Flash Accessories and TLC
flash & tlc
Flash Accessories and TLC Reveleris® Flash Chromatography System Verification Kits
Solid Loaders s¬(IGH¬PRESSURE¬DESIGN s¬%ASY¬TO¬USE s¬)DEAL¬FOR¬LOW¬SOLUBILITY¬LOADING
s¬+ITS¬INCLUDE¬¬TUBES¬WITH¬PREABSORBED¬TEXT¬MIX¬AND¬lVE¬ G¬mASH¬CARTRIDGES Reveleris® System Verification Kits Description
Solid Loaders Qty.
Part No.
Empty 3g Empty 15g Empty 40g Silica 3g Silica 15g Silica 40g Adjustable 3g Plunger Adjustable 15g Plunger Adjustable 40g Plunger 3g Frit Insertion Rod 15g Frit Insertion Rod 40g Frit Insertion Rod
100 100 50 20 16 12 ea ea ea ea ea ea
5142050 5142051 5147808 5152371 5142034 5147772 5148510 5148511 5148512 5162931 5162902 5162901
Reveleris® Method Development TLC Plates and C18 Scouting Columns One of the first steps in scale-up of flash chromatography separations is to optimize the mobile phase. Two methods are commonly used to determine the optimum mobile phase composition. Resulting data is used to automatically generate flash gradient profiles in the Reveleris® Navigator™ software. For normal phase purifications, thin layer chromatography (TLC) plates made with the same high purity silica as used in the Reveleris® and GraceResolv™ cartridges are used to ensure the same selectivity and allow simple scale-up. For reversed-phase applications, Reveleris® C18 scouting columns are the perfect method development tool to optimize mobile phase choice. Flash TLC Plates Description
GraceResolv™ Silica TLC Plates Reveleris® Silica TLC Plates Reversed-Phase C18 TLC Plate Silica Aluminum-backed TLC Plates (UV254) Silica Aluminum-backed TLC Plates (no UV)
Size
Qty.
Part No.
20 x 20cm 20 x 20cm 10 x 20cm 20 x 20cm 20 x 20cm
25 25 25 25 25
8618900 8621250 8625320 8628490 8628492
5157882 5157883
Flash Cartridge Kits s¬/PTIMIZED¬FOR¬SPECIlC¬APPLICATION¬AREAS s¬-ETHOD¬DEVELOPMENT¬PACKS Flash Cartridge Kits Description
Part No.
Reveleris® Silica Cartridge Select Pack (2) 4g Si, (2) 12g Si, (2) 40g Si Radiochem Flash Kit (3) 4g Si, (3) 4g C18, (3) 4g Diol, (10) 3g Loaders Impurity Isolation Flash Kit (2) 12g C18, (2) 12g Diol, (1) 120g C18, (1) 120g Diol Natural Product Flash Kit (3) 12g C18, (3) 12g Si, (3) 3g Loaders Carbohydrate Flash Kit (3) 12g C18, (3) 12g Amino Lipid Flash Kit (3) 12g Si, (3) 12g C18, (3) 12g Diol
flash
Description
Part No.
Reveleris® System Verification Kit High Concentration Flash Test Mix Reveleris® iES System Verification Kit Low Concentration Flash Test Mix
5158903 5157384 5157386 5157388 5157385 5157387
Flash System Adapters Flash System Adapters Description
Part No.
Reveleris® Flow Diverting Bypass Kit Bypasses the Column Position to Connect Large Cartridges to the Reveleris® Flash System Includes Bypass Tube (Part No. 8627100), Fittings, and Tubing GraceResolv™ 750g Flash Cartridge Adapter Kit Adapts GraceResolv™ 750g Cartridge to the Reveleris® Flash System Also Requires Flow Diverting Bypass Kit (Part No. 5164530) GraceResolv™ 1500g Flash Cartridge Adapter Kit Adapts GraceResolv™ 1500g Cartridge to the Reveleris® Flash System Also Requires Flow Diverting Bypass Kit (Part No. 5164530)
5164530
5157890
5156862
Reveleris® C18 HPLC Columns Reveleris® C18 HPLC Columns* Description
C18 HPLC Column C18 HPLC Column C18 HPLC Column
Size
Qty.
Part No.
