Microbac Laboratories, Inc., New York Division
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Jefferson-Lewis-Hamilton-Herkimer-Oneida BOCES
Project Name: J. Boak
Fred Hauck 20104 NYS Route 3 Watertown, NY 13601
Project / PO Number: N/A Received: 10/28/2016 12:00 Reported: 12/15/2016 11:57 [TOC_1]Analytical Sample Results[TOC]
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-01[TOC]
1 J6K0410-01 Grab
Collection Date: Collection Time:
10/28/16 05:40
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00530
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2209
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-02[TOC]
8 J6K0410-02 Grab
Collection Date: Collection Time:
10/28/16 05:48
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
0.0319
0.0150
0.00100
mg/L
G
12/06/16 1741
12/07/16 2209
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-03[TOC]
6B J6K0410-03 Grab
Collection Date: Collection Time:
10/28/16 05:42
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.0102
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2210
Method: EPA 200.8 Rev 5.4
Lead
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 1 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-04[TOC]
60 J6K0410-04 Grab
Collection Date: Collection Time:
10/28/16 05:42
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.0133
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2211
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-05[TOC]
7 J6K0410-05 Grab
Collection Date: Collection Time:
10/28/16 05:46
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
1.69
0.0150
0.00100
mg/L
GE
12/06/16 1741
12/07/16 2211
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-06[TOC]
10 J6K0410-06 Grab
Collection Date: Collection Time:
10/28/16 05:47
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.0118
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2212
Method: EPA 200.8 Rev 5.4
Lead
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 2 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-07[TOC]
9 J6K0410-07 Grab
Collection Date: Collection Time:
10/28/16 05:47
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
0.0166
0.0150
0.00100
mg/L
G
12/06/16 1741
12/07/16 2213
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-08[TOC]
4C J6K0410-08 Grab
Collection Date: Collection Time:
10/28/16 05:41
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00588
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2215
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-09[TOC]
40 J6K0410-09 Grab
Collection Date: Collection Time:
10/28/16 05:41
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.0144
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2215
Method: EPA 200.8 Rev 5.4
Lead
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 3 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-10[TOC]
4A J6K0410-10 Grab
Collection Date: Collection Time:
10/28/16 05:41
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00557
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2216
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-11[TOC]
4B J6K0410-11 Grab
Collection Date: Collection Time:
10/28/16 05:41
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00345
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2217
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-12[TOC]
3 J6K0410-12 Grab
Collection Date: Collection Time:
10/28/16 05:44
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
0.0217
0.0150
0.00100
mg/L
G
12/06/16 1741
12/07/16 2219
Method: EPA 200.8 Rev 5.4
Lead
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 4 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-13[TOC]
5 J6K0410-13 Grab
Collection Date: Collection Time:
10/28/16 05:42
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00307
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2219
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-14[TOC]
2 J6K0410-14 Grab
Collection Date: Collection Time:
10/28/16 05:44
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
0.181
0.0150
0.00100
mg/L
GE
12/06/16 1741
12/07/16 2220
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-15[TOC]
6C J6K0410-15 Grab
Collection Date: Collection Time:
10/28/16 05:42
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00735
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2221
Method: EPA 200.8 Rev 5.4
Lead
Laboratory NY:
Microbac Laboratories, Inc., New York Division
[TOC_1]Notes and Definitions[TOC]
Definitions AL: E: RL: G:
Action Level Estimated result Reporting Limit Result fails applicable NYS drinking water standards
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 5 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Cooler Receipt Log Cooler ID:
[TOC_1]Cooler Receipt[TOC] Default Cooler
Temp:
ºC
Cooler Inspection Checklist Custody Seals Intact and/or No Evidence of Tampering COC/Labels Agree Received on Ice (or not required)
Yes Yes Yes
Containers Intact Preservation Correct (or not required)
Yes Yes
Project Requested Certification(s) Microbac Laboratories, Inc., New York Division NY Lab ID No.: 10795 Microbac Laboratories, Inc. - Chicagoland NY Lab ID No: 12006 PA DEP ID: 68-04863
New York State Department of Health New York State Department of Health Pennsylvania Department of Environmental Protection
Report Comments
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted.
Michael Fifield
Go Green: Contact Michael Fifield to set up email reporting and invoicing options.
Division Manager 12/15/2016 11:57
The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are present and an authorized signature is included. For any feedback concerning our services, please contact Michael Fifield, Project Manager at [email protected]. You may also contact Michael Fifield, Managing Director at [email protected] or Robert Crookston, President at [email protected].
