supplemental information for bidders
SUPPLEMENTAL INFORMATION FOR BIDDERS
SUMMARY OF GROUNDWATER ELEVATION DATA (GOLDER, NOVEMBER 7, 2011)
SUMMARY OF SEDIMENT AND WASTEWATER SAMPLING METAL CLEANING WASTE BASINS AND OILY WASTE COLLECTION BASINS (GOLDER, JUNE 23, 2011)
June 23, 2011
113-82520
Mr. Alan Ehrle St Johns River Power Park 11201 New Berlin Road Jacksonville, FL 32226 RE:
RESULTS OF SEDIMENT AND WASTEWATER SAMPLING OILY WASTE AND METAL CLEANING WASTE BASINS ST. JOHNS RIVER POWER PARK JACKSONVILLE, FLORIDA
Dear Mr. Ehrle: Golder Associates Inc. (Golder) is pleased to provide St. Johns River Power Park (SJRPP) with the results of the recent sampling of sediment and wastewater in the Oily Waste and the Metal Cleaning Waste Basins. A bid document for the re-lining of these basins is being prepared and the sampling was performed to provide SJRPP with sediment and wastewater quality data for the basins such that SJRPP can better direct bidders as to the handling and disposal requirements for these materials.
FIELD SAMPLING On June 3, 2011, a representative from Golder collected grab samples of sediment from the northern (primary) Oily Waste Basin (sample designated OWCB-P) and the east and west Metal Cleaning Waste Basins (samples designated MCWB-E and MCWB-W)). In addition, a wastewater sample was collected from the northern (primary) Oily Waste Basin. Approximate sample locations are shown on Figure 1.
ANALYTICAL TESTING Samples were sent to TestAmerica Tallahassee for analysis of the following parameters:
Sediment – TCLP Appendix I volatiles and metals
Wastewater – Total Dissolved Solids (TDS), Total Suspended Solids (TSS), pH, turbidity, specific gravity, oil & grease, and residual chlorine.
RESULTS For the parameters analyzed, the TCLP testing of the sediment grab samples did not detect any constituents above the limits established by 40 CFR 261.24. For comparison purposes only, the TCLP results were also compared to Florida Groundwater standards under Chapter 62-777, FAC (see Table 1). The TCLP results were higher than Florida Groundwater standards for several metals including arsenic, nickel, selenium, and vanadium. For the parameters analyzed, the wastewater grab sample collected from the northern (primary) Oily Waste Basin exceeded JEA pretreatment standards for oil and grease. It is noted that these standards are not directly applicable as SJRPP has its own treatment plant and are provided for comparison purposes only.
CONCLUSIONS The results of the sediment sampling indicated that, for the parameters analyzed, those materials did not exceed any of the standards established under 40 CFR 261.24. As such, those materials could be handled and disposed of as non-hazardous. While the sediment from the Oily Waste basin did not report Golder Associates Inc. 9428 Baymeadows Road, Suite 400 Jacksonville, FL 32256 USA Tel: (904) 363-3430 Fax: (904) 363-3445 www.golder.com Golder Associates: Operations in Africa, Asia, Australasia, Europe, North America and South America
Mr. Alan Ehrle St. Johns River Power Park
2
June 23, 2011 113-82520
much in the volatile scan, it is noted that the wastewater sample detected high levels of oil and grease and it is possible that the sediment could also contain high levels of oil and grease.
CLOSING Golder appreciates the opportunity to provide these services to SJRPP. Please feel free to contact us with any questions or comments concerning this report. Sincerely, GOLDER ASSOCIATES INC.
Samuel F. Stafford Staff Engineer
Kenneth B. Karably, PE, PG Principal Attachment:
Table 1 – Summary of Detections, Sediment TCLP Analyses Table 2 – Summary of Detections, Wastewater Sample Figure 1 – Sample Location Plan Attachment A – TestAmerica Report (6/15/2011)
FN: G:\Projects\113\113-82\113-82520\200 Draft Rpts\SJRPP - OWB and MWCB Sampling (06.23.2011).docx
SJRPP - OWB and MWCB Sampling (06.23.2011).docx
June 2011
113-82520
TABLE 1 SUMMARY OF DETECTIONS - SEDIMENT TCLP ANALYSES OILY WASTE COLLECTION AND METAL CLEANING WASTE BASINS ST. JOHNS RIVER POWER PARK - JACKSONVILLE, FLORIDA
Standard SAMPLE GCTL LOCATION D-LIST MCWB-W MCWB-E OWCB-P
Arsenic 0.010 5 0.050 U 0.050 U 0.058 I
Barium 2 100 0.59 I 0.73 I 0.50 U
Copper 1 NL 0.29 I 0.12 I 0.050 U
Nickel 0.1 NL 0.16 I 0.10 U 0.18 I
Selenium Vanadium 0.05 0.049 1.0 NL 0.070 I 0.050 U 0.050 U 0.050 U 0.050 U 0.070 I
Zinc 5 NL 0.95 I 0.74 I 2.4 I
2-Butanone 4.2 200 0.21 I 0.14 I 0.16 I
NOTES: Pond sediment samples collected by Golder on 6/3/2011 and analyzed by TestAmerica TCLP = Toxicity Characteristic Leaching Procedure All concentrations listed in milligrams per liter (mg/L) GCTL = Groundwater Cleanup Target Level per Ch. 62-777, FAC. D-List = Maximum Concentration of Contaminants for Toxicity Characteristic per 40 CFR 261.24 NL = Compound was not listed in standard MCWB = Metal Cleaning Waste Basin OWCB = Oily Waste Collection Basin U = Indicates that the compound was analyzed for but not detected I = The reported value is between the laboratory method detection limit and laboratory practical quantitation limit
Checked by: SFS Reviewed by: KBK
G:\Projects\113\113-82\113-82520\200 Draft Rpts\202 - Sampling Report\Basin Sampling Results.xlsx\Table 1
Golder Associates
June 2011
113-82520
TABLE 2 SUMMARY OF DETECTIONS - WASTEWATER SAMPLE OILY WASTE COLLECTION BASIN ST. JOHNS RIVER POWER PARK - JACKSONVILLE, FLORIDA
Standard SAMPLE JEA LOCATION OWCB-P
HEM 100 19,000
Turbidity NL 420
TDS NL 12,000
TSS NL 1,300
Chlorine NL 0.42
pH 5.5-12.0 6.72
NOTES: Basin wastewater sample collected by Golder on 6/3/2011 and analyzed by TestAmerica All concentrations listed in milligrams per liter (mg/L), except Turbidty (NTU) and pH (SU). OWCB = Oily Waste Collection Basin HEM = n-hexane extractable material (Oil and Grease) JEA = JEA Industrial Pretreatment Regulation
Checked by: SFS Reviewed by: KBK
G:\Projects\113\113-82\113-82520\200 Draft Rpts\202 - Sampling Report\Basin Sampling Results.xlsx\Table 2
Golder Associates
1 2 3 4 5
ANALYTICAL REPORT
6
TestAmerica Laboratories, Inc. TestAmerica Tallahassee 2846 Industrial Plaza Drive Tallahassee, FL 32301 Tel: (850)878-3994
7 8 9
TestAmerica Job ID: 640-33835-1 Client Project/Site: St. Johns Power Park
10
For: Golder Associates Inc. 9428 Baymeadows Road Suite 400 Jacksonville, Florida 32256
11 12 13
Attn: Mr. Kenneth Karably
Authorized for release by: 06/15/2011 04:23:05 PM Chad Bechtold Project Manager II [email protected]
Results relate only to the items tested and the sample(s) as received by the laboratory. The test results in this report meet all 2003 NELAC requirements for accredited parameters, exceptions are noted in this report. Pursuant to NELAC, this report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Page 1 of 32
06/15/2011
Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Table of Contents Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
3
1 2 3 4 5 6 13 24 27 29 30 31 32
4 5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 2 of 32
06/15/2011
Definitions/Glossary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Qualifiers
3
GC/MS VOA Qualifier
Qualifier Description
I
The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
J
Estimated value; value may not be accurate.
U
Indicates that the compound was analyzed for but not detected.
4 5 6
Metals Qualifier
Qualifier Description
I
The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
U
Indicates that the compound was analyzed for but not detected.
7 8
General Chemistry Qualifier
Qualifier Description
Q
Sample held beyond the accepted holding time.
U
Indicates that the compound was analyzed for but not detected.
9 10
Glossary Abbreviation
These commonly used abbreviations may or may not be present in this report.
☼
Listed under the "D" column to designate that the result is reported on a dry weight basis.
EPA
United States Environmental Protection Agency
ND
Not Detected above the reporting level.
MDL
Method Detection Limit
RL
Reporting Limit
RE, RE1 (etc.)
Indicates a Re-extraction or Reanalysis of the sample.
%R
Percent Recovery
RPD
Relative Percent Difference, a measure of the relative difference between two points.
11 12 13
TestAmerica Tallahassee
Page 3 of 32
06/15/2011
Case Narrative Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Job ID: 640-33835-1
3
Laboratory: TestAmerica Tallahassee
4
Narrative
Job Narrative 640-33835-1
5 6
Comments No additional comments.
7
Receipt All samples were received in good condition within temperature requirements.
8
GC/MS VOA Method 8260C: The laboratory control sample recovery for Bromoform was outside control limits. This compound, qualified with a "J", was not detected in the associated samples. The matrix spike (MS) and / or matrix spike duplicate (MSD) recoveries for Acrylonitrile, Bromomethane, and Chloromethane were outside control limits.
10
No other analytical or quality issues were noted.
11
Metals No analytical or quality issues were noted.
12
9
13
General Chemistry Method SM4500 Cl G: Residual Chlorine analysis should be performed in the field within 15 minutes of collection. The sample results have been qualified with a "Q".
Method SM4500 H+ B: pH analysis should be performed in the field within 15 minutes of collection. The sample results have been qualified with a "Q". No other analytical or quality issues were noted. VOA Prep No analytical or quality issues were noted.
TestAmerica Tallahassee
Page 4 of 32
06/15/2011
Detection Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-W
Lab Sample ID: 640-33835-1
Analyte
2 Result Qualifier
PQL
MDL Unit
Dil Fac D Method
0.21 I
1.0
0.10 mg/L
100
8260C
TCLP
Barium
0.59 I
0.80
0.50 mg/L
1
6010C
TCLP
Copper
0.29 I
0.50
0.050 mg/L
1
6010C
TCLP
Nickel
0.16 I
2.5
0.10 mg/L
1
6010C
TCLP
0.070 I
0.25
0.050 mg/L
1
6010C
TCLP
0.95 I
2.5
0.10 mg/L
1
6010C
TCLP
Zinc
Client Sample ID: MCWB-E Analyte
Lab Sample ID: 640-33835-2 Result Qualifier
PQL
MDL Unit
Dil Fac D Method
Prep Type
2-Butanone (MEK)
0.14 I
1.0
0.10 mg/L
100
8260C
TCLP
Barium
0.73 I
0.80
0.50 mg/L
1
6010C
TCLP
Copper
0.12 I
0.50
0.050 mg/L
1
6010C
TCLP
Zinc
0.74 I
2.5
0.10 mg/L
1
6010C
TCLP
Client Sample ID: OWCB-P Analyte
2-Butanone (MEK) Arsenic Nickel Vanadium Zinc
Lab Sample ID: 640-33835-3 Result Qualifier
PQL
MDL Unit
Dil Fac D Method
Prep Type
0.16 I
1.0
0.10 mg/L
100
8260C
TCLP
0.058 I
0.25
0.050 mg/L
1
6010C
TCLP
0.18 I
2.5
0.10 mg/L
1
6010C
TCLP
0.070 I
0.25
0.050 mg/L
1
6010C
TCLP
2.4 I
2.5
0.10 mg/L
1
6010C
TCLP
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-4 PQL
MDL Unit
Analyte
Result Qualifier
HEM (Oil & Grease)
19000
5.3
3.5 mg/L
1
1664A
Total/NA
420
8.0
8.0 NTU
16
180.1
Total/NA
12000
100
46 mg/L
1
SM 2540C
Total/NA
1300
2.5
1.4 mg/L
1
SM 2540D
Total/NA
1
SM 2710F
Total/NA
Turbidity Total Dissolved Solids Total Suspended Solids Specific Gravity
1.0008
NONE
Dil Fac D Method
Prep Type
Chlorine, Total Residual
0.42 Q
0.10
0.043 mg/L
1
SM 4500 Cl G
Total/NA
pH
6.72 Q
1.00
1.00 SU
1
SM 4500 H+ B
Total/NA
TestAmerica Tallahassee
Page 5 of 32
3
Prep Type
2-Butanone (MEK)
Selenium
1
06/15/2011
4 5 6 7 8 9 10 11 12 13
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-W
Lab Sample ID: 640-33835-1
1 2
Date Collected: 06/03/11 13:30 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 8260C - Volatile Organic Compounds by GC/MS - TCLP Analyte
PQL
MDL Unit
1,1,1,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1,1-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1,2-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1,2,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,2,3-Trichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,2-Dibromo-3-Chloropropane
0.10 U
0.50
0.10 mg/L
06/09/11 16:24
100
1,2-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,2-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,2-Dichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,4-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
2-Hexanone
0.10 U
1.0
0.10 mg/L
06/09/11 16:24
100
Acrylonitrile
0.10 U
1.0
0.10 mg/L
06/09/11 16:24
100
Acetone
0.46 U
2.5
0.46 mg/L
06/09/11 16:24
100
Benzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Bromoform
0.10 U J
0.10
0.10 mg/L
06/09/11 16:24
100
Bromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Carbon disulfide
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Carbon tetrachloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chlorodibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
cis-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
cis-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chloroform
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chloromethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Dibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Dichlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Ethylbenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Ethylene Dibromide
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Iodomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
m-Xylene & p-Xylene
0.10 U
0.20
0.10 mg/L
06/09/11 16:24
100
2-Butanone (MEK)
0.21 I
1.0
0.10 mg/L
06/09/11 16:24
100
Methylene Chloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
4-Methyl-2-pentanone (MIBK)
0.10 U
1.0
0.10 mg/L
06/09/11 16:24
100
o-Xylene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Styrene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Tetrachloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Toluene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
trans-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
trans-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
trans-1,4-Dichloro-2-butene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Trichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Trichlorofluoromethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Vinyl acetate
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Vinyl chloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Xylenes, Total
0.10 U
0.30
0.10 mg/L
06/09/11 16:24
100
Result Qualifier
D
Prepared
Analyzed
Dil Fac
TestAmerica Tallahassee
Page 6 of 32
06/15/2011
5 6 7 8 9 10 11 12 13
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-W
Lab Sample ID: 640-33835-1
1 2
Date Collected: 06/03/11 13:30 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 6010C - Metals (ICP) - TCLP Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Arsenic
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Barium
0.59 I
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 10:45
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 10:45