4.6 x 50mm 4.6 x 150mm 4.6 x 250mm
3 3 3
5156381 5156382 5156383
&OR¬USE¬WITH¬2EVELERIS®¬.AVIGATOR™¬3OFTWARE
www.discoverysciences.com
35
flash & tlc
TLC Plates Analtech Uniplates™ TLC Plates
Adsorbosil® Soft Layer TLC Plates s¬#ONTAINS¬NO¬ORGANIC¬BINDERS s¬3AMPLE¬ZONES¬ARE¬EASY¬TO¬REMOVE¬FOR¬FURTHER¬ANALYSIS Soft Layer Adsorbosil® Prekotes TLC Plates Description
Size
Soft Layer Prekotes, Glass-Backed Conventional Adsorbosil®-Plus 20 x 20cm Adsorbosil®-Plus P* 20 x 20cm Adsorbosil®-Plus 1 20 x 20cm Adsorbosil®-Plus 1 P* 20 x 20cm
Layer Thickness
Qty.
Part No.
250μm 250μm 250μm 250μm
25 25 25 25
16384 16376 16330 16322
0¬ ¬7ITH¬&LUORESCENT¬)NDICATOR ¬¬WAVELENGTH
Silica Gel H and HF Uniplates™ TLC Plates s¬3OFT¬,AYER n¬#ONTAINS¬NO¬ORGANIC¬BINDER n¬#ONTAINS¬NO¬CALCUIM¬SULFATE¬BINDER s¬(ARD¬,AYER n¬#ONTAINS¬AN¬ORGANIC¬BINDER n¬¬WATER¬RESISTANT n¬6ISUALIZATION¬BY¬CHARRING¬UP¬TO¬# Silica Gel H and HF Uniplates™ TLC Plates
tlc
Description
Macherey-Nagel TLC Plates s¬±¬PORE¬SIZE ¬¬TO¬«M¬PARTICLE¬SIZE s¬"INDER¬IS¬ORGANIC ¬STABLE¬IN¬MOST¬ORGANIC¬SOLVENTS¬AND¬ AGGRESSIVE¬DETECTION¬REAGENTS
Soft Layer, No Binders Conventional 20 x 20cm 10 x 20cm Hard Layer, Organic Binder Conventional 20 x 20cm 10 x 20cm
Layer Thickness
Qty.
H Part No.
HF* Part No.
250μm 250μm
25 25
710011 710021
720011 7200210
250μm 250μm
25 25
746011 746021
747011 747021
& &LUORESCENT¬)NDICATOR ¬NM
Macherey-Nagel TLC Plates Description
Size
Silica Gel Plates, Glass-Backed Conventional Layers, Silica Gel 60 SIL G-25 5 x 10cm SIL G-25 5 x 20cm SIL G-25 20 x 20cm SIL G-25 UV254 5 x 20cm SIL G-25 UV254 20 x 20cm SIL G-25 UV254+366 20 x 20cm Polyester-Backed TLC Plates Silica Gel 60 SIL G 20 x 20cm SIL G/UV254 4 x 8cm SIL G/UV 254 20 x 20cm SIL N-HR/UV254 20 x 20cm
36
Layer Thickness
Qty.
Part No.
250μm 250μm 250μm 250μm 250μm 250μm
50 100 25 100 25 25
809017 809011 809013 809021 809023 809123
Silica Gel G and GF Uniplates™ TLC Plates s¬#ALCIUM¬3ULFATE¬"INDER s¬#ONTAINS¬NO¬ORGANIC¬BINDER Silica Gel G and GF Uniplates™ TLC Plates Description
250μm 250μm 250μm 200μm
25 50 25 25
805013 805021 805023 804023
Soft Layer, No Binders Conventional 20 x 20cm 10 x 20cm
Layer Thickness
Qty.
G Part No.
GF* Part No.
250μm 250μm
25 25
701011 701021
702011 702021
& &LUORESCENT¬)NDICATOR ¬NM
more info
technical assistance
For additional information about flash chromatography, including application notes and technical posters, visit our website.
Contact Tech Support: Email: [email protected] Online: www.discoverysciences.com
flash & tlc
TLC Accessories TLC Plate Cutter
TLC Tanks and Storage
s¬3CORES¬COATED¬GLASS¬PLATES¬AT¬ ANY¬POSITION s¬#OMPACT ¬PORTABLE ¬AND¬EASY¬ TO¬OPERATE
Latch-Lid TLC Tank s¬5NIQUE¬LATCHING¬DEVICE¬ASSURES¬TIGHT¬¬ SEAL¬BETWEEN¬LID¬AND¬TANK s¬.O¬MESSY¬GREASE¬SEALS
Latch-Lid Tank Description
Latch-Lid Tank/Lid Unit Latch-Lid Tank/Lid Unit
Size
Part No.