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 6 of 8
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Project Name: J. Boak
Fred Hauck 20104 NYS Route 3 Watertown, NY 13601
Project / PO Number: N/A Received: 10/28/2016 12:00 Reported: 12/15/2016 11:57 [TOC_1]Analytical Sample Results[TOC]
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-01[TOC]
1 J6K0410-01 Grab
Collection Date: Collection Time:
10/28/16 05:40
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00530
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2209
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-02[TOC]
8 J6K0410-02 Grab
Collection Date: Collection Time:
10/28/16 05:48
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
0.0319
0.0150
0.00100
mg/L
G
12/06/16 1741
12/07/16 2209
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-03[TOC]
6B J6K0410-03 Grab
Collection Date: Collection Time:
10/28/16 05:42
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.0102
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2210
Method: EPA 200.8 Rev 5.4
Lead
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 1 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-04[TOC]
60 J6K0410-04 Grab
Collection Date: Collection Time:
10/28/16 05:42
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.0133
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2211
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-05[TOC]
7 J6K0410-05 Grab
Collection Date: Collection Time:
10/28/16 05:46
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
1.69
0.0150
0.00100
mg/L
GE
12/06/16 1741
12/07/16 2211
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-06[TOC]
10 J6K0410-06 Grab
Collection Date: Collection Time:
10/28/16 05:47
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.0118
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2212
Method: EPA 200.8 Rev 5.4
Lead
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 2 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-07[TOC]
9 J6K0410-07 Grab
Collection Date: Collection Time:
10/28/16 05:47
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
0.0166
0.0150
0.00100
mg/L
G
12/06/16 1741
12/07/16 2213
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-08[TOC]
4C J6K0410-08 Grab
Collection Date: Collection Time:
10/28/16 05:41
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00588
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2215
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-09[TOC]
40 J6K0410-09 Grab
Collection Date: Collection Time:
10/28/16 05:41
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.0144
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2215
Method: EPA 200.8 Rev 5.4
Lead
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 3 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-10[TOC]
4A J6K0410-10 Grab
Collection Date: Collection Time:
10/28/16 05:41
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00557
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2216
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-11[TOC]
4B J6K0410-11 Grab
Collection Date: Collection Time:
10/28/16 05:41
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00345
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2217
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-12[TOC]
3 J6K0410-12 Grab
Collection Date: Collection Time:
10/28/16 05:44
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
0.0217
0.0150
0.00100
mg/L
G
12/06/16 1741
12/07/16 2219
Method: EPA 200.8 Rev 5.4
Lead
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 4 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-13[TOC]
5 J6K0410-13 Grab
Collection Date: Collection Time:
10/28/16 05:42
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00307
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2219
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-14[TOC]
2 J6K0410-14 Grab
Collection Date: Collection Time:
10/28/16 05:44
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
Note
Prepared
Analyzed
0.181
0.0150
0.00100
mg/L
GE
12/06/16 1741
12/07/16 2220
Method: EPA 200.8 Rev 5.4
Lead
Analytical Testing Parameters Client Sample ID: Lab Sample ID: Sample Type:
[TOC_1]Results - J6K0410-15[TOC]
6C J6K0410-15 Grab
Collection Date: Collection Time:
10/28/16 05:42
Analyses Subcontracted to: Microbac Laboratories, Inc. - Chicagoland Metals
Result
Limit
PQL
Units
0.00735
0.0150
0.00100
mg/L
Note
Prepared
Analyzed
12/06/16 1741
12/07/16 2221
Method: EPA 200.8 Rev 5.4
Lead
Laboratory NY:
Microbac Laboratories, Inc., New York Division
[TOC_1]Notes and Definitions[TOC]
Definitions AL: E: RL: G:
Action Level Estimated result Reporting Limit Result fails applicable NYS drinking water standards
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
Page 5 of 8
Microbac Laboratories, Inc., New York Division CERTIFICATE OF ANALYSIS J6K0410 Cooler Receipt Log Cooler ID:
[TOC_1]Cooler Receipt[TOC] Default Cooler
Temp:
ºC
Cooler Inspection Checklist Custody Seals Intact and/or No Evidence of Tampering COC/Labels Agree Received on Ice (or not required)
Yes Yes Yes
Containers Intact Preservation Correct (or not required)
Yes Yes
Project Requested Certification(s) Microbac Laboratories, Inc., New York Division NY Lab ID No.: 10795 Microbac Laboratories, Inc. - Chicagoland NY Lab ID No: 12006 PA DEP ID: 68-04863
New York State Department of Health New York State Department of Health Pennsylvania Department of Environmental Protection
Report Comments
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted.
Michael Fifield
Go Green: Contact Michael Fifield to set up email reporting and invoicing options.
Division Manager 12/15/2016 11:57
The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are present and an authorized signature is included. For any feedback concerning our services, please contact Michael Fifield, Project Manager at [email protected]. You may also contact Michael Fifield, Managing Director at [email protected] or Robert Crookston, President at [email protected].
Microbac Laboratories, Inc. 3821 Buck Dr. | Cortland, NY 13045 | 607-753-3403 p | www.microbac.com
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