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Copper
0.29 I
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Nickel
0.16 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:45
1
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Selenium
0.070 I
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Vanadium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
0.95 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:45
1
Lead
Zinc
Result Qualifier
D
Dil Fac
5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 7 of 32
06/15/2011
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-E
Lab Sample ID: 640-33835-2
1 2
Date Collected: 06/03/11 13:50 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 8260C - Volatile Organic Compounds by GC/MS - TCLP Analyte
PQL
MDL Unit
1,1,1,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1,1-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1,2-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1,2,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,2,3-Trichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,2-Dibromo-3-Chloropropane
0.10 U
0.50
0.10 mg/L
06/09/11 16:48
100
1,2-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,2-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,2-Dichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,4-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
2-Hexanone
0.10 U
1.0
0.10 mg/L
06/09/11 16:48
100
Acrylonitrile
0.10 U
1.0
0.10 mg/L
06/09/11 16:48
100
Acetone
0.46 U
2.5
0.46 mg/L
06/09/11 16:48
100
Benzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Bromoform
0.10 U J
0.10
0.10 mg/L
06/09/11 16:48
100
Bromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Carbon disulfide
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Carbon tetrachloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chlorodibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
cis-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
cis-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chloroform
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chloromethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Dibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Dichlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Ethylbenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Ethylene Dibromide
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Iodomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
m-Xylene & p-Xylene
0.10 U
0.20
0.10 mg/L
06/09/11 16:48
100
2-Butanone (MEK)
0.14 I
1.0
0.10 mg/L
06/09/11 16:48
100
Methylene Chloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
4-Methyl-2-pentanone (MIBK)
0.10 U
1.0
0.10 mg/L
06/09/11 16:48
100
o-Xylene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Styrene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Tetrachloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Toluene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
trans-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
trans-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
trans-1,4-Dichloro-2-butene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Trichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Trichlorofluoromethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Vinyl acetate
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Vinyl chloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Xylenes, Total
0.10 U
0.30
0.10 mg/L
06/09/11 16:48
100
Result Qualifier
D
Prepared
Analyzed
Dil Fac
TestAmerica Tallahassee
Page 8 of 32
06/15/2011
5 6 7 8 9 10 11 12 13
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-E
Lab Sample ID: 640-33835-2
1 2
Date Collected: 06/03/11 13:50 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 6010C - Metals (ICP) - TCLP Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Arsenic
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Barium
0.73 I
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 10:52
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 10:52
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Copper
0.12 I
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Nickel
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:52
1
Lead
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Selenium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Vanadium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
0.74 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:52
1
Zinc
Result Qualifier
D
Dil Fac
5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 9 of 32
06/15/2011
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-3
1 2
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 8260C - Volatile Organic Compounds by GC/MS - TCLP Analyte
PQL
MDL Unit
1,1,1,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1,1-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1,2-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1,2,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,2,3-Trichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,2-Dibromo-3-Chloropropane
0.10 U
0.50
0.10 mg/L
06/09/11 17:13
100
1,2-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,2-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,2-Dichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,4-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
2-Hexanone
0.10 U
1.0
0.10 mg/L
06/09/11 17:13
100
Acrylonitrile
0.10 U
1.0
0.10 mg/L
06/09/11 17:13
100
Acetone
0.46 U
2.5
0.46 mg/L
06/09/11 17:13
100
Benzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Bromoform
0.10 U J
0.10
0.10 mg/L
06/09/11 17:13
100
Bromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Carbon disulfide
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Carbon tetrachloride
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chlorodibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
cis-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
cis-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chloroform
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chloromethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Dibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Dichlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Ethylbenzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Ethylene Dibromide
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Iodomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
m-Xylene & p-Xylene
0.10 U
0.20
0.10 mg/L
06/09/11 17:13
100
2-Butanone (MEK)
0.16 I
1.0
0.10 mg/L
06/09/11 17:13
100
Methylene Chloride
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
4-Methyl-2-pentanone (MIBK)
0.10 U
1.0
0.10 mg/L
06/09/11 17:13
100
o-Xylene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Styrene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Tetrachloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Toluene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
trans-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
trans-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
trans-1,4-Dichloro-2-butene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Trichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Trichlorofluoromethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Vinyl acetate
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Vinyl chloride
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Xylenes, Total
0.10 U
0.30
0.10 mg/L
06/09/11 17:13
100
Result Qualifier
D
Prepared
Analyzed
Dil Fac
TestAmerica Tallahassee
Page 10 of 32
06/15/2011
5 6 7 8 9 10 11 12 13
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-3
1 2
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 6010C - Metals (ICP) - TCLP Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Arsenic
0.058 I
Result Qualifier
D
Dil Fac
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
0.50 U
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 11:00
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 11:00
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Copper
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Nickel
0.18 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 11:00
1
Lead
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Selenium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Vanadium
0.070 I
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
2.4 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 11:00
1
Barium
Zinc
5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 11 of 32
06/15/2011
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-4
1 2
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Water
3 4
General Chemistry Analyte
Result Qualifier
HEM (Oil & Grease)
19000
Turbidity Total Dissolved Solids Total Suspended Solids Specific Gravity
PQL
MDL Unit
5.3
3.5 mg/L
D
Prepared
Analyzed
06/14/11 08:30
06/14/11 08:30
Dil Fac
1
420
8.0
8.0 NTU
06/05/11 12:45
16
12000
100
46 mg/L
06/07/11 10:15
1
1300
2.5
1.4 mg/L
06/07/11 10:09
1
06/08/11 12:10
1
NONE
1.0008
Chlorine, Total Residual
0.42 Q
0.10
0.043 mg/L
06/07/11 10:00
1
pH
6.72 Q
1.00
1.00 SU
06/06/11 14:00
1
5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 12 of 32
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Method: 8260C - Volatile Organic Compounds by GC/MS
3
Lab Sample ID: MB 700-101524/6 Matrix: Solid Analysis Batch: 101524
Client Sample ID: Method Blank Prep Type: Total/NA MB MB
Analyte
Result Qualifier
PQL
MDL Unit
1,1,1,2-Tetrachloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1,1-Trichloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1,2-Trichloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1,2,2-Tetrachloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1-Dichloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,2,3-Trichloropropane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1-Dichloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,2-Dibromo-3-Chloropropane
0.0010 U
0.0050
0.0010 mg/L
06/09/11 08:57
1
1,2-Dichlorobenzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,2-Dichloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,2-Dichloropropane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,4-Dichlorobenzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
2-Hexanone
0.0010 U
0.010
0.0010 mg/L
06/09/11 08:57
1
Acrylonitrile
0.0010 U
0.010
0.0010 mg/L
06/09/11 08:57
1
Acetone
0.0046 U
0.025
0.0046 mg/L
06/09/11 08:57
1
Benzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Bromoform
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Bromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Carbon disulfide
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Carbon tetrachloride
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chlorobenzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chlorobromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chlorodibromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
cis-1,2-Dichloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
cis-1,3-Dichloropropene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chloroform
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chloromethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Dibromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Dichlorobromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Ethylbenzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Ethylene Dibromide
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Iodomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
m-Xylene & p-Xylene
0.0010 U
0.0020
0.0010 mg/L
06/09/11 08:57
1
2-Butanone (MEK)
0.0010 U
0.010
0.0010 mg/L
06/09/11 08:57
1
Methylene Chloride
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
4-Methyl-2-pentanone (MIBK)
0.0010 U
0.010
0.0010 mg/L
06/09/11 08:57
1
o-Xylene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Styrene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Tetrachloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Toluene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
trans-1,2-Dichloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
trans-1,3-Dichloropropene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
trans-1,4-Dichloro-2-butene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Trichloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Trichlorofluoromethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Vinyl acetate
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Vinyl chloride
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Xylenes, Total
0.0010 U
0.0030
0.0010 mg/L
06/09/11 08:57
1
D
Prepared
Analyzed
Dil Fac
TestAmerica Tallahassee
Page 13 of 32
06/15/2011
4 5 6 7 8 9 10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)
3
Lab Sample ID: LCS 700-101524/3 Matrix: Solid Analysis Batch: 101524
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
LCS LCS
Added
Result Qualifier
Unit
1,1,1,2-Tetrachloroethane
0.0250
0.0209
mg/L
84
70 - 130
1,1,1-Trichloroethane
0.0250
0.0205
mg/L
82
70 - 130
1,1,2-Trichloroethane
0.0250
0.0240
mg/L
96
70 - 130
1,1,2,2-Tetrachloroethane
0.0250
0.0225
mg/L
90
70 - 130
1,1-Dichloroethane
0.0250
0.0276
mg/L
111
70 - 130
1,1-Dichloroethene
0.0250
0.0197
mg/L
79
56 - 146
1,2-Dichlorobenzene
0.0250
0.0235
mg/L
94
70 - 130
1,2-Dichloroethane
0.0250
0.0218
mg/L
87
67 - 136
1,2-Dichloropropane
0.0250
0.0246
mg/L
98
70 - 130
1,4-Dichlorobenzene
0.0250
0.0236
mg/L
95
70 - 130
0.100
0.0778
mg/L
78
50 - 150
Acetone
0.100
0.0926
mg/L
93
50 - 150
Benzene
0.0250
0.0252
mg/L
101
68 - 135
Bromoform
0.0250
0.0159 J
mg/L
63
64 - 131
Bromomethane
0.0250
0.0217
mg/L
87
50 - 130
Carbon disulfide
D
% Rec
Limits
0.100
0.0746
mg/L
75
50 - 150
Carbon tetrachloride
0.0250
0.0197
mg/L
79
50 - 135
Chlorobenzene
0.0250
0.0235
mg/L
94
71 - 132
Chlorobromomethane
0.0250
0.0248
mg/L
99
50 - 130
Chlorodibromomethane
0.0250
0.0214
mg/L
86
50 - 130
cis-1,2-Dichloroethene
0.0250
0.0235
mg/L
94
50 - 130
cis-1,3-Dichloropropene
0.0250
0.0208
mg/L
83
50 - 130
Chloroethane
0.0250
0.0173
mg/L
69
61 - 115
Chloroform
0.0250
0.0257
mg/L
103
64 - 131
Chloromethane
0.0250
0.0157
mg/L
63
63 - 125
Dibromomethane
0.0250
0.0230
mg/L
92
50 - 130
Dichlorobromomethane
0.0250
0.0230
mg/L
92
70 - 130
Ethylbenzene
0.0250
0.0238
mg/L
95
50 - 150
Ethylene Dibromide
0.0250
0.0230
mg/L
92
50 - 130
0.100
0.0994
mg/L
99
50 - 150
0.0500
0.0524
mg/L
105
70 - 130
2-Butanone (MEK)
0.100
0.0990
mg/L
99
45 - 139
Methylene Chloride
0.0250
0.0266
mg/L
107
70 - 130
0.100
0.0767
mg/L
77
50 - 150
o-Xylene
0.0250
0.0231
mg/L
93
70 - 130
Styrene
0.0250
