
0.750
0.772
% Rec.
Unit
D
mg/L
% Rec
99
RPD
Limits
80 - 120
RPD
Limit
0.6
20
Method: EPA 1664A - General Chemistry Parameters Client Sample ID: 11C5376-BLK1 Prep Type: total Prep Batch: 11C5376_P Blank Blank RL
Result Qualifier
Oil & Grease HEM
ND
MDL Unit
5.21
D
mg/L
Prepared
Analyzed
03/22/11 12:43
03/23/11 16:28
Lab Sample ID: 11C5376-BS1 Matrix: Water Analysis Batch: 11C5376 Analyte
Added
Oil & Grease HEM
40.0
LCS LCS Result Qualifier
36.9
Unit
D
mg/L
% Rec
92
Limits
78 - 114
Client Sample ID: 11C5376-BSD1 Prep Type: total Prep Batch: 11C5376_P
Analyte
Oil & Grease HEM
Spike
LCS Dup LCS Dup
Added
Result Qualifier
40.0
39.5
% Rec. Unit
D
mg/L
% Rec
99
Lab Sample ID: 11C5376-MS1 Matrix: Water Analysis Batch: 11C5376
Limits
78 - 114
RPD RPD
Limit
7
18
Client Sample ID: NUC1440-01 Prep Type: total Prep Batch: 11C5376_P Sample Sample
Oil & Grease HEM
1.00
% Rec.
Lab Sample ID: 11C5376-BSD1 Matrix: Water Analysis Batch: 11C5376
Analyte
Dil Fac
Client Sample ID: 11C5376-BS1 Prep Type: total Prep Batch: 11C5376_P Spike
Result Qualifier
1.15
Spike Added
40.0
Matrix Spike Matrix Spike Result Qualifier
41.8
% Rec. Unit
D
mg/L
% Rec
102
Limits
78 - 114
Method: EPA 170.1 - General Chemistry Parameters Lab Sample ID: 11C4508-DUP1 Matrix: Water Analysis Batch: 11C4508
Client Sample ID: NUC2986-01 Prep Type: total Prep Batch: 11C4508_P Sample Sample
Analyte
Temperature of pH determination
Result Qualifier
23.4
Duplicate Duplicate Result Qualifier
23.4
RPD Unit
D
Deg C
Lab Sample ID: 11C4508-DUP2 Matrix: Water Analysis Batch: 11C4508
Temperature of pH determination
RPD
Limit
0
200
Client Sample ID: NUC3008-01 Prep Type: total Prep Batch: 11C4508_P Sample Sample
Analyte
Result Qualifier
23.4
4 5 6 7
Lab Sample ID: 11C5376-BLK1 Matrix: Water Analysis Batch: 11C5376 Analyte
1
Duplicate Duplicate Result Qualifier
23.4
RPD Unit
Deg C
D
RPD
Limit
0
200
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03/24/2011
8 9 10 11 12
Quality Control Data Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Method: SM 4500 H B - General Chemistry Parameters
3
Lab Sample ID: 11C4508-BS1 Matrix: Water Analysis Batch: 11C4508
Client Sample ID: 11C4508-BS1 Prep Type: total Prep Batch: 11C4508_P Spike
Analyte
Added
pH
7.00
LCS LCS Result Qualifier
6.97
D
pH Units
100
Added
pH
7.00
LCS LCS Result Qualifier
7.04
D
pH Units
% Rec
101
Result Qualifier
6.30
Result Qualifier
6.30
D
pH Units
RPD
Limit
0
10
Client Sample ID: NUC3008-01 Prep Type: total Prep Batch: 11C4508_P Sample Sample Result Qualifier
7.80
Duplicate Duplicate Result Qualifier
7.80
RPD Unit
pH Units
D
RPD
Limit
0
10
TestAmerica Nashville
Page 19 of 29
8 9
95 - 105
RPD Unit
7
Limits
Duplicate Duplicate
Lab Sample ID: 11C4508-DUP2 Matrix: Water Analysis Batch: 11C4508
pH
6
Client Sample ID: NUC2986-01 Prep Type: total Prep Batch: 11C4508_P Sample Sample
Analyte
95 - 105
% Rec. Unit
Lab Sample ID: 11C4508-DUP1 Matrix: Water Analysis Batch: 11C4508
pH
Limits
Client Sample ID: 11C4508-BS2 Prep Type: total Prep Batch: 11C4508_P Spike
Analyte
% Rec
4 5
% Rec. Unit
Lab Sample ID: 11C4508-BS2 Matrix: Water Analysis Batch: 11C4508 Analyte