10 x 10cm Plates 20 x 20cm Plates
7542 7536
Multiple Plate Development Rack
The TLC plate cutter has a high-quality carbide scriber mounted into a movable plastic head. It is designed to produce optimal scoring on the glass surface of 20 x 20cm TLC plates with a total thickness (glass + coating) of 2mm. A smaller template is included with the unit for ease in cutting 10 x 10cm plates. TLC Plate Cutter
s¬3AVES¬TIME¬AND¬MONEY
Qty.
Part No.
TLC Plate Cutter Replacement Scribers Replacement Scribers
ea ea 3
7535 7565 7575
tlc
Description
Multiple Plate Development Rack Description
Anodized Aluminum Rack Anodized Aluminum Rack
Size
Part No.
20 x 20cm Plates 10 x 10cm Plates
17051 17053
Sample Applicators Uncalibrated Disposable Micropipettes Uncalibrated disposable glass micropipettes are intended for rapid qualitative sample application on TLC plates. Thick walls make these pipettes strong and easy to handle. Overall length is about three inches. Capacity is approximately 2–8μL.
Preval® Sprayers Compressed Gas Sprayer Compressed Gas Sprayers provide a constant pressure and uniform distribution of fine mist on your TLC plate. The pressure unit contains difluoroethane. Unit sprays up to 16oz of liquid. Caution: Wetted parts are made of polypropylene or nylon. Do not store with dip tube immersed in reagent.
Uncalibrated Disposable Micropipettes Description
Glass Micropipettes Glass Micropipettes
Complete Spray Unit with Glass Jar Replacement Glass Jar with Lid Replacement Compressed Gas Unit
Part No.
7616 17203
Qty.
Part No.
100
3842
Drummond® Wiretrol® Micropipettes
Compressed Gas Sprayer Description
Qty.
300 1440
Qty.
Part No.
3 6 6
14654 14655 14657
Spraying Accessories
s¬#OMBINES¬THE¬ACCURACY¬OF ¬A¬ MICROSYRINGE¬WITH¬THE¬EASE¬AND¬ ECONOMY¬OF ¬A¬DISPOSABLE¬PIPETTE
Drummond® Wiretrol® Micropipettes Description/Capacity
Disposable Spray Box
1.0 to 5.0μL (Calibrated)
s¬(EAVY¬DUTY¬CARDBOARD¬WITH¬DISPOSAL¬ BAG¬PROVIDED
TLC Spray Supports Description
Disposable Spray Box
Qty.
Part No.
5
16408
www.discoverysciences.com
37
Flash Accessories and TLC Reveleris® Flash Chromatography System Verification Kits
Solid Loaders s¬(IGH¬PRESSURE¬DESIGN s¬%ASY¬TO¬USE s¬)DEAL¬FOR¬LOW¬SOLUBILITY¬LOADING
s¬+ITS¬INCLUDE¬¬TUBES¬WITH¬PREABSORBED¬TEXT¬MIX¬AND¬lVE¬ G¬mASH¬CARTRIDGES Reveleris® System Verification Kits Description
Solid Loaders Qty.
Part No.
Empty 3g Empty 15g Empty 40g Silica 3g Silica 15g Silica 40g Adjustable 3g Plunger Adjustable 15g Plunger Adjustable 40g Plunger 3g Frit Insertion Rod 15g Frit Insertion Rod 40g Frit Insertion Rod
100 100 50 20 16 12 ea ea ea ea ea ea
5142050 5142051 5147808 5152371 5142034 5147772 5148510 5148511 5148512 5162931 5162902 5162901
Reveleris® Method Development TLC Plates and C18 Scouting Columns One of the first steps in scale-up of flash chromatography separations is to optimize the mobile phase. Two methods are commonly used to determine the optimum mobile phase composition. Resulting data is used to automatically generate flash gradient profiles in the Reveleris® Navigator™ software. For normal phase purifications, thin layer chromatography (TLC) plates made with the same high purity silica as used in the Reveleris® and GraceResolv™ cartridges are used to ensure the same selectivity and allow simple scale-up. For reversed-phase applications, Reveleris® C18 scouting columns are the perfect method development tool to optimize mobile phase choice. Flash TLC Plates Description
GraceResolv™ Silica TLC Plates Reveleris® Silica TLC Plates Reversed-Phase C18 TLC Plate Silica Aluminum-backed TLC Plates (UV254) Silica Aluminum-backed TLC Plates (no UV)
Size
Qty.
Part No.
20 x 20cm 20 x 20cm 10 x 20cm 20 x 20cm 20 x 20cm
25 25 25 25 25
8618900 8621250 8625320 8628490 8628492
5157882 5157883
Flash Cartridge Kits s¬/PTIMIZED¬FOR¬SPECIlC¬APPLICATION¬AREAS s¬-ETHOD¬DEVELOPMENT¬PACKS Flash Cartridge Kits Description
Part No.