0.0213
mg/L
85
70 - 130
Tetrachloroethene
0.0250
0.0224
mg/L
90
51 - 154
Toluene
0.0250
0.0247
mg/L
99
70 - 130
trans-1,2-Dichloroethene
0.0250
0.0269
mg/L
107
50 - 130
trans-1,3-Dichloropropene
0.0250
0.0186
mg/L
74
50 - 130
Trichloroethene
0.0250
0.0226
mg/L
91
67 - 132
Trichlorofluoromethane
0.0250
0.0147
mg/L
59
50 - 130
Vinyl acetate
0.100
0.0562
mg/L
56
50 - 150
Vinyl chloride
0.0250
0.0145
mg/L
58
55 - 142
Iodomethane m-Xylene & p-Xylene
4-Methyl-2-pentanone (MIBK)
6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 14 of 32
4 5
% Rec.
Analyte
2-Hexanone
1
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: LCSD 700-101524/4 Matrix: Solid Analysis Batch: 101524
3 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA
Spike
LCSD LCSD
% Rec.
Analyte
Added
Result Qualifier
Unit
1,1,1,2-Tetrachloroethane
0.0250
0.0216
mg/L
87
1,1,1-Trichloroethane
0.0250
0.0202
mg/L
81
1,1,2-Trichloroethane
0.0250
0.0250
mg/L
1,1,2,2-Tetrachloroethane
0.0250
0.0232
mg/L
1,1-Dichloroethane
0.0250
0.0281
1,1-Dichloroethene
0.0250
0.0198
1,2-Dichlorobenzene
0.0250
1,2-Dichloroethane
0.0250
1,2-Dichloropropane 1,4-Dichlorobenzene
Limit
70 - 130
3
30
70 - 130
1
30
100
70 - 130
4
30
93
70 - 130
3
30
mg/L
112
70 - 130
2
30
mg/L
79
56 - 146
0
30
0.0246
mg/L
99
70 - 130
5
30
0.0221
mg/L
88
67 - 136
1
23
0.0250
0.0257
mg/L
103
70 - 130
4
30
0.0250
0.0243
mg/L
97
70 - 130
3
30
0.100
0.0874
mg/L
87
50 - 150
12
30
Acetone
0.100
0.0957
mg/L
96
50 - 150
3
30
Benzene
0.0250
0.0252
mg/L
101
68 - 135
0
37
Bromoform
0.0250
0.0177
mg/L
71
64 - 131
11
30
Bromomethane
0.0250
0.0220
mg/L
88
50 - 130
1
30
Carbon disulfide
D
% Rec
Limits
RPD RPD
2-Hexanone
0.100
0.0771
mg/L
77
50 - 150
3
30
Carbon tetrachloride
0.0250
0.0194
mg/L
78
50 - 135
1
38
Chlorobenzene
0.0250
0.0228
mg/L
91
71 - 132
3
22
Chlorobromomethane
0.0250
0.0259
mg/L
104
50 - 130
4
30
Chlorodibromomethane
0.0250
0.0227
mg/L
91
50 - 130
6
30
cis-1,2-Dichloroethene
0.0250
0.0240
mg/L
96
50 - 130
2
30
cis-1,3-Dichloropropene
0.0250
0.0219
mg/L
87
50 - 130
5
30
Chloroethane
0.0250
0.0174
mg/L
69
61 - 115
1
30
Chloroform
0.0250
0.0266
mg/L
106
64 - 131
3
20
Chloromethane
0.0250
0.0159
mg/L
63
63 - 125
1
30
Dibromomethane
0.0250
0.0234
mg/L
93
50 - 130
2
30
Dichlorobromomethane
0.0250
0.0236
mg/L
95
70 - 130
3
30
Ethylbenzene
0.0250
0.0241
mg/L
96
50 - 150
1
30
Ethylene Dibromide
0.0250
0.0245
mg/L
98
50 - 130
6
30
0.100
0.105
mg/L
105
50 - 150
6
30
0.0500
0.0530
mg/L
106
70 - 130
1
30
2-Butanone (MEK)
0.100
0.108
mg/L
108
45 - 139
9
31
Methylene Chloride
0.0250
0.0281
mg/L
113
70 - 130
6
30
0.100
0.0786
mg/L
79
50 - 150
2
30
o-Xylene
0.0250
0.0237
mg/L
95
70 - 130
2
30
Styrene
0.0250
0.0221
mg/L
88
70 - 130
4
30
Tetrachloroethene
0.0250
0.0229
mg/L
91
51 - 154
2
24
Toluene
0.0250
0.0256
mg/L
102
70 - 130
3
30
trans-1,2-Dichloroethene
0.0250
0.0281
mg/L
112
50 - 130
4
30
trans-1,3-Dichloropropene
0.0250
0.0197
mg/L
79
50 - 130
6
30
Trichloroethene
0.0250
0.0236
mg/L
94
67 - 132
4
35
Trichlorofluoromethane
0.0250
0.0146
mg/L
58
50 - 130
1
30
Vinyl acetate
0.100
0.0606
mg/L
61
50 - 150
8
30
Vinyl chloride
0.0250
0.0143
mg/L
57
55 - 142
1
21
Iodomethane m-Xylene & p-Xylene
4-Methyl-2-pentanone (MIBK)
1
TestAmerica Tallahassee
Page 15 of 32
06/15/2011
4 5 6 7 8 9 10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)
3
Lab Sample ID: MRL 700-101524/5 MRL Matrix: Solid Analysis Batch: 101524
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Analyte
Added
MRL MRL Result Qualifier
D
% Rec
Limits
0.00100
0.00199 I
mg/L
199
1 - 150
Bromoform
0.00100
0.000750 I
mg/L
75
50 - 150
trans-1,2-Dichloroethene
0.00100
0.00139
mg/L
139
50 - 150
trans-1,4-Dichloro-2-butene
0.00100
0.000647 I
mg/L
65
1 - 150
Lab Sample ID: 640-33835-3 MS Matrix: Solid Analysis Batch: 101524
6 7
Client Sample ID: OWCB-P Prep Type: TCLP Sample Sample Result Qualifier
Spike Added
MS MS Result Qualifier
8 9
% Rec. Unit
1,1,1,2-Tetrachloroethane
0.10 U
2.50
2.37
mg/L
1,1,1-Trichloroethane
0.10 U
2.50
2.20
1,1,2-Trichloroethane
0.10 U
2.50
2.71
1,1,2,2-Tetrachloroethane
0.10 U
2.50
1,1-Dichloroethane
0.10 U
2.50
1,2,3-Trichloropropane
0.10 U
1,1-Dichloroethene
0.10 U
1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene
D
% Rec
10
Limits
95
70 - 130
mg/L
88
50 - 150
mg/L
108
50 - 130
2.68
mg/L
107
70 - 130
2.59
mg/L
104
50 - 130
2.50
2.03
mg/L
81
70 - 130
2.50
2.19
mg/L
87
56 - 146
0.10 U
2.50
2.06
mg/L
83
50 - 130
0.10 U
2.50
2.74
mg/L
110
70 - 130
1,2-Dichloroethane
0.10 U
2.50
2.62
mg/L
105
67 - 136
1,2-Dichloropropane
0.10 U
2.50
2.58
mg/L
103
70 - 130
1,4-Dichlorobenzene
0.10 U
2.50
2.61
mg/L
104
50 - 130
2-Hexanone
0.10 U
10.0
9.46
mg/L
95
50 - 130
Acrylonitrile
0.10 U
25.0
29.0
mg/L
116
70 - 130
Acetone
0.46 U
10.0
10.9
mg/L
109
70 - 130
Benzene
0.10 U
2.50
2.65
mg/L
106
68 - 135
Bromoform
0.10 U J
2.50
1.95
mg/L
78
64 - 131
Bromomethane
0.10 U
2.50
1.17 J
mg/L
47
70 - 130
Carbon disulfide
0.10 U
10.0
8.14
mg/L
81
50 - 150
Carbon tetrachloride
0.10 U
2.50
2.19
mg/L
88
50 - 150
Chlorobenzene
0.10 U
2.50
2.52
mg/L
101
71 - 132
Chlorobromomethane
0.10 U
2.50
2.49
mg/L
99
70 - 130
Chlorodibromomethane
0.10 U
2.50
2.39
mg/L
96
70 - 130
cis-1,2-Dichloroethene
0.10 U
2.50
2.14
mg/L
86
50 - 130
cis-1,3-Dichloropropene
0.10 U
2.50
1.98
mg/L
79
50 - 130
Chloroethane
0.10 U
2.50
1.91
mg/L
76
61 - 115
Chloroform
0.10 U
2.50
2.53
mg/L
101
64 - 131
Chloromethane
0.10 U
2.50
1.48 J
mg/L
59
63 - 125
Dibromomethane
0.10 U
2.50
2.57
mg/L
103
70 - 130
Dichlorobromomethane
0.10 U
2.50
2.53
mg/L
101
70 - 130
Ethylbenzene
0.10 U
2.50
2.58
mg/L
103
50 - 130
Ethylene Dibromide
0.10 U
2.50
2.61
mg/L
104
70 - 130
Iodomethane
0.10 U
10.0
9.74
mg/L
97
50 - 130
m-Xylene & p-Xylene
0.10 U
5.00
5.63
mg/L
113
70 - 130
2-Butanone (MEK)
0.16 I
10.0
10.5
mg/L
104
45 - 139
Methylene Chloride
0.10 U
2.50
2.61
mg/L
104
50 - 130
4-Methyl-2-pentanone (MIBK)
0.10 U
10.0
9.21
mg/L
92
50 - 150
o-Xylene
0.10 U
2.50
2.45
mg/L
98
70 - 130
Styrene
0.10 U
2.50
2.31
mg/L
92
50 - 130
Tetrachloroethene
0.10 U
2.50
2.33
mg/L
93
51 - 154
11 12 13
TestAmerica Tallahassee
Page 16 of 32
4 5
% Rec. Unit
1,2-Dibromo-3-Chloropropane
Analyte
1
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: 640-33835-3 MS Matrix: Solid Analysis Batch: 101524
Client Sample ID: OWCB-P Prep Type: TCLP Sample Sample
Analyte
Result Qualifier
Spike Added
MS MS Result Qualifier
% Rec. Unit
D
% Rec
0.10 U
2.50
2.69
mg/L
108
70 - 130
trans-1,2-Dichloroethene
0.10 U
2.50
2.59
mg/L
104
50 - 130
trans-1,3-Dichloropropene
0.10 U
2.50
1.87
mg/L
75
50 - 130
Trichloroethene
0.10 U
2.50
2.45
mg/L
98
67 - 132
Trichlorofluoromethane
0.10 U
2.50
1.62
mg/L
65
50 - 130
Vinyl acetate
0.10 U
10.0
6.61
mg/L
66
50 - 130
Vinyl chloride
0.10 U
2.50
1.55
mg/L
62
55 - 142
Lab Sample ID: 640-33835-3 MSD Matrix: Solid Analysis Batch: 101524 Result Qualifier
Spike Added
MSD MSD Result Qualifier
7 8
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
1,1,1,2-Tetrachloroethane
0.10 U
2.50
2.31
mg/L
92
70 - 130
3
30
1,1,1-Trichloroethane
0.10 U
2.50
2.24
mg/L
89
50 - 150
1
30
1,1,2-Trichloroethane
0.10 U
2.50
2.66
mg/L
107
50 - 130
2
30
1,1,2,2-Tetrachloroethane
0.10 U
2.50
2.63
mg/L
105
70 - 130
2
30
1,1-Dichloroethane
0.10 U
2.50
2.91
mg/L
116
50 - 130
12
30
1,2,3-Trichloropropane
0.10 U
2.50
2.09
mg/L
84
70 - 130
3
30
1,1-Dichloroethene
0.10 U
2.50
2.13
mg/L
85
56 - 146
3
30
1,2-Dibromo-3-Chloropropane
0.10 U
2.50
2.27
mg/L
91
50 - 130
10
30
1,2-Dichlorobenzene
0.10 U
2.50
2.51
mg/L
100
70 - 130
9
30
1,2-Dichloroethane
0.10 U
2.50
2.55
mg/L
102
67 - 136
3
23
1,2-Dichloropropane
0.10 U
2.50
2.45
mg/L
98
70 - 130
5
30
1,4-Dichlorobenzene
0.10 U
2.50
2.48
mg/L
99
50 - 130
5
30
2-Hexanone
0.10 U
10.0
9.64
mg/L
96
50 - 130
2
30
Acrylonitrile
0.10 U
25.0
33.2 J
mg/L
133
70 - 130
13
30
Acetone
0.46 U
10.0
10.5
mg/L
105
70 - 130
3
30
Benzene
0.10 U
2.50
2.70
mg/L
108
68 - 135
2
37
Bromoform
0.10 U J
2.50
1.82
mg/L
73
64 - 131
7
30
Bromomethane
0.10 U
2.50
1.27 J
mg/L
51
70 - 130
8
30
Carbon disulfide
0.10 U
10.0
8.11
mg/L
81
50 - 150
0
30
Carbon tetrachloride
0.10 U
2.50
2.18
mg/L
87
50 - 150
0
38
Chlorobenzene
0.10 U
2.50
2.54
mg/L
102
71 - 132
1
22
Chlorobromomethane
0.10 U
2.50
2.60
mg/L
104
70 - 130
5
30
Chlorodibromomethane
0.10 U
2.50
2.33
mg/L
93
70 - 130
3
30
cis-1,2-Dichloroethene
0.10 U
2.50
2.29
mg/L
92
50 - 130
7
30
cis-1,3-Dichloropropene
0.10 U
2.50
2.05
mg/L
82
50 - 130
4
30
Chloroethane
0.10 U
2.50
1.82
mg/L
73
61 - 115
5
30
Chloroform
0.10 U
2.50
2.66
mg/L
107
64 - 131
5
20
Chloromethane
0.10 U
2.50
1.54 J
mg/L
62
63 - 125
4
30
Dibromomethane
0.10 U
2.50
2.44
mg/L
98
70 - 130
5
30
Dichlorobromomethane
0.10 U
2.50
2.44
mg/L
98
70 - 130
4
30
Ethylbenzene
0.10 U
2.50
2.58
mg/L
103
50 - 130
0
30
Ethylene Dibromide
0.10 U
2.50
2.59
mg/L
104
70 - 130
1
30
Iodomethane
0.10 U
10.0
10.4
mg/L
104
50 - 130
7
30
m-Xylene & p-Xylene
0.10 U
5.00
5.47
mg/L
109
70 - 130
3
30
2-Butanone (MEK)
0.16 I
10.0
11.5
mg/L
114
45 - 139
9
31
Methylene Chloride
0.10 U
2.50
2.83
mg/L
113
50 - 130
8
30
4-Methyl-2-pentanone (MIBK)
0.10 U
10.0
8.66
mg/L
87
50 - 150
6
30
TestAmerica Tallahassee
Page 17 of 32
4 6
Client Sample ID: OWCB-P Prep Type: TCLP Sample Sample
3 5
Limits
Toluene
Analyte
1
06/15/2011
9 10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: 640-33835-3 MSD Matrix: Solid Analysis Batch: 101524
Client Sample ID: OWCB-P Prep Type: TCLP Sample Sample
Analyte
Result Qualifier
Spike Added
MSD MSD Result Qualifier
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
o-Xylene
0.10 U
2.50
2.46
mg/L
98
70 - 130
0
30
Styrene
0.10 U
2.50
2.29
mg/L
92
50 - 130
1
30
Tetrachloroethene
0.10 U
2.50
2.38
mg/L
95
51 - 154
2
24
Toluene
0.10 U
2.50
2.60
mg/L
104
70 - 130
3
30
trans-1,2-Dichloroethene
0.10 U
2.50
2.89
mg/L
116
50 - 130
11
30
trans-1,3-Dichloropropene
0.10 U
2.50
1.86
mg/L
74
50 - 130
1
30
Trichloroethene
0.10 U
2.50
2.53
mg/L
101
67 - 132
3
35
Trichlorofluoromethane
0.10 U
2.50
1.59
mg/L
63
50 - 130
2
30
Vinyl acetate
0.10 U
10.0
7.15
mg/L
72
50 - 130
8
30
Vinyl chloride
0.10 U
2.50
1.59
mg/L
63
55 - 142
2
21
Lab Sample ID: LCS 700-101541/2-A Matrix: Solid Analysis Batch: 101639
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 101541 Spike
Analyte
3 4 5 6 7 8 9 10 11
Method: 6010C - Metals (ICP)
Added
LCS LCS Result Qualifier
% Rec. Unit
D
% Rec
Limits
Silver
5.00
5.34
mg/L
107
80 - 120
Arsenic
5.00
5.19
mg/L
104
80 - 120
Barium
5.00
5.27
mg/L
105
80 - 120
Beryllium
5.00
5.47
mg/L
109
80 - 120
Cadmium
5.00
5.10
mg/L
102
80 - 120
Cobalt
5.00
5.08
mg/L
102
80 - 120
Chromium
5.00
5.06
mg/L
101
80 - 120
Copper
5.00
5.12
mg/L
102
80 - 120
Nickel
5.00
5.10
mg/L
102
80 - 120
Lead
5.00
5.12
mg/L
102
80 - 120
Antimony
5.00
5.06
mg/L
101
80 - 120
Selenium
5.00
5.29
mg/L
106
80 - 120
Thallium
5.00
5.13
mg/L
103
80 - 120
Vanadium
5.00
5.24
mg/L
105
80 - 120
Zinc
5.00
5.24
mg/L
105
80 - 120
Lab Sample ID: LCSD 700-101541/3-A Matrix: Solid Analysis Batch: 101639
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 101541 Spike
Analyte
1
Added
LCSD LCSD Result Qualifier
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
Silver
5.00
5.32
mg/L
106
80 - 120
0
20
Arsenic
5.00
5.18
mg/L
104
80 - 120
0
20
Barium
5.00
5.20
mg/L
104
80 - 120
1
20
Beryllium
5.00
5.45
mg/L
109
80 - 120
0
20
Cadmium
5.00
5.06
mg/L
101
80 - 120
1
20
Cobalt
5.00
5.02
mg/L
100
80 - 120
1
20
Chromium
5.00
5.00
mg/L
100
80 - 120
1
20
Copper
5.00
5.10
mg/L
102
80 - 120
0
20
Nickel
5.00
5.08
mg/L
102
80 - 120
0
20
Lead
5.00
5.06
mg/L
101
80 - 120
1
20
Antimony
5.00
5.04
mg/L
101
80 - 120
0
20
TestAmerica Tallahassee
Page 18 of 32
06/15/2011
12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 6010C - Metals (ICP) (Continued) Lab Sample ID: LCSD 700-101541/3-A Matrix: Solid Analysis Batch: 101639
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 101541 LCSD LCSD
Spike Analyte
Added
Result Qualifier
% Rec. Unit
D
% Rec
RPD
Limits
RPD
Limit
Selenium
5.00
5.26
mg/L
105
80 - 120
1
20
Thallium
5.00
5.12
mg/L
102
80 - 120
0
20
Vanadium
5.00
5.24
mg/L
105
80 - 120
0
20
Zinc
5.00
5.18
mg/L
104
80 - 120
1
20
Lab Sample ID: LB 700-101438/1-B LB Matrix: Solid Analysis Batch: 101639
Client Sample ID: Method Blank Prep Type: TCLP Prep Batch: 101541 LB LB
Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Arsenic
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Barium
0.50 U
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 10:38
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 10:38
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Copper
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Result Qualifier
D
Dil Fac
Nickel
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:38
1
Lead
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Selenium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Vanadium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:38
1
Zinc
Lab Sample ID: LB2 700-101438/2-B LB2 Matrix: Solid Analysis Batch: 101639
Client Sample ID: Method Blank Prep Type: TCLP Prep Batch: 101541 LB2 LB2
Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Arsenic
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Barium
0.50 U
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 10:56
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 10:56
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Copper
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Nickel
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:56
1
Lead
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Selenium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Vanadium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:56
1
Zinc
1
Result Qualifier
D
Dil Fac
TestAmerica Tallahassee
Page 19 of 32
06/15/2011
3 4 5 6 7 8 9 10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 1664A - HEM and SGT-HEM
3
Lab Sample ID: MB 700-101773/1-A Matrix: Water Analysis Batch: 101774
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 101773 MB MB
Analyte
PQL
Result Qualifier
HEM (Oil & Grease)
3.5 U
MDL Unit
5.3
D
3.5 mg/L
Lab Sample ID: LCS 700-101773/2-A Matrix: Water Analysis Batch: 101774
Prepared
Analyzed
Dil Fac
06/14/11 08:30
06/14/11 08:30
1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 101773 LCS LCS
Spike Analyte
Added
HEM (Oil & Grease)
Result Qualifier
42.1
43.8
Lab Sample ID: LCSD 700-101773/3-A Matrix: Water Analysis Batch: 101774
% Rec. Unit
D
mg/L
% Rec
104
LCSD LCSD
Analyte
Added
HEM (Oil & Grease)
Result Qualifier
42.1
42.9
D
mg/L
% Rec
102
RPD
Limits
RPD
Limit
2
18
79 - 114
Lab Sample ID: MB 640-81587/1 Matrix: Water Analysis Batch: 81587
Client Sample ID: Method Blank Prep Type: Total/NA MB MB Result Qualifier