1
03/24/2011
10 11 12
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
GCMS Volatiles
3
Prep Batch: 11C5504_P Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C5504-BS1
11C5504-BS1
total
Water
EPA 5030B
Prep Batch
11C5504-BSD1
11C5504-BSD1
total
Water
EPA 5030B
11C5504-BLK1
11C5504-BLK1
total
Water
EPA 5030B
NUC3001-01
0316201122801
total
Ground Water
EPA 5030B
NUC3001-02
Trip Blank
total
Water
EPA 5030B
4 5 6 7
Analysis Batch: U004725 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5504-BS1
11C5504-BS1
total
Water
SW846 8260B
11C5504_P
11C5504-BSD1
11C5504-BSD1
total
Water
SW846 8260B
11C5504_P
11C5504-BLK1
11C5504-BLK1
total
Water
SW846 8260B
11C5504_P
NUC3001-01
0316201122801
total
Ground Water
SW846 8260B
11C5504_P
NUC3001-02
Trip Blank
total
Water
SW846 8260B
11C5504_P
8 9 10
Pesticides
11
Prep Batch: 11C4872_P
12
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4872-BLK1
11C4872-BLK1
Dissolved
Water
RSK 175/3810
Prep Batch
11C4872-BS1
11C4872-BS1
Dissolved
Water
RSK 175/3810
11C4872-BSD1
11C4872-BSD1
Dissolved
Water
RSK 175/3810
11C4872-MS1
NUC2978-01
Dissolved
Water
RSK 175/3810
11C4872-MSD1
NUC2978-01
Dissolved
Water
RSK 175/3810
NUC3001-01
0316201122801
Dissolved
Ground Water
RSK 175/3810
NUC3001-01 - RE1
0316201122801
Dissolved
Ground Water
RSK 175/3810
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4872-BLK1
11C4872-BLK1
Dissolved
Water
RSK 175
11C4872_P
11C4872-BS1
11C4872-BS1
Dissolved
Water
RSK 175
11C4872_P
11C4872-BSD1
11C4872-BSD1
Dissolved
Water
RSK 175
11C4872_P
11C4872-MS1
NUC2978-01
Dissolved
Water
RSK 175
11C4872_P
11C4872-MSD1
NUC2978-01
Dissolved
Water
RSK 175
11C4872_P
NUC3001-01
0316201122801
Dissolved
Ground Water
RSK 175
11C4872_P
NUC3001-01 - RE1
0316201122801
Dissolved
Ground Water
RSK 175
11C4872_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4512-BLK1
11C4512-BLK1
total
Water
SW846 7470A
11C4512_P
11C4512-BS1
11C4512-BS1
total
Water
SW846 7470A
11C4512_P
11C4512-BSD1
11C4512-BSD1
total
Water
SW846 7470A
11C4512_P
11C4512-MS1
NUC2982-01
total
Water
SW846 7470A
11C4512_P
11C4512-MSD1
NUC2982-01
total
Water
SW846 7470A
11C4512_P
NUC3001-01
0316201122801
total
Ground Water
SW846 7470A
11C4512_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4512-BLK1
11C4512-BLK1
total
Water
EPA 7470
11C4512-BS1
11C4512-BS1
total
Water
EPA 7470
11C4512-BSD1
11C4512-BSD1
total
Water
EPA 7470
Analysis Batch: U004542
Metals Analysis Batch: 11C4512
Prep Batch: 11C4512_P
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Page 20 of 29
03/24/2011
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
Metals (Continued)
3
Prep Batch: 11C4512_P (Continued) Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4512-MS1
NUC2982-01
total
Water
EPA 7470
Prep Batch
11C4512-MSD1
NUC2982-01
total
Water
EPA 7470
NUC3001-01
0316201122801
total
Ground Water
EPA 7470
4 5 6
Analysis Batch: 11C4553 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4553-BLK1
11C4553-BLK1
total
Water
SW846 6010C
11C4553_P
11C4553-BS1
11C4553-BS1
total
Water
SW846 6010C
11C4553_P
11C4553-BSD1
11C4553-BSD1
total
Water
SW846 6010C
11C4553_P
11C4553-MS1