Reveleris® Silica Cartridge Select Pack (2) 4g Si, (2) 12g Si, (2) 40g Si Radiochem Flash Kit (3) 4g Si, (3) 4g C18, (3) 4g Diol, (10) 3g Loaders Impurity Isolation Flash Kit (2) 12g C18, (2) 12g Diol, (1) 120g C18, (1) 120g Diol Natural Product Flash Kit (3) 12g C18, (3) 12g Si, (3) 3g Loaders Carbohydrate Flash Kit (3) 12g C18, (3) 12g Amino Lipid Flash Kit (3) 12g Si, (3) 12g C18, (3) 12g Diol
flash
Description
Part No.
Reveleris® System Verification Kit High Concentration Flash Test Mix Reveleris® iES System Verification Kit Low Concentration Flash Test Mix
5158903 5157384 5157386 5157388 5157385 5157387
Flash System Adapters Flash System Adapters Description
Part No.
Reveleris® Flow Diverting Bypass Kit Bypasses the Column Position to Connect Large Cartridges to the Reveleris® Flash System Includes Bypass Tube (Part No. 8627100), Fittings, and Tubing GraceResolv™ 750g Flash Cartridge Adapter Kit Adapts GraceResolv™ 750g Cartridge to the Reveleris® Flash System Also Requires Flow Diverting Bypass Kit (Part No. 5164530) GraceResolv™ 1500g Flash Cartridge Adapter Kit Adapts GraceResolv™ 1500g Cartridge to the Reveleris® Flash System Also Requires Flow Diverting Bypass Kit (Part No. 5164530)
5164530
5157890
5156862
Reveleris® C18 HPLC Columns Reveleris® C18 HPLC Columns* Description
C18 HPLC Column C18 HPLC Column C18 HPLC Column
Size
Qty.
Part No.
4.6 x 50mm 4.6 x 150mm 4.6 x 250mm
3 3 3
5156381 5156382 5156383
&OR¬USE¬WITH¬2EVELERIS®¬.AVIGATOR™¬3OFTWARE
www.discoverysciences.com
35
flash & tlc
TLC Plates Analtech Uniplates™ TLC Plates
Adsorbosil® Soft Layer TLC Plates s¬#ONTAINS¬NO¬ORGANIC¬BINDERS s¬3AMPLE¬ZONES¬ARE¬EASY¬TO¬REMOVE¬FOR¬FURTHER¬ANALYSIS Soft Layer Adsorbosil® Prekotes TLC Plates Description
Size
Soft Layer Prekotes, Glass-Backed Conventional Adsorbosil®-Plus 20 x 20cm Adsorbosil®-Plus P* 20 x 20cm Adsorbosil®-Plus 1 20 x 20cm Adsorbosil®-Plus 1 P* 20 x 20cm
Layer Thickness
Qty.
Part No.
250μm 250μm 250μm 250μm
25 25 25 25
16384 16376 16330 16322
0¬ ¬7ITH¬&LUORESCENT¬)NDICATOR ¬¬WAVELENGTH
Silica Gel H and HF Uniplates™ TLC Plates s¬3OFT¬,AYER n¬#ONTAINS¬NO¬ORGANIC¬BINDER n¬#ONTAINS¬NO¬CALCUIM¬SULFATE¬BINDER s¬(ARD¬,AYER n¬#ONTAINS¬AN¬ORGANIC¬BINDER n¬¬WATER¬RESISTANT n¬6ISUALIZATION¬BY¬CHARRING¬UP¬TO¬# Silica Gel H and HF Uniplates™ TLC Plates
tlc
Description
Macherey-Nagel TLC Plates s¬±¬PORE¬SIZE ¬¬TO¬«M¬PARTICLE¬SIZE s¬"INDER¬IS¬ORGANIC ¬STABLE¬IN¬MOST¬ORGANIC¬SOLVENTS¬AND¬ AGGRESSIVE¬DETECTION¬REAGENTS
Soft Layer, No Binders Conventional 20 x 20cm 10 x 20cm Hard Layer, Organic Binder Conventional 20 x 20cm 10 x 20cm
Layer Thickness
Qty.
H Part No.
HF* Part No.
