CHEM 053

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SBE & Experiment 1

CHEM  053  

Determining  an  Empirical  Formula  

Today’s  Agenda:   •  •  •  • 

CHEM  053  

Review  announcements   Discuss  safety  and  lab  accidents   SBE:  Mass  and  Volume  Measurement   EF:  Determining  an  EF  

•  Things  that  are  DUE:   •  BEFORE  TOMORROW:  safety  agreement  &   safety  quiz   •  IN  LAB:  SBE  questions  (done  in  Notebook),   EF  notebook  pages  (data  collections)   •  NEXT  WEEK:  EF  Data  Sheet  

Where  are  we  going?  

CHEM  053  

UNIT  1:   Understanding  Substances  &  Reactions   UNIT  2:   Analyzing  Elements  &  Substances   UNIT  3:   Investigating  Reactions   We  will  now  begin  learning  lab  techniques  and  doing   experiments  to  understand  chemical  substances  

Course  Material  

CHEM  053  

All you need to know about the structure of this Chemistry Lab is posted online.

Link to Blackboard: https://courseweb.library.upenn.edu  

Let’s review the most important points!

What  do  you  need?  

CHEM  053  

§ Yourself  -­‐  Participation  MANDATORY   § Calculator  and/or  laptop  computer   § Lab  Notebook   § Your  Penn  ID  

Lab  Notebooks  

CHEM  053  

What  are  some  of  the  guidelines  for  keeping  a  lab   notebook?   • Pre-­‐write  tables,  etc.   • Leave  a  lot  of  space   • ?   • ?    

LAB  SAFETY  !?!  

CHEM  053  

We  expect  everyone  to  LEARN  and   FOLLOW  safe  lab  practices!   We  will  take  a  few  minutes  now  to  review  some  basic   safety  information.  You  can  always  consult  the  safety   section  on  Blackboard,  your  instructor,  or  TA  for  more   information.  

What  to  do  if…  

CHEM  053  

You  spill  acid  on  the  bench?   You  spill  acid  on  your  arm?   You  get  a  chemical  in  your  eye?   You  break  a  piece  of  glassware?  

In  Lab  This  Week!  

CHEM  053  

  Skill  Building  Exercise   &  Empirical  Formula       You  MUST  attend  lab  on  time!   Let’s  review  the  experiments:  

SBE!   Transferring  and     Measuring  chemicals     Using  a  Balance  

CHEM  053  

Mass  &  Volume   Measurement!  

CHEM  053  

Comparing  Vol.  pipet  and  graduate   cylinder!   Using  a  graduated  pipet!   Using  transfer  pipet!  

SBE!   Using  a   Balance  

CHEM  053  

Lab  Etiquette  

CHEM  053  

Recap ALL Bottles at hood and balance bench. Clean up after yourself.

CHEM  053  

This  Week!   Experiment  1    

Determining  an  Empirical  Formula    Using  a  Balance    Becoming  familiar  with  the  lab    Keeping  a  notebook  

Textbook  Readings  

CHEM  053  

§  3.1 & 3.2 Atomic Masses and the Mole §  3.4

Percent Composition

§  3.5

Determining Formulas

(Review NAMING in Chapter 2 if you are not comfortable with naming ions and compounds) MEMORIZE Table 2.5!

CHEM  053   Molecular  or  Covalent  Compounds   Substances in which “particles” are composed of two or more DIFFERENT ATOMS joined together are called compounds.

H2 O

Molecule

Molecular Formula

Symbolic

Compound

Pure substance

Macroscopic

All “particles” are identical

(Water)

Microscopic

CHEM  053  

How  do  we  know  how  many   atoms  of  each  type?  

We perform elemental analysis of the compound Find the percentage of each element present in the substance and use it to find relative proportions. During physical activity, a substance forms in muscle tissue and is responsible for muscle soreness. 40.0% C, 6.71% H, 53.3% O Always the same proportions à Chemical Compound

Counting  Particles  

CHEM  053  

Is it practical, in a lab situation, to physically COUNT the particles? NO!! The particles are too small! So – how do we typically measure the amount of a substance we have in a laboratory? We use the MASS to determine the amount of substance. How is mass related to the number of particles?

Molar  Mass  

CHEM  053  

The mass of one mole of atoms is called the Molar Mass of the element Average Mass (g) = Molar Mass The Molar Mass is the mass of 6.0221 x 1023 of particles of a given substance. 1 mol of C = 6.0221 x 1023 atoms of C M(C) = 12.0107 g/mol

How  do  they  compare?  

CHEM  053  

6.0221 x 1023 particles or units in each If we weigh them, the mass we get is called the “Molar Mass”

These are one mole of 6 different substances.

In  Lab  This  Week…  

CHEM  053  

You  can  complete  the  data  sheet  and  turn  it  in  before   you  leave.  

A  few  more  reminders…  

CHEM  053  

§  Next  time,  remember  to  bring:   §  Your  lab  notebook   §  A  lock  for  the  locker  in  the  hall   §  Your  drawer  key   §  Your  Penn  ID   §  Wear  appropriate  clothes  and  bring  your   safety  glasses  and  apron.   §  Sign  the  safety  agreement  online  and  take  the   safety  quiz  on  Bb  

Questions?  

CHEM  053  

Your  TA  and  I  are   here  to  help.   Check  Blackboard  FREQUENTLY.    

Email  with  any  questions!  

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