NUC2783-02
total
Water
SW846 6010C
11C4553_P
11C4553-MSD1
NUC2783-02
total
Water
SW846 6010C
11C4553_P
NUC3001-01
0316201122801
total
Ground Water
SW846 6010C
11C4553_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4553-BLK1
11C4553-BLK1
total
Water
11C4553-BS1
11C4553-BS1
total
Water
11C4553-BSD1
11C4553-BSD1
total
Water
11C4553-MS1
NUC2783-02
total
Water
11C4553-MSD1
NUC2783-02
total
Water
NUC3001-01
0316201122801
total
Ground Water
EPA 3010A / 6010 EPA 3010A / 6010 EPA 3010A / 6010 EPA 3010A / 6010 EPA 3010A / 6010 EPA 3010A / 6010
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4511-BLK1
11C4511-BLK1
total
Water
SM5540 C
11C4511_P
11C4511-BS1
11C4511-BS1
total
Water
SM5540 C
11C4511_P
11C4511-MS1
NUC2953-01
total
Water
SM5540 C
11C4511_P
11C4511-MSD1
NUC2953-01
total
Water
SM5540 C
11C4511_P
NUC3001-01
0316201122801
total
Ground Water
SM5540 C
11C4511_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4511-BLK1
11C4511-BLK1
total
Water
SM5540C
11C4511-BS1
11C4511-BS1
total
Water
SM5540C
11C4511-MS1
NUC2953-01
total
Water
SM5540C
11C4511-MSD1
NUC2953-01
total
Water
SM5540C
NUC3001-01
0316201122801
total
Ground Water
SM5540C
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4582-BLK1
11C4582-BLK1
total
Water
EPA 180.1
11C4582_P
11C4582-BS1
11C4582-BS1
total
Water
EPA 180.1
11C4582_P
11C4582-BSD1
11C4582-BSD1
total
Water
EPA 180.1
11C4582_P
11C4582-DUP1
NUC2987-01
total
Water
EPA 180.1
11C4582_P
11C4582-DUP2
NUC3009-01
total
Water
EPA 180.1
11C4582_P
NUC3001-01
0316201122801
total
Ground Water
EPA 180.1
11C4582_P
Prep Batch: 11C4553_P
8 9 10 11 12
WetChem Analysis Batch: 11C4511
Prep Batch: 11C4511_P
Analysis Batch: 11C4582
TestAmerica Nashville
Page 21 of 29
7
03/24/2011
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
WetChem (Continued)
3
Prep Batch: 11C4582_P Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4582-BLK1
11C4582-BLK1
total
Water
NO PREP
Prep Batch
11C4582-BS1
11C4582-BS1
total
Water
NO PREP
11C4582-BSD1
11C4582-BSD1
total
Water
NO PREP
11C4582-DUP1
NUC2987-01
total
Water
NO PREP
11C4582-DUP2
NUC3009-01
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4583-BLK1
11C4583-BLK1
total
Water
NO PREP
11C4583-BS1
11C4583-BS1
total
Water
NO PREP
11C4583-MS1
NUC2986-01
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
11C4583-DUP1
NUC3019-01
total
Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4645-BLK1
11C4645-BLK1
total
Water
SM 2320B
11C4645_P
11C4645-DUP1
NUC2952-01
total
Water
SM 2320B
11C4645_P
11C4645-DUP2
NUC2954-01
total
Water
SM 2320B
11C4645_P
NUC3001-01
0316201122801
total
Ground Water
SM 2320B
11C4645_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4645-BLK1
11C4645-BLK1
total
Water
NO PREP
11C4645-DUP1
NUC2952-01
total
Water
NO PREP
11C4645-DUP2
NUC2954-01
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4657-BLK1
11C4657-BLK1
total
Water
SM 2320B
11C4657_P
11C4657-DUP1
NUC2952-01
total
Water
SM 2320B
11C4657_P
NUC3001-01
0316201122801
total
Ground Water
SM 2320B
11C4657_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4657-BLK1
11C4657-BLK1
total
Water
NO PREP
11C4657-DUP1
NUC2952-01