0.50 U
PQL
MDL Unit
0.50
0.50 NTU
D
Prepared
Added
Turbidity
40.0
LCS LCS Result Qualifier
40.0
Lab Sample ID: LCSD 640-81587/3 Matrix: Water Analysis Batch: 81587
1
% Rec. Unit
D
NTU
% Rec
100
Limits
90 - 110
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike
Analyte
Added
Turbidity
40.0
LCSD LCSD Result Qualifier
40.0
% Rec. Unit
D
NTU
% Rec
100
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 81587
Limits
90 - 110
RPD RPD
Limit
0
30
Client Sample ID: OWCB-P Prep Type: Total/NA Sample Sample
Turbidity
Dil Fac
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Analyte
Analyzed
06/05/11 12:45
Lab Sample ID: LCS 640-81587/2 Matrix: Water Analysis Batch: 81587 Analyte
Result Qualifier
420
6 7 8 10 11 12 13
Method: 180.1 - Turbidity, Nephelometric
Turbidity
5
9
79 - 114
% Rec. Unit
4
Limits
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 101773 Spike
Analyte
1
DU DU Result Qualifier
421
RPD Unit
NTU
D
RPD
Limit
0
30
TestAmerica Tallahassee
Page 20 of 32
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: SM 2540C - Solids, Total Dissolved (TDS)
3
Lab Sample ID: MB 640-81646/1 Matrix: Water Analysis Batch: 81646
Client Sample ID: Method Blank Prep Type: Total/NA MB MB
Analyte
PQL
Result Qualifier
Total Dissolved Solids
2.3 U
MDL Unit
5.0
D
Prepared
2.3 mg/L
Analyzed
Dil Fac
06/07/11 10:15
Lab Sample ID: LCS 640-81646/2 Matrix: Water Analysis Batch: 81646
1
Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS
Spike Analyte
Added
Total Dissolved Solids
Result Qualifier
300
293
D
% Rec
98
LCSD LCSD
Analyte
Added
Total Dissolved Solids
Result Qualifier
300
282
D
mg/L
% Rec
94
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 81646
RPD
Limits
RPD
Limit
4
25
80 - 120
Client Sample ID: OWCB-P Prep Type: Total/NA DU DU
Sample Sample
RPD
Analyte
Result Qualifier
Result Qualifier
Unit
Total Dissolved Solids
12000
12400
mg/L
D
RPD
Limit
0.6
25
Method: SM 2540D - Solids, Total Suspended (TSS) Lab Sample ID: MB 640-81644/1 Matrix: Water Analysis Batch: 81644
Client Sample ID: Method Blank Prep Type: Total/NA MB MB
Total Suspended Solids
PQL
Result Qualifier
1.2 U
MDL Unit
2.0
D
Added
100
LCS LCS Result Qualifier
87.0
Lab Sample ID: LCSD 640-81644/3 Matrix: Water Analysis Batch: 81644
Total Suspended Solids
1
% Rec. Unit
D
mg/L
% Rec
87
Limits
80 - 120
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike
Analyte
Dil Fac
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Total Suspended Solids
Analyzed
06/07/11 10:09
Lab Sample ID: LCS 640-81644/2 Matrix: Water Analysis Batch: 81644 Analyte
Prepared
1.2 mg/L
Added
100
LCSD LCSD Result Qualifier
97.5
% Rec. Unit
mg/L
D
% Rec
98
Limits
80 - 120
RPD RPD
Limit
11
25
TestAmerica Tallahassee
Page 21 of 32
6 7 9
80 - 120
% Rec. Unit
5
Limits
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike
4
8
% Rec. Unit
mg/L
Lab Sample ID: LCSD 640-81646/3 Matrix: Water Analysis Batch: 81646
Analyte
1
06/15/2011
10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: SM 2710F - Specific Gravity, Density
3
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 101470
Client Sample ID: OWCB-P Prep Type: Total/NA DU DU
Sample Sample Analyte
Result Qualifier
Specific Gravity
1.0008
Result Qualifier
1.00
RPD Unit
D
NONE
RPD
Limit
0.4
20
Method: SM 4500 Cl G - Chlorine, Residual Client Sample ID: Method Blank Prep Type: Total/NA
Result Qualifier
0.043 U
PQL
MDL Unit
0.10
0.043 mg/L
D
Prepared
Added
Chlorine, Total Residual
1.00
LCS LCS Result Qualifier
0.930
Lab Sample ID: LCSD 700-101464/3 Matrix: Water Analysis Batch: 101464 Spike Added
Chlorine, Total Residual
1.00
Unit
D
mg/L
93
LCSD LCSD Result Qualifier
Result Qualifier
0.42 Q
Result Qualifier
0.42 Q
0.900
D
mg/L
Chlorine, Total Residual
% Rec
90
Spike Added
0.264
MS MS Result Qualifier
Limits
90 - 110
RPD RPD
Limit
3.3
10.0
0.690
% Rec. Unit
D
mg/L
% Rec
102
Spike Added
0.264
MSD MSD Result Qualifier
Limits
90 - 110
0.690
% Rec. Unit
D
mg/L
% Rec
102
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 101464
Limits
90 - 110
RPD RPD
Limit
0.0
10.0
Client Sample ID: OWCB-P Prep Type: Total/NA Sample Sample Result Qualifier
0.42 Q
8
DU DU Result Qualifier
0.390
RPD Unit
mg/L
D
RPD
Limit
7
TestAmerica Tallahassee
Page 22 of 32
10 11 13
Client Sample ID: OWCB-P Prep Type: Total/NA Sample Sample
Analyte
Limits
90 - 110
% Rec. Unit
Lab Sample ID: 640-33835-4 MSD Matrix: Solid Analysis Batch: 101464
Chlorine, Total Residual
% Rec
Client Sample ID: OWCB-P Prep Type: Total/NA Sample Sample
6
12
% Rec.
Lab Sample ID: 640-33835-4 MS Matrix: Solid Analysis Batch: 101464
Analyte
1
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA
Analyte
Chlorine, Total Residual
Dil Fac
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Analyte
Analyzed
06/07/11 10:00
Lab Sample ID: LCS 700-101464/2 Matrix: Water Analysis Batch: 101464 Analyte
5
9
MB MB
Chlorine, Total Residual
4
7
Lab Sample ID: MB 700-101464/1 Matrix: Water Analysis Batch: 101464 Analyte
1
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: SM 4500 H+ B - pH
3
Lab Sample ID: LCS 640-81609/1 Matrix: Water Analysis Batch: 81609
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Analyte
Added
pH
9.22
LCS LCS Result Qualifier
9.200
D
SU
Sample Sample
pH
Result Qualifier
6.72 Q
% Rec
100
Limits
90 - 110
6
Client Sample ID: OWCB-P Prep Type: Total/NA
7
RPD
8
DU DU Result Qualifier
6.750
Unit
SU
D
4 5
% Rec. Unit
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 81609 Analyte
1
RPD
Limit
0.4
40
9 10 11 12 13
TestAmerica Tallahassee
Page 23 of 32
06/15/2011
QC Association Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
GC/MS VOA
3
Leach Batch: 101440 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
640-33835-3
OWCB-P
TCLP
Solid
1311
640-33835-3 MS
OWCB-P
TCLP
Solid
1311
640-33835-3 MSD
OWCB-P
TCLP
Solid
1311
640-33835-2
MCWB-E
TCLP
Solid
1311
640-33835-1
MCWB-W
TCLP
Solid
1311
Prep Batch
4 5 6 7
Analysis Batch: 101524 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 700-101524/3
Lab Control Sample
Total/NA
Solid
8260C
LCSD 700-101524/4
Lab Control Sample Dup
Total/NA
Solid
8260C
MRL 700-101524/5 MRL
Lab Control Sample
Total/NA
Solid
8260C
MB 700-101524/6
Method Blank
Total/NA
Solid
8260C
640-33835-1
MCWB-W
TCLP
Solid
8260C
640-33835-2
MCWB-E
TCLP
Solid
8260C
640-33835-3
OWCB-P
TCLP
Solid
8260C
640-33835-3 MS
OWCB-P
TCLP
Solid
8260C
640-33835-3 MSD
OWCB-P
TCLP
Solid
8260C
Prep Batch
8 9 10 11 12 13
Metals Leach Batch: 101438 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LB 700-101438/1-B LB
Method Blank
TCLP
Solid
1311
Prep Batch
LB2 700-101438/2-B LB2
Method Blank
TCLP
Solid
1311
640-33835-1
MCWB-W
TCLP
Solid
1311
640-33835-2
MCWB-E
TCLP
Solid
1311
640-33835-3
OWCB-P
TCLP
Solid
1311
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 700-101541/2-A
Lab Control Sample
Total/NA
Solid
3010A
LCSD 700-101541/3-A
Lab Control Sample Dup
Total/NA
Solid
3010A
LB 700-101438/1-B LB
Method Blank
TCLP
Solid
3010A
101438
640-33835-1
MCWB-W
TCLP
Solid
3010A
101438
640-33835-2
MCWB-E
TCLP
Solid
3010A
101438
LB2 700-101438/2-B LB2
Method Blank
TCLP
Solid
3010A
101438
640-33835-3
OWCB-P
TCLP
Solid
3010A
101438
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 700-101541/2-A
Lab Control Sample
Total/NA
Solid
6010C
101541
LCSD 700-101541/3-A
Lab Control Sample Dup
Total/NA
Solid
6010C
101541
LB 700-101438/1-B LB
Method Blank
TCLP
Solid
6010C
101541
640-33835-1
MCWB-W
TCLP
Solid
6010C
101541
640-33835-2
MCWB-E
TCLP
Solid
6010C
101541
LB2 700-101438/2-B LB2
Method Blank
TCLP
Solid
6010C
101541
640-33835-3
OWCB-P
TCLP
Solid
6010C
101541
Prep Batch: 101541 Prep Batch
Analysis Batch: 101639 Prep Batch
TestAmerica Tallahassee
Page 24 of 32
06/15/2011
QC Association Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
General Chemistry
3
Analysis Batch: 81587 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 640-81587/1
Method Blank
Total/NA
Water
180.1
LCS 640-81587/2
Lab Control Sample
Total/NA
Water
180.1
LCSD 640-81587/3
Lab Control Sample Dup
Total/NA
Water
180.1
640-33835-4
OWCB-P
Total/NA
Water
180.1
640-33835-4 DU
OWCB-P
Total/NA
Solid
180.1
Prep Batch
4 5 6 7
Analysis Batch: 81609 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 640-81609/1
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
640-33835-4
OWCB-P
Total/NA
Water
SM 4500 H+ B
640-33835-4 DU
OWCB-P
Total/NA
Solid
SM 4500 H+ B
Prep Batch
8 9 10
Analysis Batch: 81644 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 640-81644/1
Method Blank
Total/NA
Water
SM 2540D
LCS 640-81644/2
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 640-81644/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
640-33835-4
OWCB-P
Total/NA
Water
SM 2540D
Prep Batch
11 12 13
Analysis Batch: 81646 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 640-81646/1
Method Blank
Total/NA
Water
SM 2540C
LCS 640-81646/2
Lab Control Sample
Total/NA
Water
SM 2540C
LCSD 640-81646/3
Lab Control Sample Dup
Total/NA
Water
SM 2540C
640-33835-4
OWCB-P
Total/NA
Water
SM 2540C
640-33835-4 DU
OWCB-P
Total/NA
Solid
SM 2540C
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 700-101464/1
Method Blank
Total/NA
Water
SM 4500 Cl G
LCS 700-101464/2
Lab Control Sample
Total/NA
Water
SM 4500 Cl G
LCSD 700-101464/3
Lab Control Sample Dup
Total/NA
Water
SM 4500 Cl G
640-33835-4
OWCB-P
Total/NA
Water
SM 4500 Cl G
640-33835-4 DU
OWCB-P
Total/NA
Solid
SM 4500 Cl G
640-33835-4 MS
OWCB-P
Total/NA
Solid
SM 4500 Cl G
640-33835-4 MSD
OWCB-P
Total/NA
Solid
SM 4500 Cl G
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 700-101470/1
Lab Control Sample
Total/NA
Water
SM 2710F
LCSD 700-101470/2
Lab Control Sample Dup
Total/NA
Water
SM 2710F
640-33835-4
OWCB-P
Total/NA
Water
SM 2710F
640-33835-4 DU
OWCB-P
Total/NA
Solid
SM 2710F
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 700-101773/1-A
Method Blank
Total/NA
Water
1664A
LCS 700-101773/2-A
Lab Control Sample
Total/NA
Water
1664A
LCSD 700-101773/3-A
Lab Control Sample Dup
Total/NA
Water
1664A
640-33835-4
OWCB-P
Total/NA
Water
1664A
Prep Batch
Analysis Batch: 101464 Prep Batch
Analysis Batch: 101470 Prep Batch
Prep Batch: 101773 Prep Batch
TestAmerica Tallahassee
Page 25 of 32
06/15/2011
QC Association Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
General Chemistry (Continued)
3
Analysis Batch: 101774 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 700-101773/1-A
Method Blank
Total/NA
Water
1664A
Prep Batch
101773
LCS 700-101773/2-A
Lab Control Sample
Total/NA
Water
1664A
101773
LCSD 700-101773/3-A
Lab Control Sample Dup
Total/NA
Water
1664A
101773
640-33835-4
OWCB-P
Total/NA
Water
1664A
101773
4 5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 26 of 32
06/15/2011
Lab Chronicle Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-W
Lab Sample ID: 640-33835-1
2
Date Collected: 06/03/11 13:30 Date Received: 06/04/11 10:05
Matrix: Solid
Batch
Batch
Prep Type
Type
Method
TCLP
Leach
1311
TCLP
Analysis
8260C
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010C
Run
Batch
Factor
Number
Or Analyzed
Analyst
Lab
101440
06/07/11 17:10
MEB
TAL MOB
101524
06/09/11 16:24
JB
TAL MOB
101438
06/07/11 17:04
MEB
TAL MOB
101541
06/09/11 12:05
MEB
TAL MOB
101639
06/10/11 10:45
ZST
TAL MOB
100
1
Prepared
Lab Sample ID: 640-33835-2
Date Collected: 06/03/11 13:50 Date Received: 06/04/11 10:05
Matrix: Solid
Batch
Batch
Type
Method
TCLP
Leach
1311
TCLP
Analysis
8260C
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010C
Run
Dilution
Batch
Factor
Number
Or Analyzed
101440 101524
100
1
Analyst
Lab
06/07/11 17:10
MEB
TAL MOB
06/09/11 16:48
JB
TAL MOB
101438
06/07/11 17:04
MEB
TAL MOB
101541
06/09/11 12:05
MEB
TAL MOB
101639
06/10/11 10:52
ZST
TAL MOB
Lab Sample ID: 640-33835-3
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Solid
Batch
Batch
Prep Type
Type
Method
Dilution
Batch
Factor
Number
Or Analyzed
TCLP
Leach
1311
Analyst
Lab
101440
06/07/11 17:10
MEB
TCLP
Analysis
8260C
TAL MOB
101524
06/09/11 17:13
JB
TAL MOB
TCLP
Leach
TCLP
Prep
1311
101438
06/07/11 17:04
MEB
TAL MOB
3010A
101541
06/09/11 12:05
MEB
TCLP
Analysis
6010C
TAL MOB
101639
06/10/11 11:00
ZST
TAL MOB
Run
100
1
Prepared
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-4
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Water
Batch
Batch
Prep Type
Type
Method
Dilution
Batch
Factor
Number
Total/NA
Analysis
180.1
Analyst
Lab
16
81587
06/05/11 12:45
JS
TAL TAL
Total/NA
Analysis
SM 4500 H+ B
1
81609
06/06/11 14:00
JS
TAL TAL
Total/NA
Analysis
SM 2540D
1
81644
DA
TAL TAL
DA
TAL TAL
Run
Prepared Or Analyzed
(Start): 06/07/11 10:09 (End): 06/08/11 09:03 Total/NA
Analysis
SM 2540C
1
81646 (Start): 06/07/11 10:15 (End): 06/08/11 12:44
Total/NA
Analysis
SM 4500 Cl G
1
101464
06/07/11 10:00
JDP
TAL MOB
Total/NA
Analysis
SM 2710F
1
101470
06/08/11 12:10
TKN
TAL MOB
Total/NA
Analysis
1664A
1
101774
06/14/11 08:30
HPG
TAL MOB
Total/NA
Prep
1664A
101773
06/14/11 08:30
HPG
TAL MOB
TestAmerica Tallahassee
Page 27 of 32
5 6 7 8 9 10
Prepared
Client Sample ID: OWCB-P
3 4
Dilution
Client Sample ID: MCWB-E
Prep Type
1
06/15/2011
11 12 13
Lab Chronicle Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2 3
Laboratory References:
TAL MOB = TestAmerica Mobile, 900 Lakeside Drive, Mobile, AL 36693, TEL (251)666-6633 TAL TAL = TestAmerica Tallahassee, 2846 Industrial Plaza Drive, Tallahassee, FL 32301, TEL (850)878-3994
4 5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 28 of 32
06/15/2011
Certification Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Laboratory
Authority
Program
EPA Region
Certification ID
TestAmerica Tallahassee
Florida
NELAC
4
E81005
TestAmerica Tallahassee
Louisiana
NELAC
6
30663
TestAmerica Tallahassee
New Jersey
NELAC
2
FL012
TestAmerica Tallahassee
Oklahoma
State Program
6
9986
TestAmerica Tallahassee
Texas
NELAC
6
T104704459-11-2
TestAmerica Tallahassee
USDA
USDA
0
P330-08-00158
TestAmerica Mobile
Alabama
State Program
4
40030
TestAmerica Mobile
Arkansas
State Program
6
88-0765
TestAmerica Mobile
Florida
NELAC
4
E87089
TestAmerica Mobile
Georgia
State Program
4
952
TestAmerica Mobile
Louisiana
NELAC
6
LA0900026
TestAmerica Mobile
Louisiana
NELAC
6
30673
TestAmerica Mobile
Mississippi
State Program
4
N/A
TestAmerica Mobile
North Carolina
North Carolina DENR
4
395
TestAmerica Mobile
South Carolina
State Program
4
75002
TestAmerica Mobile
Tennessee
State Program
4
2979
TestAmerica Mobile
Texas
NELAC
6
T104704460-09A-TX
TestAmerica Mobile
USDA
USDA
0
P330-08-00039
TestAmerica Mobile
Washington
State Program
10
C1918
4 5 6 7 8 9 10 11 12 13
Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s current list of certified methods and analytes.