250μm 250μm
25 25
710011 710021
720011 7200210
250μm 250μm
25 25
746011 746021
747011 747021
& &LUORESCENT¬)NDICATOR ¬NM
Macherey-Nagel TLC Plates Description
Size
Silica Gel Plates, Glass-Backed Conventional Layers, Silica Gel 60 SIL G-25 5 x 10cm SIL G-25 5 x 20cm SIL G-25 20 x 20cm SIL G-25 UV254 5 x 20cm SIL G-25 UV254 20 x 20cm SIL G-25 UV254+366 20 x 20cm Polyester-Backed TLC Plates Silica Gel 60 SIL G 20 x 20cm SIL G/UV254 4 x 8cm SIL G/UV 254 20 x 20cm SIL N-HR/UV254 20 x 20cm
36
Layer Thickness
Qty.
Part No.
250μm 250μm 250μm 250μm 250μm 250μm
50 100 25 100 25 25
809017 809011 809013 809021 809023 809123
Silica Gel G and GF Uniplates™ TLC Plates s¬#ALCIUM¬3ULFATE¬"INDER s¬#ONTAINS¬NO¬ORGANIC¬BINDER Silica Gel G and GF Uniplates™ TLC Plates Description
250μm 250μm 250μm 200μm
25 50 25 25
805013 805021 805023 804023
Soft Layer, No Binders Conventional 20 x 20cm 10 x 20cm
Layer Thickness
Qty.
G Part No.
GF* Part No.
250μm 250μm
25 25
701011 701021
702011 702021
& &LUORESCENT¬)NDICATOR ¬NM
more info
technical assistance
For additional information about flash chromatography, including application notes and technical posters, visit our website.
Contact Tech Support: Email: [email protected] Online: www.discoverysciences.com
flash & tlc
TLC Accessories TLC Plate Cutter
TLC Tanks and Storage
s¬3CORES¬COATED¬GLASS¬PLATES¬AT¬ ANY¬POSITION s¬#OMPACT ¬PORTABLE ¬AND¬EASY¬ TO¬OPERATE
Latch-Lid TLC Tank s¬5NIQUE¬LATCHING¬DEVICE¬ASSURES¬TIGHT¬¬ SEAL¬BETWEEN¬LID¬AND¬TANK s¬.O¬MESSY¬GREASE¬SEALS
Latch-Lid Tank Description
Latch-Lid Tank/Lid Unit Latch-Lid Tank/Lid Unit
Size
Part No.
10 x 10cm Plates 20 x 20cm Plates
7542 7536
Multiple Plate Development Rack
The TLC plate cutter has a high-quality carbide scriber mounted into a movable plastic head. It is designed to produce optimal scoring on the glass surface of 20 x 20cm TLC plates with a total thickness (glass + coating) of 2mm. A smaller template is included with the unit for ease in cutting 10 x 10cm plates. TLC Plate Cutter
s¬3AVES¬TIME¬AND¬MONEY
Qty.
Part No.
TLC Plate Cutter Replacement Scribers Replacement Scribers
ea ea 3
7535 7565 7575
tlc
Description
Multiple Plate Development Rack Description
Anodized Aluminum Rack Anodized Aluminum Rack
Size
Part No.
20 x 20cm Plates 10 x 10cm Plates
17051 17053
Sample Applicators Uncalibrated Disposable Micropipettes Uncalibrated disposable glass micropipettes are intended for rapid qualitative sample application on TLC plates. Thick walls make these pipettes strong and easy to handle. Overall length is about three inches. Capacity is approximately 2–8μL.
Preval® Sprayers Compressed Gas Sprayer Compressed Gas Sprayers provide a constant pressure and uniform distribution of fine mist on your TLC plate. The pressure unit contains difluoroethane. Unit sprays up to 16oz of liquid. Caution: Wetted parts are made of polypropylene or nylon. Do not store with dip tube immersed in reagent.
Uncalibrated Disposable Micropipettes Description
Glass Micropipettes Glass Micropipettes
Complete Spray Unit with Glass Jar Replacement Glass Jar with Lid Replacement Compressed Gas Unit
Part No.
7616 17203
Qty.
Part No.
100
3842
Drummond® Wiretrol® Micropipettes
Compressed Gas Sprayer Description
Qty.
300 1440
Qty.
Part No.
3 6 6
14654 14655 14657
Spraying Accessories
s¬#OMBINES¬THE¬ACCURACY¬OF ¬A¬ MICROSYRINGE¬WITH¬THE¬EASE¬AND¬ ECONOMY¬OF ¬A¬DISPOSABLE¬PIPETTE
Drummond® Wiretrol® Micropipettes Description/Capacity
Disposable Spray Box
1.0 to 5.0μL (Calibrated)
s¬(EAVY¬DUTY¬CARDBOARD¬WITH¬DISPOSAL¬ BAG¬PROVIDED
TLC Spray Supports Description
Disposable Spray Box
Qty.
Part No.
5
16408
www.discoverysciences.com
37