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4897-BLK1
11C4897-BLK1
Dissolved
Water
SM2540 C
11C4897_P
11C4897-BS1
11C4897-BS1
Dissolved
Water
SM2540 C
11C4897_P
11C4897-DUP1
NUC3009-01
Dissolved
Water
SM2540 C
11C4897_P
NUC3001-01
0316201122801
Dissolved
Ground Water
SM2540 C
11C4897_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4897-BLK1
11C4897-BLK1
Dissolved
Water
SOLIDS
11C4897-BS1
11C4897-BS1
Dissolved
Water
SOLIDS
5 6 7
Prep Batch: 11C4583_P Prep Batch
8 9 10 11
Analysis Batch: 11C4645
Prep Batch: 11C4645_P
Analysis Batch: 11C4657
Prep Batch: 11C4657_P
Analysis Batch: 11C4897
Prep Batch: 11C4897_P
TestAmerica Nashville
Page 22 of 29
4
03/24/2011
12
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
WetChem (Continued)
3
Prep Batch: 11C4897_P (Continued) Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C4897-DUP1
NUC3009-01
Dissolved
Water
SOLIDS
Prep Batch
NUC3001-01
0316201122801
Dissolved
Ground Water
SOLIDS
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5102-BLK1
11C5102-BLK1
total
Water
SM2540 D
11C5102_P
11C5102-BS1
11C5102-BS1
total
Water
SM2540 D
11C5102_P
11C5102-DUP1
NUC2446-01
total
Water
SM2540 D
11C5102_P
11C5102-DUP2
0316201122801
total
Water
SM2540 D
11C5102_P
NUC3001-01
0316201122801
total
Ground Water
SM2540 D
11C5102_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5102-BLK1
11C5102-BLK1
total
Water
SOLIDS
11C5102-BS1
11C5102-BS1
total
Water
SOLIDS
11C5102-DUP1
NUC2446-01
total
Water
SOLIDS
11C5102-DUP2
0316201122801
total
Water
SOLIDS
NUC3001-01
0316201122801
total
Ground Water
SOLIDS
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5551-BLK1
11C5551-BLK1
total
Water
SM 2320B
11C5551_P
11C5551-DUP1
NUC2956-01RE1
total
Water
SM 2320B
11C5551_P
NUC3001-01 - RE1
0316201122801
total
Ground Water
SM 2320B
11C5551_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5551-BLK1
11C5551-BLK1
total
Water
NO PREP
11C5551-DUP1
NUC2956-01RE1
total
Water
NO PREP
NUC3001-01 - RE1
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5627-BLK1
11C5627-BLK1
total
Water
SM2510 B
11C5627_P
11C5627-BS1
11C5627-BS1
total
Water
SM2510 B
11C5627_P
11C5627-DUP1
NUC0332-01RE1
total
Water
SM2510 B
11C5627_P
NUC3001-01
0316201122801
total
Ground Water
SM2510 B
11C5627_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5627-BLK1
11C5627-BLK1
total
Water
NO PREP
11C5627-BS1
11C5627-BS1
total
Water
NO PREP
11C5627-DUP1
NUC0332-01RE1
total
Water
NO PREP
NUC3001-01
0316201122801
total
Ground Water
NO PREP
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4583-BLK1
11C4583-BLK1
total
Water
EPA 300.0
11C4583_P
11C4583-BS1
11C4583-BS1
total
Water
EPA 300.0
11C4583_P
11C4583-MS1
NUC2986-01
total
Water
EPA 300.0
11C4583_P
NUC3001-01
0316201122801
total
Ground Water
EPA 300.0
11C4583_P
11C4583-DUP1
NUC3019-01
total
Water
EPA 300.0
11C4583_P
4 5
Analysis Batch: 11C5102
6 7 8 9
Prep Batch: 11C5102_P
11 12
Analysis Batch: 11C5551
Prep Batch: 11C5551_P
Analysis Batch: 11C5627
Prep Batch: 11C5627_P
Analysis Batch: U004576
TestAmerica Nashville
Page 23 of 29
10
03/24/2011
QC Association Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
Extractions