TestAmerica Tallahassee
Page 29 of 32
3
06/15/2011
Method Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Method
Method Description
Protocol
Laboratory
8260C
Volatile Organic Compounds by GC/MS
SW846
TAL MOB
6010C
Metals (ICP)
SW846
TAL MOB
1664A
HEM and SGT-HEM
1664A
TAL MOB
180.1
Turbidity, Nephelometric
MCAWW
TAL TAL
SM 2540C
Solids, Total Dissolved (TDS)
SM
TAL TAL
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL TAL
SM 2710F
Specific Gravity, Density
SM
TAL MOB
SM 4500 Cl G
Chlorine, Residual
SM
TAL MOB
SM 4500 H+ B
pH
SM
TAL TAL
3 4 5 6 7 8
Protocol References:
1664A = EPA-821-98-002
9
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater",
10
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
11
Laboratory References:
TAL MOB = TestAmerica Mobile, 900 Lakeside Drive, Mobile, AL 36693, TEL (251)666-6633
12
TAL TAL = TestAmerica Tallahassee, 2846 Industrial Plaza Drive, Tallahassee, FL 32301, TEL (850)878-3994
13
TestAmerica Tallahassee
Page 30 of 32
06/15/2011
Sample Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
640-33835-1
MCWB-W
Solid
06/03/11 13:30
06/04/11 10:05
640-33835-2
MCWB-E
Solid
06/03/11 13:50
06/04/11 10:05
640-33835-3
OWCB-P
Solid
06/03/11 14:15
06/04/11 10:05
640-33835-4
OWCB-P
Water
06/03/11 14:15
06/04/11 10:05
3 4 5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 31 of 32
06/15/2011
1 2 3 4 5 6 7 8 9 10 11 12 13
Page 32 of 32
06/15/2011
SUMMARY OF GROUNDWATER ELEVATION DATA (GOLDER, NOVEMBER 7, 2011)
SUMMARY OF SEDIMENT AND WASTEWATER SAMPLING METAL CLEANING WASTE BASINS AND OILY WASTE COLLECTION BASINS (GOLDER, JUNE 23, 2011)
June 23, 2011
113-82520
Mr. Alan Ehrle St Johns River Power Park 11201 New Berlin Road Jacksonville, FL 32226 RE:
RESULTS OF SEDIMENT AND WASTEWATER SAMPLING OILY WASTE AND METAL CLEANING WASTE BASINS ST. JOHNS RIVER POWER PARK JACKSONVILLE, FLORIDA
Dear Mr. Ehrle: Golder Associates Inc. (Golder) is pleased to provide St. Johns River Power Park (SJRPP) with the results of the recent sampling of sediment and wastewater in the Oily Waste and the Metal Cleaning Waste Basins. A bid document for the re-lining of these basins is being prepared and the sampling was performed to provide SJRPP with sediment and wastewater quality data for the basins such that SJRPP can better direct bidders as to the handling and disposal requirements for these materials.
FIELD SAMPLING On June 3, 2011, a representative from Golder collected grab samples of sediment from the northern (primary) Oily Waste Basin (sample designated OWCB-P) and the east and west Metal Cleaning Waste Basins (samples designated MCWB-E and MCWB-W)). In addition, a wastewater sample was collected from the northern (primary) Oily Waste Basin. Approximate sample locations are shown on Figure 1.
ANALYTICAL TESTING Samples were sent to TestAmerica Tallahassee for analysis of the following parameters:
Sediment – TCLP Appendix I volatiles and metals
Wastewater – Total Dissolved Solids (TDS), Total Suspended Solids (TSS), pH, turbidity, specific gravity, oil & grease, and residual chlorine.
RESULTS For the parameters analyzed, the TCLP testing of the sediment grab samples did not detect any constituents above the limits established by 40 CFR 261.24. For comparison purposes only, the TCLP results were also compared to Florida Groundwater standards under Chapter 62-777, FAC (see Table 1). The TCLP results were higher than Florida Groundwater standards for several metals including arsenic, nickel, selenium, and vanadium. For the parameters analyzed, the wastewater grab sample collected from the northern (primary) Oily Waste Basin exceeded JEA pretreatment standards for oil and grease. It is noted that these standards are not directly applicable as SJRPP has its own treatment plant and are provided for comparison purposes only.
CONCLUSIONS The results of the sediment sampling indicated that, for the parameters analyzed, those materials did not exceed any of the standards established under 40 CFR 261.24. As such, those materials could be handled and disposed of as non-hazardous. While the sediment from the Oily Waste basin did not report Golder Associates Inc. 9428 Baymeadows Road, Suite 400 Jacksonville, FL 32256 USA Tel: (904) 363-3430 Fax: (904) 363-3445 www.golder.com Golder Associates: Operations in Africa, Asia, Australasia, Europe, North America and South America
Mr. Alan Ehrle St. Johns River Power Park
2
June 23, 2011 113-82520
much in the volatile scan, it is noted that the wastewater sample detected high levels of oil and grease and it is possible that the sediment could also contain high levels of oil and grease.
CLOSING Golder appreciates the opportunity to provide these services to SJRPP. Please feel free to contact us with any questions or comments concerning this report. Sincerely, GOLDER ASSOCIATES INC.
Samuel F. Stafford Staff Engineer
Kenneth B. Karably, PE, PG Principal Attachment:
Table 1 – Summary of Detections, Sediment TCLP Analyses Table 2 – Summary of Detections, Wastewater Sample Figure 1 – Sample Location Plan Attachment A – TestAmerica Report (6/15/2011)
FN: G:\Projects\113\113-82\113-82520\200 Draft Rpts\SJRPP - OWB and MWCB Sampling (06.23.2011).docx
SJRPP - OWB and MWCB Sampling (06.23.2011).docx
June 2011
113-82520
TABLE 1 SUMMARY OF DETECTIONS - SEDIMENT TCLP ANALYSES OILY WASTE COLLECTION AND METAL CLEANING WASTE BASINS ST. JOHNS RIVER POWER PARK - JACKSONVILLE, FLORIDA
Standard SAMPLE GCTL LOCATION D-LIST MCWB-W MCWB-E OWCB-P
Arsenic 0.010 5 0.050 U 0.050 U 0.058 I
Barium 2 100 0.59 I 0.73 I 0.50 U
Copper 1 NL 0.29 I 0.12 I 0.050 U
Nickel 0.1 NL 0.16 I 0.10 U 0.18 I
Selenium Vanadium 0.05 0.049 1.0 NL 0.070 I 0.050 U 0.050 U 0.050 U 0.050 U 0.070 I
Zinc 5 NL 0.95 I 0.74 I 2.4 I
2-Butanone 4.2 200 0.21 I 0.14 I 0.16 I
NOTES: Pond sediment samples collected by Golder on 6/3/2011 and analyzed by TestAmerica TCLP = Toxicity Characteristic Leaching Procedure All concentrations listed in milligrams per liter (mg/L) GCTL = Groundwater Cleanup Target Level per Ch. 62-777, FAC. D-List = Maximum Concentration of Contaminants for Toxicity Characteristic per 40 CFR 261.24 NL = Compound was not listed in standard MCWB = Metal Cleaning Waste Basin OWCB = Oily Waste Collection Basin U = Indicates that the compound was analyzed for but not detected I = The reported value is between the laboratory method detection limit and laboratory practical quantitation limit
Checked by: SFS Reviewed by: KBK
G:\Projects\113\113-82\113-82520\200 Draft Rpts\202 - Sampling Report\Basin Sampling Results.xlsx\Table 1
Golder Associates
June 2011
113-82520
TABLE 2 SUMMARY OF DETECTIONS - WASTEWATER SAMPLE OILY WASTE COLLECTION BASIN ST. JOHNS RIVER POWER PARK - JACKSONVILLE, FLORIDA
Standard SAMPLE JEA LOCATION OWCB-P
HEM 100 19,000
Turbidity NL 420
TDS NL 12,000
TSS NL 1,300
Chlorine NL 0.42
pH 5.5-12.0 6.72
NOTES: Basin wastewater sample collected by Golder on 6/3/2011 and analyzed by TestAmerica All concentrations listed in milligrams per liter (mg/L), except Turbidty (NTU) and pH (SU). OWCB = Oily Waste Collection Basin HEM = n-hexane extractable material (Oil and Grease) JEA = JEA Industrial Pretreatment Regulation
Checked by: SFS Reviewed by: KBK
G:\Projects\113\113-82\113-82520\200 Draft Rpts\202 - Sampling Report\Basin Sampling Results.xlsx\Table 2
Golder Associates
1 2 3 4 5
ANALYTICAL REPORT
6
TestAmerica Laboratories, Inc. TestAmerica Tallahassee 2846 Industrial Plaza Drive Tallahassee, FL 32301 Tel: (850)878-3994
7 8 9
TestAmerica Job ID: 640-33835-1 Client Project/Site: St. Johns Power Park
10
For: Golder Associates Inc. 9428 Baymeadows Road Suite 400 Jacksonville, Florida 32256
11 12 13
Attn: Mr. Kenneth Karably
Authorized for release by: 06/15/2011 04:23:05 PM Chad Bechtold Project Manager II [email protected]
Results relate only to the items tested and the sample(s) as received by the laboratory. The test results in this report meet all 2003 NELAC requirements for accredited parameters, exceptions are noted in this report. Pursuant to NELAC, this report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Page 1 of 32
06/15/2011
Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Table of Contents Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
3
1 2 3 4 5 6 13 24 27 29 30 31 32
4 5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 2 of 32
06/15/2011
Definitions/Glossary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Qualifiers
3
GC/MS VOA Qualifier
Qualifier Description
I
The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
J
Estimated value; value may not be accurate.
U
Indicates that the compound was analyzed for but not detected.
4 5 6
Metals Qualifier
Qualifier Description
I
The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
U
Indicates that the compound was analyzed for but not detected.
7 8
General Chemistry Qualifier
Qualifier Description
Q
Sample held beyond the accepted holding time.
U
Indicates that the compound was analyzed for but not detected.
9 10
Glossary Abbreviation
These commonly used abbreviations may or may not be present in this report.
☼
Listed under the "D" column to designate that the result is reported on a dry weight basis.
EPA
United States Environmental Protection Agency
ND
Not Detected above the reporting level.
MDL
Method Detection Limit
RL
Reporting Limit
RE, RE1 (etc.)
Indicates a Re-extraction or Reanalysis of the sample.
%R
Percent Recovery
RPD
Relative Percent Difference, a measure of the relative difference between two points.
11 12 13
TestAmerica Tallahassee
Page 3 of 32
06/15/2011
Case Narrative Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Job ID: 640-33835-1
3
Laboratory: TestAmerica Tallahassee
4
Narrative
Job Narrative 640-33835-1
5 6
Comments No additional comments.
7
Receipt All samples were received in good condition within temperature requirements.
8
GC/MS VOA Method 8260C: The laboratory control sample recovery for Bromoform was outside control limits. This compound, qualified with a "J", was not detected in the associated samples. The matrix spike (MS) and / or matrix spike duplicate (MSD) recoveries for Acrylonitrile, Bromomethane, and Chloromethane were outside control limits.
10
No other analytical or quality issues were noted.
11
Metals No analytical or quality issues were noted.
12
9
13
General Chemistry Method SM4500 Cl G: Residual Chlorine analysis should be performed in the field within 15 minutes of collection. The sample results have been qualified with a "Q".
Method SM4500 H+ B: pH analysis should be performed in the field within 15 minutes of collection. The sample results have been qualified with a "Q". No other analytical or quality issues were noted. VOA Prep No analytical or quality issues were noted.