3
Analysis Batch: 11C5376 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C5376-BLK1
11C5376-BLK1
total
Water
EPA 1664A
11C5376_P
11C5376-BS1
11C5376-BS1
total
Water
EPA 1664A
11C5376_P
11C5376-BSD1
11C5376-BSD1
total
Water
EPA 1664A
11C5376_P
11C5376-MS1
NUC1440-01
total
Water
EPA 1664A
11C5376_P
NUC3001-01
0316201122801
total
Ground Water
EPA 1664A
11C5376_P
4 5 6 7
Prep Batch: 11C5376_P Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
11C5376-BLK1
11C5376-BLK1
total
Water
11C5376-BS1
11C5376-BS1
total
Water
11C5376-BSD1
11C5376-BSD1
total
Water
11C5376-MS1
NUC1440-01
total
Water
NUC3001-01
0316201122801
total
Ground Water
1664 HEM/SGTHEM 1664 HEM/SGTHEM 1664 HEM/SGTHEM 1664 HEM/SGTHEM 1664 HEM/SGTHEM
Prep Batch
8 9 10 11 12
TCLP Analysis Batch: 11C4508 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4508-BS1
11C4508-BS1
total
Water
SM 4500 H B
11C4508_P
11C4508-BS2
11C4508-BS2
total
Water
SM 4500 H B
11C4508_P
11C4508-DUP1
NUC2986-01
total
Water
SM 4500 H B
11C4508_P
11C4508-DUP1
NUC2986-01
total
Water
EPA 170.1
11C4508_P
11C4508-DUP2
NUC3008-01
total
Water
SM 4500 H B
11C4508_P
11C4508-DUP2
NUC3008-01
total
Water
EPA 170.1
11C4508_P
NUC3001-01
0316201122801
total
Ground Water
SM 4500 H B
11C4508_P
NUC3001-01
0316201122801
total
Ground Water
EPA 170.1
11C4508_P
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
11C4508-BS1
11C4508-BS1
total
Water
METHOD PREP
11C4508-BS2
11C4508-BS2
total
Water
METHOD PREP
11C4508-DUP1
NUC2986-01
total
Water
METHOD PREP
11C4508-DUP2
NUC3008-01
total
Water
METHOD PREP
NUC3001-01
0316201122801
total
Ground Water
METHOD PREP
Prep Batch: 11C4508_P
TestAmerica Nashville
Page 24 of 29
03/24/2011
Lab Chronicle Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
2
Client Sample ID: 0316201122801
Lab Sample ID: NUC3001-01
Date Collected: 03/16/11 10:50 Date Received: 03/18/11 08:30
Matrix: Ground Water
Dilution
Batch
Batch
Prepared
Prep Type
Type
Method
Factor
Number
Analyst
Lab
total
Prep
EPA 5030B
1.00
11C5504_P
03/21/11 10:05
TSP
TestAmerica Nashville
total
Analysis
SW846 8260B
1.00
U004725
03/22/11 16:18
FE
TestAmerica Nashville
Dissolved
Prep
RSK 175/3810
1.00
11C4872_P
03/21/11 09:00
WAM
TestAmerica Nashville
Dissolved
Analysis
RSK 175
1.00
U004542
03/21/11 10:49
ljt
TestAmerica Nashville
Dissolved
Prep
RSK 175/3810
RE1
1.00
11C4872_P
03/21/11 09:00
WAM
TestAmerica Nashville
Dissolved
Analysis
RSK 175
RE1
5.00
U004542
03/21/11 10:53
ljt
TestAmerica Nashville
total
Prep
1.00
11C4553_P
03/19/11 09:13
MET
TestAmerica Nashville
total
Analysis
EPA 3010A / 6010 SW846 6010C
1.00
11C4553
03/21/11 12:57
LTB
TestAmerica Nashville
total
Prep
EPA 7470
1.00
11C4512_P
03/21/11 10:25
DEB
TestAmerica Nashville
total
Analysis
SW846 7470A
1.00
11C4512
03/21/11 13:53
DEB
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C4645_P
03/18/11 16:29
JAG2
TestAmerica Nashville
total
Analysis
SM 2320B
1.00
11C4645
03/19/11 02:02
JAG2
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C4657_P
03/18/11 16:39
JAG2
TestAmerica Nashville
total
Analysis
SM 2320B
1.00
11C4657
03/19/11 02:02
JAG2
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C4583_P
03/18/11 14:32
amc
TestAmerica Nashville
total
Analysis
EPA 300.0
5.00
U004576
03/19/11 16:17
amc
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C5627_P
03/23/11 10:12
TEM
TestAmerica Nashville
total
Analysis
SM2510 B
1.00
11C5627
03/23/11 13:13
TEM
TestAmerica Nashville
total
Analysis
SM5540 C
1.00
11C4511
03/18/11 13:05
JJR
TestAmerica Nashville
total
Prep
SM5540C
1.00
11C4511_P
03/18/11 13:05
AMJ
TestAmerica Nashville
Dissolved
Analysis
SM2540 C
1.00
11C4897
03/19/11 23:30
cob
TestAmerica Nashville
Dissolved
Prep
SOLIDS
1.00
11C4897_P
03/19/11 23:30
cob
TestAmerica Nashville
total
Analysis
SM2540 D
1.43
11C5102
03/21/11 19:04
bmc
TestAmerica Nashville
total
Prep
SOLIDS
1.43
11C5102_P
03/21/11 19:04
bmc
TestAmerica Nashville
total
Analysis
EPA 180.1
1.00
11C4582
03/18/11 14:31
KJA
TestAmerica Nashville
total
Prep
NO PREP
1.00
11C4582_P
03/18/11 14:31
KJA
TestAmerica Nashville
total
Prep
NO PREP
RE1
1.00
11C5551_P
03/22/11 22:24
JAG2
TestAmerica Nashville
total
Analysis
SM 2320B
RE1
1.00
11C5551
03/23/11 03:28
JAG2
TestAmerica Nashville
total
Prep
1.00
11C5376_P
03/23/11 10:00
BJM
TestAmerica Nashville
total
Analysis
1664 HEM/SGTHEM EPA 1664A
1.00
11C5376
03/23/11 16:28
MSR
TestAmerica Nashville
total
Analysis
SM 4500 H B
1.00
11C4508
03/18/11 15:30
SJM
TestAmerica Nashville
total
Prep
METHOD PREP
1.00
11C4508_P
03/18/11 15:30
SJM
TestAmerica Nashville
total
Analysis
EPA 170.1
1.00
11C4508
03/18/11 15:30
SJM
TestAmerica Nashville
Or Analyzed
Client Sample ID: Trip Blank
5 6 7 8 9 10 11 12
Lab Sample ID: NUC3001-02
Date Collected: 03/16/11 00:01 Date Received: 03/18/11 08:30
Matrix: Water
Batch
Batch
Prep Type
Type
Method
Dilution
Batch
Factor
Number
total
Prep
Analyst
Lab
EPA 5030B
1.00
11C5504_P
03/21/11 10:05
TSP
total
Analysis
TestAmerica Nashville
SW846 8260B
1.00
U004725
03/22/11 16:49
FE
TestAmerica Nashville
Run
Prepared Or Analyzed
TestAmerica Nashville
Page 25 of 29
3 4
Batch
Run
1
03/24/2011
Method Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
TestAmerica Job ID: NUC3001
1 2
Method
Method Description
EPA 1664A
General Chemistry Parameters
Protocol
Laboratory
TAL NSH
EPA 170.1
General Chemistry Parameters
TAL NSH
SM 4500 H B
General Chemistry Parameters
TAL NSH
SW846 8260B
Volatile Organic Compounds by EPA Method 8260B
TAL NSH
RSK 175
Methane, Ethane, and Ethene by GC
TAL NSH
SW846 6010C
Total Metals by EPA 6010C
TAL NSH
SW846 7470A
Mercury by EPA Methods 7470A/7471A
TAL NSH
EPA 180.1
General Chemistry Parameters
TAL NSH
EPA 300.0
General Chemistry Parameters
TAL NSH
SM 2320B
General Chemistry Parameters
TAL NSH
SM2510 B
General Chemistry Parameters
TAL NSH
SM2540 C
General Chemistry Parameters
TAL NSH
SM2540 D
General Chemistry Parameters
TAL NSH
SM5540 C
General Chemistry Parameters
TAL NSH
3 4 5 6 7 8 9 10
Protocol References:
11 12
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Road, Nashville, TN 37204, TEL 800-765-0980
TestAmerica Nashville
Page 26 of 29
03/24/2011
Certification Summary Client: SAIC Energy, Environment & Infrastructure, LLC/CHK Project/Site: Property ID# 908055
Laboratory
Authority