TestAmerica Tallahassee
Page 4 of 32
06/15/2011
Detection Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-W
Lab Sample ID: 640-33835-1
Analyte
2 Result Qualifier
PQL
MDL Unit
Dil Fac D Method
0.21 I
1.0
0.10 mg/L
100
8260C
TCLP
Barium
0.59 I
0.80
0.50 mg/L
1
6010C
TCLP
Copper
0.29 I
0.50
0.050 mg/L
1
6010C
TCLP
Nickel
0.16 I
2.5
0.10 mg/L
1
6010C
TCLP
0.070 I
0.25
0.050 mg/L
1
6010C
TCLP
0.95 I
2.5
0.10 mg/L
1
6010C
TCLP
Zinc
Client Sample ID: MCWB-E Analyte
Lab Sample ID: 640-33835-2 Result Qualifier
PQL
MDL Unit
Dil Fac D Method
Prep Type
2-Butanone (MEK)
0.14 I
1.0
0.10 mg/L
100
8260C
TCLP
Barium
0.73 I
0.80
0.50 mg/L
1
6010C
TCLP
Copper
0.12 I
0.50
0.050 mg/L
1
6010C
TCLP
Zinc
0.74 I
2.5
0.10 mg/L
1
6010C
TCLP
Client Sample ID: OWCB-P Analyte
2-Butanone (MEK) Arsenic Nickel Vanadium Zinc
Lab Sample ID: 640-33835-3 Result Qualifier
PQL
MDL Unit
Dil Fac D Method
Prep Type
0.16 I
1.0
0.10 mg/L
100
8260C
TCLP
0.058 I
0.25
0.050 mg/L
1
6010C
TCLP
0.18 I
2.5
0.10 mg/L
1
6010C
TCLP
0.070 I
0.25
0.050 mg/L
1
6010C
TCLP
2.4 I
2.5
0.10 mg/L
1
6010C
TCLP
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-4 PQL
MDL Unit
Analyte
Result Qualifier
HEM (Oil & Grease)
19000
5.3
3.5 mg/L
1
1664A
Total/NA
420
8.0
8.0 NTU
16
180.1
Total/NA
12000
100
46 mg/L
1
SM 2540C
Total/NA
1300
2.5
1.4 mg/L
1
SM 2540D
Total/NA
1
SM 2710F
Total/NA
Turbidity Total Dissolved Solids Total Suspended Solids Specific Gravity
1.0008
NONE
Dil Fac D Method
Prep Type
Chlorine, Total Residual
0.42 Q
0.10
0.043 mg/L
1
SM 4500 Cl G
Total/NA
pH
6.72 Q
1.00
1.00 SU
1
SM 4500 H+ B
Total/NA
TestAmerica Tallahassee
Page 5 of 32
3
Prep Type
2-Butanone (MEK)
Selenium
1
06/15/2011
4 5 6 7 8 9 10 11 12 13
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-W
Lab Sample ID: 640-33835-1
1 2
Date Collected: 06/03/11 13:30 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 8260C - Volatile Organic Compounds by GC/MS - TCLP Analyte
PQL
MDL Unit
1,1,1,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1,1-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1,2-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1,2,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,2,3-Trichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,1-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,2-Dibromo-3-Chloropropane
0.10 U
0.50
0.10 mg/L
06/09/11 16:24
100
1,2-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,2-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,2-Dichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
1,4-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
2-Hexanone
0.10 U
1.0
0.10 mg/L
06/09/11 16:24
100
Acrylonitrile
0.10 U
1.0
0.10 mg/L
06/09/11 16:24
100
Acetone
0.46 U
2.5
0.46 mg/L
06/09/11 16:24
100
Benzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Bromoform
0.10 U J
0.10
0.10 mg/L
06/09/11 16:24
100
Bromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Carbon disulfide
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Carbon tetrachloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chlorodibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
cis-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
cis-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chloroform
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Chloromethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Dibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Dichlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Ethylbenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Ethylene Dibromide
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Iodomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
m-Xylene & p-Xylene
0.10 U
0.20
0.10 mg/L
06/09/11 16:24
100
2-Butanone (MEK)
0.21 I
1.0
0.10 mg/L
06/09/11 16:24
100
Methylene Chloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
4-Methyl-2-pentanone (MIBK)
0.10 U
1.0
0.10 mg/L
06/09/11 16:24
100
o-Xylene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Styrene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Tetrachloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Toluene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
trans-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
trans-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
trans-1,4-Dichloro-2-butene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Trichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Trichlorofluoromethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Vinyl acetate
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Vinyl chloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:24
100
Xylenes, Total
0.10 U
0.30
0.10 mg/L
06/09/11 16:24
100
Result Qualifier
D
Prepared
Analyzed
Dil Fac
TestAmerica Tallahassee
Page 6 of 32
06/15/2011
5 6 7 8 9 10 11 12 13
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-W
Lab Sample ID: 640-33835-1
1 2
Date Collected: 06/03/11 13:30 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 6010C - Metals (ICP) - TCLP Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Arsenic
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Barium
0.59 I
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 10:45
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 10:45
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Copper
0.29 I
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Nickel
0.16 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:45
1
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Selenium
0.070 I
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
Vanadium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:45
1
0.95 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:45
1
Lead
Zinc
Result Qualifier
D
Dil Fac
5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 7 of 32
06/15/2011
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-E
Lab Sample ID: 640-33835-2
1 2
Date Collected: 06/03/11 13:50 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 8260C - Volatile Organic Compounds by GC/MS - TCLP Analyte
PQL
MDL Unit
1,1,1,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1,1-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1,2-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1,2,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,2,3-Trichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,1-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,2-Dibromo-3-Chloropropane
0.10 U
0.50
0.10 mg/L
06/09/11 16:48
100
1,2-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,2-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,2-Dichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
1,4-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
2-Hexanone
0.10 U
1.0
0.10 mg/L
06/09/11 16:48
100
Acrylonitrile
0.10 U
1.0
0.10 mg/L
06/09/11 16:48
100
Acetone
0.46 U
2.5
0.46 mg/L
06/09/11 16:48
100
Benzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Bromoform
0.10 U J
0.10
0.10 mg/L
06/09/11 16:48
100
Bromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Carbon disulfide
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Carbon tetrachloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chlorodibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
cis-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
cis-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chloroform
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Chloromethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Dibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Dichlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Ethylbenzene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Ethylene Dibromide
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Iodomethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
m-Xylene & p-Xylene
0.10 U
0.20
0.10 mg/L
06/09/11 16:48
100
2-Butanone (MEK)
0.14 I
1.0
0.10 mg/L
06/09/11 16:48
100
Methylene Chloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
4-Methyl-2-pentanone (MIBK)
0.10 U
1.0
0.10 mg/L
06/09/11 16:48
100
o-Xylene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Styrene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Tetrachloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Toluene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
trans-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
trans-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
trans-1,4-Dichloro-2-butene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Trichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Trichlorofluoromethane
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Vinyl acetate
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Vinyl chloride
0.10 U
0.10
0.10 mg/L
06/09/11 16:48
100
Xylenes, Total
0.10 U
0.30
0.10 mg/L
06/09/11 16:48
100
Result Qualifier
D
Prepared
Analyzed
Dil Fac
TestAmerica Tallahassee
Page 8 of 32
06/15/2011
5 6 7 8 9 10 11 12 13
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-E
Lab Sample ID: 640-33835-2
1 2
Date Collected: 06/03/11 13:50 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 6010C - Metals (ICP) - TCLP Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Arsenic
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Barium
0.73 I
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 10:52
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 10:52
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Copper
0.12 I
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Nickel
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:52
1
Lead
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Selenium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
Vanadium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:52
1
0.74 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:52
1
Zinc
Result Qualifier
D
Dil Fac
5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 9 of 32
06/15/2011
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-3
1 2
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 8260C - Volatile Organic Compounds by GC/MS - TCLP Analyte
PQL
MDL Unit
1,1,1,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1,1-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1,2-Trichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1,2,2-Tetrachloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,2,3-Trichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,1-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,2-Dibromo-3-Chloropropane
0.10 U
0.50
0.10 mg/L
06/09/11 17:13
100
1,2-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,2-Dichloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,2-Dichloropropane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
1,4-Dichlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
2-Hexanone
0.10 U
1.0
0.10 mg/L
06/09/11 17:13
100
Acrylonitrile
0.10 U
1.0
0.10 mg/L
06/09/11 17:13
100
Acetone
0.46 U
2.5
0.46 mg/L
06/09/11 17:13
100
Benzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Bromoform
0.10 U J
0.10
0.10 mg/L
06/09/11 17:13
100
Bromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Carbon disulfide
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Carbon tetrachloride
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chlorobenzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chlorodibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
cis-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
cis-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chloroethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chloroform
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Chloromethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Dibromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Dichlorobromomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Ethylbenzene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Ethylene Dibromide
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Iodomethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
m-Xylene & p-Xylene
0.10 U
0.20
0.10 mg/L
06/09/11 17:13
100
2-Butanone (MEK)
0.16 I
1.0
0.10 mg/L
06/09/11 17:13
100
Methylene Chloride
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
4-Methyl-2-pentanone (MIBK)
0.10 U
1.0
0.10 mg/L
06/09/11 17:13
100
o-Xylene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Styrene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Tetrachloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Toluene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
trans-1,2-Dichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
trans-1,3-Dichloropropene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
trans-1,4-Dichloro-2-butene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Trichloroethene
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Trichlorofluoromethane
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Vinyl acetate
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Vinyl chloride
0.10 U
0.10
0.10 mg/L
06/09/11 17:13
100
Xylenes, Total
0.10 U
0.30
0.10 mg/L
06/09/11 17:13
100
Result Qualifier
D
Prepared
Analyzed
Dil Fac
TestAmerica Tallahassee
Page 10 of 32
06/15/2011
5 6 7 8 9 10 11 12 13
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-3
1 2
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Solid
3 4
Method: 6010C - Metals (ICP) - TCLP Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Arsenic
0.058 I
Result Qualifier
D
Dil Fac
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
0.50 U
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 11:00
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 11:00
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Copper
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Nickel
0.18 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 11:00
1
Lead
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Selenium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
Vanadium
0.070 I
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 11:00
1
2.4 I
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 11:00
1
Barium
Zinc
5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 11 of 32
06/15/2011
Client Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-4
1 2
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Water
3 4
General Chemistry Analyte
Result Qualifier
HEM (Oil & Grease)
19000
Turbidity Total Dissolved Solids Total Suspended Solids Specific Gravity
PQL
MDL Unit
5.3
3.5 mg/L
D
Prepared
Analyzed
06/14/11 08:30
06/14/11 08:30
Dil Fac
1
420
8.0
8.0 NTU
06/05/11 12:45
16
12000
100
46 mg/L
06/07/11 10:15
1
1300
2.5
1.4 mg/L
06/07/11 10:09
1
06/08/11 12:10
1
NONE
1.0008
Chlorine, Total Residual
0.42 Q
0.10
0.043 mg/L
06/07/11 10:00
1
pH
6.72 Q
1.00
1.00 SU
06/06/11 14:00
1
5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 12 of 32
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Method: 8260C - Volatile Organic Compounds by GC/MS
3
Lab Sample ID: MB 700-101524/6 Matrix: Solid Analysis Batch: 101524
Client Sample ID: Method Blank Prep Type: Total/NA MB MB
Analyte
Result Qualifier
PQL
MDL Unit
1,1,1,2-Tetrachloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1,1-Trichloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1,2-Trichloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1,2,2-Tetrachloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1-Dichloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,2,3-Trichloropropane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,1-Dichloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,2-Dibromo-3-Chloropropane
0.0010 U
0.0050
0.0010 mg/L
06/09/11 08:57
1
1,2-Dichlorobenzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,2-Dichloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,2-Dichloropropane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
1,4-Dichlorobenzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
2-Hexanone
0.0010 U
0.010
0.0010 mg/L
06/09/11 08:57
1
Acrylonitrile
0.0010 U
0.010
0.0010 mg/L
06/09/11 08:57
1
Acetone
0.0046 U
0.025
0.0046 mg/L
06/09/11 08:57
1
Benzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Bromoform
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Bromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Carbon disulfide
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Carbon tetrachloride
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chlorobenzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chlorobromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chlorodibromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
cis-1,2-Dichloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
cis-1,3-Dichloropropene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chloroethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chloroform
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Chloromethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Dibromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Dichlorobromomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Ethylbenzene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Ethylene Dibromide
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Iodomethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
m-Xylene & p-Xylene
0.0010 U
0.0020
0.0010 mg/L
06/09/11 08:57
1
2-Butanone (MEK)
0.0010 U
0.010
0.0010 mg/L
06/09/11 08:57
1
Methylene Chloride
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
4-Methyl-2-pentanone (MIBK)
0.0010 U
0.010
0.0010 mg/L
06/09/11 08:57
1
o-Xylene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Styrene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Tetrachloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Toluene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
trans-1,2-Dichloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
trans-1,3-Dichloropropene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
trans-1,4-Dichloro-2-butene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Trichloroethene
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Trichlorofluoromethane
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Vinyl acetate
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Vinyl chloride
0.0010 U
0.0010
0.0010 mg/L
06/09/11 08:57
1
Xylenes, Total
0.0010 U
0.0030
0.0010 mg/L
06/09/11 08:57
1
D
Prepared
Analyzed
Dil Fac
TestAmerica Tallahassee
Page 13 of 32
06/15/2011
4 5 6 7 8 9 10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)
3
Lab Sample ID: LCS 700-101524/3 Matrix: Solid Analysis Batch: 101524
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
LCS LCS
Added
Result Qualifier
Unit
1,1,1,2-Tetrachloroethane
0.0250
0.0209
mg/L
84
70 - 130
1,1,1-Trichloroethane
0.0250
0.0205
mg/L
82
70 - 130
1,1,2-Trichloroethane
0.0250
0.0240
mg/L
96
70 - 130
1,1,2,2-Tetrachloroethane
0.0250
0.0225
mg/L
90
70 - 130
1,1-Dichloroethane
0.0250
0.0276
mg/L
111
70 - 130
1,1-Dichloroethene
0.0250
0.0197
mg/L
79
56 - 146
1,2-Dichlorobenzene
0.0250
0.0235
mg/L
94
70 - 130
1,2-Dichloroethane
0.0250
0.0218
mg/L
87
67 - 136
1,2-Dichloropropane
0.0250
0.0246
mg/L
98
70 - 130
1,4-Dichlorobenzene
0.0250
0.0236
mg/L
95
70 - 130
0.100
0.0778
mg/L
78
50 - 150
Acetone
0.100
0.0926
mg/L
93
50 - 150
Benzene
0.0250
0.0252
mg/L
101
68 - 135
Bromoform
0.0250
0.0159 J
mg/L
63
64 - 131
Bromomethane
0.0250
0.0217
mg/L
87
50 - 130
Carbon disulfide
D
% Rec
Limits
0.100
0.0746
mg/L
75
50 - 150
Carbon tetrachloride
0.0250
0.0197
mg/L
79
50 - 135
Chlorobenzene
0.0250
0.0235
mg/L
94
71 - 132
Chlorobromomethane
0.0250
0.0248
mg/L
99
50 - 130
Chlorodibromomethane
0.0250
0.0214
mg/L
86
50 - 130
cis-1,2-Dichloroethene
0.0250
0.0235
mg/L
94
50 - 130
cis-1,3-Dichloropropene
0.0250
0.0208
mg/L
83
50 - 130
Chloroethane
0.0250
0.0173
mg/L
69
61 - 115
Chloroform
0.0250
0.0257
mg/L
103
64 - 131
Chloromethane
0.0250
0.0157
mg/L
63
63 - 125
Dibromomethane
0.0250
0.0230
mg/L
92
50 - 130
Dichlorobromomethane
0.0250
0.0230
mg/L
92
70 - 130
Ethylbenzene
0.0250
0.0238
mg/L
95
50 - 150
Ethylene Dibromide
0.0250
0.0230
mg/L
92
50 - 130
0.100
0.0994
mg/L
99
50 - 150
0.0500
0.0524
mg/L
105
70 - 130
2-Butanone (MEK)
0.100
0.0990
mg/L
99
45 - 139
Methylene Chloride
0.0250
0.0266
mg/L
107
70 - 130
0.100
0.0767
mg/L
77
50 - 150
o-Xylene
0.0250
0.0231
mg/L
93
70 - 130
Styrene
0.0250
0.0213
mg/L
85
70 - 130
Tetrachloroethene
0.0250
0.0224
mg/L
90
51 - 154
Toluene
0.0250
0.0247
mg/L
99
70 - 130
trans-1,2-Dichloroethene
0.0250
0.0269
mg/L
107
50 - 130
trans-1,3-Dichloropropene
0.0250
0.0186
mg/L
74
50 - 130
Trichloroethene
0.0250
0.0226
mg/L
91
67 - 132
Trichlorofluoromethane
0.0250
0.0147
mg/L
59
50 - 130
Vinyl acetate
0.100
0.0562
mg/L
56
50 - 150
Vinyl chloride
0.0250
0.0145
mg/L
58
55 - 142
Iodomethane m-Xylene & p-Xylene
4-Methyl-2-pentanone (MIBK)
6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 14 of 32
4 5
% Rec.
Analyte
2-Hexanone
1
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: LCSD 700-101524/4 Matrix: Solid Analysis Batch: 101524
3 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA
Spike
LCSD LCSD
% Rec.
Analyte
Added
Result Qualifier
Unit
1,1,1,2-Tetrachloroethane
0.0250
0.0216
mg/L
87
1,1,1-Trichloroethane
0.0250
0.0202
mg/L
81
1,1,2-Trichloroethane
0.0250
0.0250
mg/L
1,1,2,2-Tetrachloroethane
0.0250
0.0232
mg/L
1,1-Dichloroethane
0.0250
0.0281
1,1-Dichloroethene
0.0250
0.0198
1,2-Dichlorobenzene
0.0250
1,2-Dichloroethane
0.0250
1,2-Dichloropropane 1,4-Dichlorobenzene
Limit
70 - 130
3
30
70 - 130
1
30
100
70 - 130
4
30
93
70 - 130
3
30
mg/L
112
70 - 130
2
30
mg/L
79
56 - 146
0
30
0.0246
mg/L
99
70 - 130
5
30
0.0221
mg/L
88
67 - 136
1
23
0.0250
0.0257
mg/L
103
70 - 130
4
30
0.0250
0.0243
mg/L
97
70 - 130
3
30
0.100
0.0874
mg/L
87
50 - 150
12
30
Acetone
0.100
0.0957
mg/L
96
50 - 150
3
30
Benzene
0.0250
0.0252
mg/L
101
68 - 135
0
37
Bromoform
0.0250
0.0177
mg/L
71
64 - 131
11
30
Bromomethane
0.0250
0.0220
mg/L
88
50 - 130
1
30
Carbon disulfide
D
% Rec
Limits
RPD RPD
2-Hexanone
0.100
0.0771
mg/L
77
50 - 150
3
30
Carbon tetrachloride
0.0250
0.0194
mg/L
78
50 - 135
1
38
Chlorobenzene
0.0250
0.0228
mg/L
91
71 - 132
3
22
Chlorobromomethane
0.0250
0.0259
mg/L
104
50 - 130
4
30
Chlorodibromomethane
0.0250
0.0227
mg/L
91
50 - 130
6
30
cis-1,2-Dichloroethene
0.0250
0.0240
mg/L
96
50 - 130
2
30
cis-1,3-Dichloropropene
0.0250
0.0219
mg/L
87
50 - 130
5
30
Chloroethane
0.0250
0.0174
mg/L
69
61 - 115
1
30
Chloroform
0.0250
0.0266
mg/L
106
64 - 131
3
20
Chloromethane
0.0250
0.0159
mg/L
63
63 - 125
1
30
Dibromomethane
0.0250
0.0234
mg/L
93
50 - 130
2
30
Dichlorobromomethane
0.0250
0.0236
mg/L
95
70 - 130
3
30
Ethylbenzene
0.0250
0.0241
mg/L
96
50 - 150
1
30
Ethylene Dibromide
0.0250
0.0245
mg/L
98
50 - 130
6
30
0.100
0.105
mg/L
105
50 - 150
6
30
0.0500
0.0530
mg/L
106
70 - 130
1
30
2-Butanone (MEK)
0.100
0.108
mg/L
108
45 - 139
9
31
Methylene Chloride
0.0250
0.0281
mg/L
113
70 - 130
6
30
0.100
0.0786
mg/L
79
50 - 150
2
30
o-Xylene
0.0250
0.0237
mg/L
95
70 - 130
2
30
Styrene
0.0250
0.0221
mg/L
88
70 - 130
4
30
Tetrachloroethene
0.0250
0.0229
mg/L
91
51 - 154
2
24
Toluene
0.0250
0.0256
mg/L
102
70 - 130
3
30
trans-1,2-Dichloroethene
0.0250
0.0281
mg/L
112
50 - 130
4
30
trans-1,3-Dichloropropene
0.0250
0.0197
mg/L
79
50 - 130
6
30
Trichloroethene
0.0250
0.0236
mg/L
94
67 - 132
4
35
Trichlorofluoromethane
0.0250
0.0146
mg/L
58
50 - 130
1
30
Vinyl acetate
0.100
0.0606
mg/L
61
50 - 150
8
30
Vinyl chloride
0.0250
0.0143
mg/L
57
55 - 142
1
21
Iodomethane m-Xylene & p-Xylene
4-Methyl-2-pentanone (MIBK)
1
TestAmerica Tallahassee
Page 15 of 32
06/15/2011
4 5 6 7 8 9 10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)
3
Lab Sample ID: MRL 700-101524/5 MRL Matrix: Solid Analysis Batch: 101524
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Analyte
Added
MRL MRL Result Qualifier
D
% Rec
Limits
0.00100
0.00199 I
mg/L
199
1 - 150
Bromoform
0.00100
0.000750 I
mg/L
75
50 - 150
trans-1,2-Dichloroethene
0.00100
0.00139
mg/L
139
50 - 150
trans-1,4-Dichloro-2-butene
0.00100
0.000647 I
mg/L
65
1 - 150
Lab Sample ID: 640-33835-3 MS Matrix: Solid Analysis Batch: 101524
6 7
Client Sample ID: OWCB-P Prep Type: TCLP Sample Sample Result Qualifier
Spike Added
MS MS Result Qualifier
8 9
% Rec. Unit
1,1,1,2-Tetrachloroethane
0.10 U
2.50
2.37
mg/L
1,1,1-Trichloroethane
0.10 U
2.50
2.20
1,1,2-Trichloroethane
0.10 U
2.50
2.71
1,1,2,2-Tetrachloroethane
0.10 U
2.50
1,1-Dichloroethane
0.10 U
2.50
1,2,3-Trichloropropane
0.10 U
1,1-Dichloroethene
0.10 U
1,2-Dibromo-3-Chloropropane 1,2-Dichlorobenzene
D
% Rec
10
Limits
95
70 - 130
mg/L
88
50 - 150
mg/L
108
50 - 130
2.68
mg/L
107
70 - 130
2.59
mg/L
104
50 - 130
2.50
2.03
mg/L
81
70 - 130
2.50
2.19
mg/L
87
56 - 146
0.10 U
2.50
2.06
mg/L
83
50 - 130
0.10 U
2.50
2.74
mg/L
110
70 - 130
1,2-Dichloroethane
0.10 U
2.50
2.62
mg/L
105
67 - 136
1,2-Dichloropropane
0.10 U
2.50
2.58
mg/L
103
70 - 130
1,4-Dichlorobenzene
0.10 U
2.50
2.61
mg/L
104
50 - 130
2-Hexanone
0.10 U
10.0
9.46
mg/L
95
50 - 130
Acrylonitrile
0.10 U
25.0
29.0
mg/L
116
70 - 130
Acetone
0.46 U
10.0
10.9
mg/L
109
70 - 130
Benzene
0.10 U
2.50
2.65
mg/L
106
68 - 135
Bromoform
0.10 U J
2.50
1.95
mg/L
78
64 - 131
Bromomethane
0.10 U
2.50
1.17 J
mg/L
47
70 - 130
Carbon disulfide
0.10 U
10.0
8.14
mg/L
81
50 - 150
Carbon tetrachloride
0.10 U
2.50
2.19
mg/L
88
50 - 150
Chlorobenzene
0.10 U
2.50
2.52
mg/L
101
71 - 132
Chlorobromomethane
0.10 U
2.50
2.49
mg/L
99
70 - 130
Chlorodibromomethane
0.10 U
2.50
2.39
mg/L
96
70 - 130
cis-1,2-Dichloroethene
0.10 U
2.50
2.14
mg/L
86
50 - 130
cis-1,3-Dichloropropene
0.10 U
2.50
1.98
mg/L
79
50 - 130
Chloroethane
0.10 U
2.50
1.91
mg/L
76
61 - 115
Chloroform
0.10 U
2.50
2.53
mg/L
101
64 - 131
Chloromethane
0.10 U
2.50
1.48 J
mg/L
59
63 - 125
Dibromomethane
0.10 U
2.50
2.57
mg/L
103
70 - 130
Dichlorobromomethane
0.10 U
2.50
2.53
mg/L
101
70 - 130
Ethylbenzene
0.10 U
2.50
2.58
mg/L
103
50 - 130
Ethylene Dibromide
0.10 U
2.50
2.61
mg/L
104
70 - 130
Iodomethane
0.10 U
10.0
9.74
mg/L
97
50 - 130
m-Xylene & p-Xylene
0.10 U
5.00
5.63
mg/L
113
70 - 130
2-Butanone (MEK)
0.16 I
10.0
10.5
mg/L
104
45 - 139
Methylene Chloride
0.10 U
2.50
2.61
mg/L
104
50 - 130
4-Methyl-2-pentanone (MIBK)
0.10 U
10.0
9.21
mg/L
92
50 - 150
o-Xylene
0.10 U
2.50
2.45
mg/L
98
70 - 130
Styrene
0.10 U
2.50
2.31
mg/L
92
50 - 130
Tetrachloroethene
0.10 U
2.50
2.33
mg/L
93
51 - 154
11 12 13
TestAmerica Tallahassee
Page 16 of 32
4 5
% Rec. Unit
1,2-Dibromo-3-Chloropropane
Analyte
1
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: 640-33835-3 MS Matrix: Solid Analysis Batch: 101524
Client Sample ID: OWCB-P Prep Type: TCLP Sample Sample
Analyte
Result Qualifier
Spike Added
MS MS Result Qualifier
% Rec. Unit
D
% Rec
0.10 U
2.50
2.69
mg/L
108
70 - 130
trans-1,2-Dichloroethene
0.10 U
2.50
2.59
mg/L
104
50 - 130
trans-1,3-Dichloropropene
0.10 U
2.50
1.87
mg/L
75
50 - 130
Trichloroethene
0.10 U
2.50
2.45
mg/L
98
67 - 132
Trichlorofluoromethane
0.10 U
2.50
1.62
mg/L
65
50 - 130
Vinyl acetate
0.10 U
10.0
6.61
mg/L
66
50 - 130
Vinyl chloride
0.10 U
2.50
1.55
mg/L
62
55 - 142
Lab Sample ID: 640-33835-3 MSD Matrix: Solid Analysis Batch: 101524 Result Qualifier
Spike Added
MSD MSD Result Qualifier
7 8
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
1,1,1,2-Tetrachloroethane
0.10 U
2.50
2.31
mg/L
92
70 - 130
3
30
1,1,1-Trichloroethane
0.10 U
2.50
2.24
mg/L
89
50 - 150
1
30
1,1,2-Trichloroethane
0.10 U
2.50
2.66
mg/L
107
50 - 130
2
30
1,1,2,2-Tetrachloroethane
0.10 U
2.50
2.63
mg/L
105
70 - 130
2
30
1,1-Dichloroethane
0.10 U
2.50
2.91
mg/L
116
50 - 130
12
30
1,2,3-Trichloropropane
0.10 U
2.50
2.09
mg/L
84
70 - 130
3
30
1,1-Dichloroethene
0.10 U
2.50
2.13
mg/L
85
56 - 146
3
30
1,2-Dibromo-3-Chloropropane
0.10 U
2.50
2.27
mg/L
91
50 - 130
10
30
1,2-Dichlorobenzene
0.10 U
2.50
2.51
mg/L
100
70 - 130
9
30
1,2-Dichloroethane
0.10 U
2.50
2.55
mg/L
102
67 - 136
3
23
1,2-Dichloropropane
0.10 U
2.50
2.45
mg/L
98
70 - 130
5
30
1,4-Dichlorobenzene
0.10 U
2.50
2.48
mg/L
99
50 - 130
5
30
2-Hexanone
0.10 U
10.0
9.64
mg/L
96
50 - 130
2
30
Acrylonitrile
0.10 U
25.0
33.2 J
mg/L
133
70 - 130
13
30
Acetone
0.46 U
10.0
10.5
mg/L
105
70 - 130
3
30
Benzene
0.10 U
2.50
2.70
mg/L
108
68 - 135
2
37
Bromoform
0.10 U J
2.50
1.82
mg/L
73
64 - 131
7
30
Bromomethane
0.10 U
2.50
1.27 J
mg/L
51
70 - 130
8
30
Carbon disulfide
0.10 U
10.0
8.11
mg/L
81
50 - 150
0
30
Carbon tetrachloride
0.10 U
2.50
2.18
mg/L
87
50 - 150
0
38
Chlorobenzene
0.10 U
2.50
2.54
mg/L
102
71 - 132
1
22
Chlorobromomethane
0.10 U
2.50
2.60
mg/L
104
70 - 130
5
30
Chlorodibromomethane
0.10 U
2.50
2.33
mg/L
93
70 - 130
3
30
cis-1,2-Dichloroethene
0.10 U
2.50
2.29
mg/L
92
50 - 130
7
30
cis-1,3-Dichloropropene
0.10 U
2.50
2.05
mg/L
82
50 - 130
4
30
Chloroethane
0.10 U
2.50
1.82
mg/L
73
61 - 115
5
30
Chloroform
0.10 U
2.50
2.66
mg/L
107
64 - 131
5
20
Chloromethane
0.10 U
2.50
1.54 J
mg/L
62
63 - 125
4
30
Dibromomethane
0.10 U
2.50
2.44
mg/L
98
70 - 130
5
30
Dichlorobromomethane
0.10 U
2.50
2.44
mg/L
98
70 - 130
4
30
Ethylbenzene
0.10 U
2.50
2.58
mg/L
103
50 - 130
0
30
Ethylene Dibromide
0.10 U
2.50
2.59
mg/L
104
70 - 130
1
30
Iodomethane
0.10 U
10.0
10.4
mg/L
104
50 - 130
7
30
m-Xylene & p-Xylene
0.10 U
5.00
5.47
mg/L
109
70 - 130
3
30
2-Butanone (MEK)
0.16 I
10.0
11.5
mg/L
114
45 - 139
9
31
Methylene Chloride
0.10 U
2.50
2.83
mg/L
113
50 - 130
8
30
4-Methyl-2-pentanone (MIBK)
0.10 U
10.0
8.66
mg/L
87
50 - 150
6
30
TestAmerica Tallahassee
Page 17 of 32
4 6
Client Sample ID: OWCB-P Prep Type: TCLP Sample Sample
3 5
Limits
Toluene
Analyte
1
06/15/2011
9 10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued) Lab Sample ID: 640-33835-3 MSD Matrix: Solid Analysis Batch: 101524
Client Sample ID: OWCB-P Prep Type: TCLP Sample Sample
Analyte
Result Qualifier
Spike Added
MSD MSD Result Qualifier
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
o-Xylene
0.10 U
2.50
2.46
mg/L
98
70 - 130
0
30
Styrene
0.10 U
2.50
2.29
mg/L
92
50 - 130
1
30
Tetrachloroethene
0.10 U
2.50
2.38
mg/L
95
51 - 154
2
24
Toluene
0.10 U
2.50
2.60
mg/L
104
70 - 130
3
30
trans-1,2-Dichloroethene
0.10 U
2.50
2.89
mg/L
116
50 - 130
11
30
trans-1,3-Dichloropropene
0.10 U
2.50
1.86
mg/L
74
50 - 130
1
30
Trichloroethene
0.10 U
2.50
2.53
mg/L
101
67 - 132
3
35
Trichlorofluoromethane
0.10 U
2.50
1.59
mg/L
63
50 - 130
2
30
Vinyl acetate
0.10 U
10.0
7.15
mg/L
72
50 - 130
8
30
Vinyl chloride
0.10 U
2.50
1.59
mg/L
63
55 - 142
2
21
Lab Sample ID: LCS 700-101541/2-A Matrix: Solid Analysis Batch: 101639
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 101541 Spike
Analyte
3 4 5 6 7 8 9 10 11
Method: 6010C - Metals (ICP)
Added
LCS LCS Result Qualifier
% Rec. Unit
D
% Rec
Limits
Silver
5.00
5.34
mg/L
107
80 - 120
Arsenic
5.00
5.19
mg/L
104
80 - 120
Barium
5.00
5.27
mg/L
105
80 - 120
Beryllium
5.00
5.47
mg/L
109
80 - 120
Cadmium
5.00
5.10
mg/L
102
80 - 120
Cobalt
5.00
5.08
mg/L
102
80 - 120
Chromium
5.00
5.06
mg/L
101
80 - 120
Copper
5.00
5.12
mg/L
102
80 - 120
Nickel
5.00
5.10
mg/L
102
80 - 120
Lead
5.00
5.12
mg/L
102
80 - 120
Antimony
5.00
5.06
mg/L
101
80 - 120
Selenium
5.00
5.29
mg/L
106
80 - 120
Thallium
5.00
5.13
mg/L
103
80 - 120
Vanadium
5.00
5.24
mg/L
105
80 - 120
Zinc
5.00
5.24
mg/L
105
80 - 120
Lab Sample ID: LCSD 700-101541/3-A Matrix: Solid Analysis Batch: 101639
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 101541 Spike
Analyte
1
Added
LCSD LCSD Result Qualifier
% Rec. Unit
D
% Rec
Limits
RPD RPD
Limit
Silver
5.00
5.32
mg/L
106
80 - 120
0
20
Arsenic
5.00
5.18
mg/L
104
80 - 120
0
20
Barium
5.00
5.20
mg/L
104
80 - 120
1
20
Beryllium
5.00
5.45
mg/L
109
80 - 120
0
20
Cadmium
5.00
5.06
mg/L
101
80 - 120
1
20
Cobalt
5.00
5.02
mg/L
100
80 - 120
1
20
Chromium
5.00
5.00
mg/L
100
80 - 120
1
20
Copper
5.00
5.10
mg/L
102
80 - 120
0
20
Nickel
5.00
5.08
mg/L
102
80 - 120
0
20
Lead
5.00
5.06
mg/L
101
80 - 120
1
20
Antimony
5.00
5.04
mg/L
101
80 - 120
0
20
TestAmerica Tallahassee
Page 18 of 32
06/15/2011
12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 6010C - Metals (ICP) (Continued) Lab Sample ID: LCSD 700-101541/3-A Matrix: Solid Analysis Batch: 101639
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 101541 LCSD LCSD
Spike Analyte
Added
Result Qualifier
% Rec. Unit
D
% Rec
RPD
Limits
RPD
Limit
Selenium
5.00
5.26
mg/L
105
80 - 120
1
20
Thallium
5.00
5.12
mg/L
102
80 - 120
0
20
Vanadium
5.00
5.24
mg/L
105
80 - 120
0
20
Zinc
5.00
5.18
mg/L
104
80 - 120
1
20
Lab Sample ID: LB 700-101438/1-B LB Matrix: Solid Analysis Batch: 101639
Client Sample ID: Method Blank Prep Type: TCLP Prep Batch: 101541 LB LB
Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Arsenic
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Barium
0.50 U
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 10:38
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 10:38
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Copper