TestAmerica Nashville
TestAmerica Job ID: NUC3001
2
Program
EPA Region
AIHA
TestAmerica Nashville
1
USDA
Certification ID
* Expiration Date
100790
09/01/11
S-48469
11/02/13
TestAmerica Nashville
A2LA
A2LA
0
0453.07
12/31/11
TestAmerica Nashville
A2LA
WY UST
0
453.07
12/31/11
TestAmerica Nashville
Alabama
State Program
4
41150
03/19/11
TestAmerica Nashville
Alaska
Alaska UST
10
UST-087
07/24/11
TestAmerica Nashville
Arizona
State Program
9
AZ0473
05/05/11
TestAmerica Nashville
Arkansas
State Program
6
88-0737
04/25/11
TestAmerica Nashville
CALA
CALA
0
3744
03/08/14
TestAmerica Nashville
California
NELAC
9
1168CA
10/31/11
TestAmerica Nashville
Colorado
State Program
8
N/A
02/28/12
TestAmerica Nashville
Connecticut
State Program
1
PH-0220
12/31/11
TestAmerica Nashville
Florida
NELAC
4
E87358
06/30/11
TestAmerica Nashville
Illinois
NELAC
5
200010
12/09/11
TestAmerica Nashville
Iowa
State Program
7
131
05/01/12
TestAmerica Nashville
Kansas
NELAC
7
E-10229
10/31/11
TestAmerica Nashville
Kentucky
Kentucky UST
4
19
07/13/12
TestAmerica Nashville
Kentucky
State Program
4
90038
12/31/11
TestAmerica Nashville
Louisiana
NELAC
6
LA100011
12/31/11
TestAmerica Nashville
Louisiana
NELAC
6
30613
06/30/11
TestAmerica Nashville
Maryland
State Program
3
316
03/31/11
TestAmerica Nashville
Massachusetts
State Program
1
M-TN032
06/30/11
TestAmerica Nashville
Minnesota
NELAC
5
047-999-345
12/31/11
TestAmerica Nashville
Mississippi
State Program
4
N/A
06/30/11
TestAmerica Nashville
Montana
MT DEQ UST
8
NA
01/01/15
TestAmerica Nashville
Nevada
State Program
9
TN00032
07/31/11
TestAmerica Nashville
New Hampshire
NELAC
1
2963
10/09/11
TestAmerica Nashville
New Jersey
NELAC
2
TN965
06/30/11
TestAmerica Nashville
New York
NELAC
2
11342
04/01/11
TestAmerica Nashville
North Carolina
North Carolina DENR
4
387
12/31/11
TestAmerica Nashville
North Dakota
State Program
8
R-146
06/30/11
TestAmerica Nashville
Ohio
OVAP
5
CL0033
04/01/12
TestAmerica Nashville
Oklahoma
State Program
6
9412
08/31/11
TestAmerica Nashville
Oregon
NELAC
10
TN200001
04/30/11
TestAmerica Nashville
Pennsylvania
NELAC
3
68-00585
06/30/11
TestAmerica Nashville
Rhode Island
State Program
1
LAO00268
12/30/11
TestAmerica Nashville
South Carolina
State Program
4
84009
03/19/11
TestAmerica Nashville
South Carolina
State Program
4
84009
04/30/11
TestAmerica Nashville
Tennessee
State Program
4
2008
03/19/11
TestAmerica Nashville
Texas
NELAC
6
T104704077-09-TX
08/31/11
TestAmerica Nashville
Utah
NELAC
8
TAN
06/30/11
TestAmerica Nashville
Virginia
State Program
3
00323
06/30/11
TestAmerica Nashville
Washington
State Program
10
C789
07/19/11
TestAmerica Nashville
West Virginia
West Virginia DEP
3
219
04/30/11
TestAmerica Nashville
Wisconsin
State Program
5
998020430
08/31/11
Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s current list of certified methods and analytes. * Any expired certifications in this list are currently pending renewal and are considered valid.
TestAmerica Nashville
Page 27 of 29
03/24/2011
3 4 5 6 7 8 9 10 11 12
1 2 3 4 5 6 7 8 9 10 11 12
Page 28 of 29
03/24/2011
1 2 3 4 5 6 7 8 9 10 11 12
Page 29 of 29
03/24/2011