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Result Qualifier
D
Dil Fac
Nickel
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:38
1
Lead
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Selenium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
Vanadium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:38
1
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:38
1
Zinc
Lab Sample ID: LB2 700-101438/2-B LB2 Matrix: Solid Analysis Batch: 101639
Client Sample ID: Method Blank Prep Type: TCLP Prep Batch: 101541 LB2 LB2
Analyte
PQL
MDL Unit
Prepared
Analyzed
Silver
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Arsenic
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Barium
0.50 U
0.80
0.50 mg/L
06/09/11 12:05
06/10/11 10:56
1
Beryllium
0.025 U
0.20
0.025 mg/L
06/09/11 12:05
06/10/11 10:56
1
Cadmium
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Cobalt
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Chromium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Copper
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Nickel
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:56
1
Lead
0.050 U
0.20
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Antimony
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Selenium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Thallium
0.050 U
0.50
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
Vanadium
0.050 U
0.25
0.050 mg/L
06/09/11 12:05
06/10/11 10:56
1
0.10 U
2.5
0.10 mg/L
06/09/11 12:05
06/10/11 10:56
1
Zinc
1
Result Qualifier
D
Dil Fac
TestAmerica Tallahassee
Page 19 of 32
06/15/2011
3 4 5 6 7 8 9 10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: 1664A - HEM and SGT-HEM
3
Lab Sample ID: MB 700-101773/1-A Matrix: Water Analysis Batch: 101774
Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 101773 MB MB
Analyte
PQL
Result Qualifier
HEM (Oil & Grease)
3.5 U
MDL Unit
5.3
D
3.5 mg/L
Lab Sample ID: LCS 700-101773/2-A Matrix: Water Analysis Batch: 101774
Prepared
Analyzed
Dil Fac
06/14/11 08:30
06/14/11 08:30
1
Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 101773 LCS LCS
Spike Analyte
Added
HEM (Oil & Grease)
Result Qualifier
42.1
43.8
Lab Sample ID: LCSD 700-101773/3-A Matrix: Water Analysis Batch: 101774
% Rec. Unit
D
mg/L
% Rec
104
LCSD LCSD
Analyte
Added
HEM (Oil & Grease)
Result Qualifier
42.1
42.9
D
mg/L
% Rec
102
RPD
Limits
RPD
Limit
2
18
79 - 114
Lab Sample ID: MB 640-81587/1 Matrix: Water Analysis Batch: 81587
Client Sample ID: Method Blank Prep Type: Total/NA MB MB Result Qualifier
0.50 U
PQL
MDL Unit
0.50
0.50 NTU
D
Prepared
Added
Turbidity
40.0
LCS LCS Result Qualifier
40.0
Lab Sample ID: LCSD 640-81587/3 Matrix: Water Analysis Batch: 81587
1
% Rec. Unit
D
NTU
% Rec
100
Limits
90 - 110
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike
Analyte
Added
Turbidity
40.0
LCSD LCSD Result Qualifier
40.0
% Rec. Unit
D
NTU
% Rec
100
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 81587
Limits
90 - 110
RPD RPD
Limit
0
30
Client Sample ID: OWCB-P Prep Type: Total/NA Sample Sample
Turbidity
Dil Fac
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Analyte
Analyzed
06/05/11 12:45
Lab Sample ID: LCS 640-81587/2 Matrix: Water Analysis Batch: 81587 Analyte
Result Qualifier
420
6 7 8 10 11 12 13
Method: 180.1 - Turbidity, Nephelometric
Turbidity
5
9
79 - 114
% Rec. Unit
4
Limits
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 101773 Spike
Analyte
1
DU DU Result Qualifier
421
RPD Unit
NTU
D
RPD
Limit
0
30
TestAmerica Tallahassee
Page 20 of 32
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: SM 2540C - Solids, Total Dissolved (TDS)
3
Lab Sample ID: MB 640-81646/1 Matrix: Water Analysis Batch: 81646
Client Sample ID: Method Blank Prep Type: Total/NA MB MB
Analyte
PQL
Result Qualifier
Total Dissolved Solids
2.3 U
MDL Unit
5.0
D
Prepared
2.3 mg/L
Analyzed
Dil Fac
06/07/11 10:15
Lab Sample ID: LCS 640-81646/2 Matrix: Water Analysis Batch: 81646
1
Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS
Spike Analyte
Added
Total Dissolved Solids
Result Qualifier
300
293
D
% Rec
98
LCSD LCSD
Analyte
Added
Total Dissolved Solids
Result Qualifier
300
282
D
mg/L
% Rec
94
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 81646
RPD
Limits
RPD
Limit
4
25
80 - 120
Client Sample ID: OWCB-P Prep Type: Total/NA DU DU
Sample Sample
RPD
Analyte
Result Qualifier
Result Qualifier
Unit
Total Dissolved Solids
12000
12400
mg/L
D
RPD
Limit
0.6
25
Method: SM 2540D - Solids, Total Suspended (TSS) Lab Sample ID: MB 640-81644/1 Matrix: Water Analysis Batch: 81644
Client Sample ID: Method Blank Prep Type: Total/NA MB MB
Total Suspended Solids
PQL
Result Qualifier
1.2 U
MDL Unit
2.0
D
Added
100
LCS LCS Result Qualifier
87.0
Lab Sample ID: LCSD 640-81644/3 Matrix: Water Analysis Batch: 81644
Total Suspended Solids
1
% Rec. Unit
D
mg/L
% Rec
87
Limits
80 - 120
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike
Analyte
Dil Fac
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Total Suspended Solids
Analyzed
06/07/11 10:09
Lab Sample ID: LCS 640-81644/2 Matrix: Water Analysis Batch: 81644 Analyte
Prepared
1.2 mg/L
Added
100
LCSD LCSD Result Qualifier
97.5
% Rec. Unit
mg/L
D
% Rec
98
Limits
80 - 120
RPD RPD
Limit
11
25
TestAmerica Tallahassee
Page 21 of 32
6 7 9
80 - 120
% Rec. Unit
5
Limits
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike
4
8
% Rec. Unit
mg/L
Lab Sample ID: LCSD 640-81646/3 Matrix: Water Analysis Batch: 81646
Analyte
1
06/15/2011
10 11 12 13
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: SM 2710F - Specific Gravity, Density
3
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 101470
Client Sample ID: OWCB-P Prep Type: Total/NA DU DU
Sample Sample Analyte
Result Qualifier
Specific Gravity
1.0008
Result Qualifier
1.00
RPD Unit
D
NONE
RPD
Limit
0.4
20
Method: SM 4500 Cl G - Chlorine, Residual Client Sample ID: Method Blank Prep Type: Total/NA
Result Qualifier
0.043 U
PQL
MDL Unit
0.10
0.043 mg/L
D
Prepared
Added
Chlorine, Total Residual
1.00
LCS LCS Result Qualifier
0.930
Lab Sample ID: LCSD 700-101464/3 Matrix: Water Analysis Batch: 101464 Spike Added
Chlorine, Total Residual
1.00
Unit
D
mg/L
93
LCSD LCSD Result Qualifier
Result Qualifier
0.42 Q
Result Qualifier
0.42 Q
0.900
D
mg/L
Chlorine, Total Residual
% Rec
90
Spike Added
0.264
MS MS Result Qualifier
Limits
90 - 110
RPD RPD
Limit
3.3
10.0
0.690
% Rec. Unit
D
mg/L
% Rec
102
Spike Added
0.264
MSD MSD Result Qualifier
Limits
90 - 110
0.690
% Rec. Unit
D
mg/L
% Rec
102
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 101464
Limits
90 - 110
RPD RPD
Limit
0.0
10.0
Client Sample ID: OWCB-P Prep Type: Total/NA Sample Sample Result Qualifier
0.42 Q
8
DU DU Result Qualifier
0.390
RPD Unit
mg/L
D
RPD
Limit
7
TestAmerica Tallahassee
Page 22 of 32
10 11 13
Client Sample ID: OWCB-P Prep Type: Total/NA Sample Sample
Analyte
Limits
90 - 110
% Rec. Unit
Lab Sample ID: 640-33835-4 MSD Matrix: Solid Analysis Batch: 101464
Chlorine, Total Residual
% Rec
Client Sample ID: OWCB-P Prep Type: Total/NA Sample Sample
6
12
% Rec.
Lab Sample ID: 640-33835-4 MS Matrix: Solid Analysis Batch: 101464
Analyte
1
Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA
Analyte
Chlorine, Total Residual
Dil Fac
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Analyte
Analyzed
06/07/11 10:00
Lab Sample ID: LCS 700-101464/2 Matrix: Water Analysis Batch: 101464 Analyte
5
9
MB MB
Chlorine, Total Residual
4
7
Lab Sample ID: MB 700-101464/1 Matrix: Water Analysis Batch: 101464 Analyte
1
06/15/2011
QC Sample Results Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
2
Method: SM 4500 H+ B - pH
3
Lab Sample ID: LCS 640-81609/1 Matrix: Water Analysis Batch: 81609
Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike
Analyte
Added
pH
9.22
LCS LCS Result Qualifier
9.200
D
SU
Sample Sample
pH
Result Qualifier
6.72 Q
% Rec
100
Limits
90 - 110
6
Client Sample ID: OWCB-P Prep Type: Total/NA
7
RPD
8
DU DU Result Qualifier
6.750
Unit
SU
D
4 5
% Rec. Unit
Lab Sample ID: 640-33835-4 DU Matrix: Solid Analysis Batch: 81609 Analyte
1
RPD
Limit
0.4
40
9 10 11 12 13
TestAmerica Tallahassee
Page 23 of 32
06/15/2011
QC Association Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
GC/MS VOA
3
Leach Batch: 101440 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
640-33835-3
OWCB-P
TCLP
Solid
1311
640-33835-3 MS
OWCB-P
TCLP
Solid
1311
640-33835-3 MSD
OWCB-P
TCLP
Solid
1311
640-33835-2
MCWB-E
TCLP
Solid
1311
640-33835-1
MCWB-W
TCLP
Solid
1311
Prep Batch
4 5 6 7
Analysis Batch: 101524 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 700-101524/3
Lab Control Sample
Total/NA
Solid
8260C
LCSD 700-101524/4
Lab Control Sample Dup
Total/NA
Solid
8260C
MRL 700-101524/5 MRL
Lab Control Sample
Total/NA
Solid
8260C
MB 700-101524/6
Method Blank
Total/NA
Solid
8260C
640-33835-1
MCWB-W
TCLP
Solid
8260C
640-33835-2
MCWB-E
TCLP
Solid
8260C
640-33835-3
OWCB-P
TCLP
Solid
8260C
640-33835-3 MS
OWCB-P
TCLP
Solid
8260C
640-33835-3 MSD
OWCB-P
TCLP
Solid
8260C
Prep Batch
8 9 10 11 12 13
Metals Leach Batch: 101438 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LB 700-101438/1-B LB
Method Blank
TCLP
Solid
1311
Prep Batch
LB2 700-101438/2-B LB2
Method Blank
TCLP
Solid
1311
640-33835-1
MCWB-W
TCLP
Solid
1311
640-33835-2
MCWB-E
TCLP
Solid
1311
640-33835-3
OWCB-P
TCLP
Solid
1311
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 700-101541/2-A
Lab Control Sample
Total/NA
Solid
3010A
LCSD 700-101541/3-A
Lab Control Sample Dup
Total/NA
Solid
3010A
LB 700-101438/1-B LB
Method Blank
TCLP
Solid
3010A
101438
640-33835-1
MCWB-W
TCLP
Solid
3010A
101438
640-33835-2
MCWB-E
TCLP
Solid
3010A
101438
LB2 700-101438/2-B LB2
Method Blank
TCLP
Solid
3010A
101438
640-33835-3
OWCB-P
TCLP
Solid
3010A
101438
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 700-101541/2-A
Lab Control Sample
Total/NA
Solid
6010C
101541
LCSD 700-101541/3-A
Lab Control Sample Dup
Total/NA
Solid
6010C
101541
LB 700-101438/1-B LB
Method Blank
TCLP
Solid
6010C
101541
640-33835-1
MCWB-W
TCLP
Solid
6010C
101541
640-33835-2
MCWB-E
TCLP
Solid
6010C
101541
LB2 700-101438/2-B LB2
Method Blank
TCLP
Solid
6010C
101541
640-33835-3
OWCB-P
TCLP
Solid
6010C
101541
Prep Batch: 101541 Prep Batch
Analysis Batch: 101639 Prep Batch
TestAmerica Tallahassee
Page 24 of 32
06/15/2011
QC Association Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
General Chemistry
3
Analysis Batch: 81587 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 640-81587/1
Method Blank
Total/NA
Water
180.1
LCS 640-81587/2
Lab Control Sample
Total/NA
Water
180.1
LCSD 640-81587/3
Lab Control Sample Dup
Total/NA
Water
180.1
640-33835-4
OWCB-P
Total/NA
Water
180.1
640-33835-4 DU
OWCB-P
Total/NA
Solid
180.1
Prep Batch
4 5 6 7
Analysis Batch: 81609 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 640-81609/1
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
640-33835-4
OWCB-P
Total/NA
Water
SM 4500 H+ B
640-33835-4 DU
OWCB-P
Total/NA
Solid
SM 4500 H+ B
Prep Batch
8 9 10
Analysis Batch: 81644 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 640-81644/1
Method Blank
Total/NA
Water
SM 2540D
LCS 640-81644/2
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 640-81644/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
640-33835-4
OWCB-P
Total/NA
Water
SM 2540D
Prep Batch
11 12 13
Analysis Batch: 81646 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 640-81646/1
Method Blank
Total/NA
Water
SM 2540C
LCS 640-81646/2
Lab Control Sample
Total/NA
Water
SM 2540C
LCSD 640-81646/3
Lab Control Sample Dup
Total/NA
Water
SM 2540C
640-33835-4
OWCB-P
Total/NA
Water
SM 2540C
640-33835-4 DU
OWCB-P
Total/NA
Solid
SM 2540C
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 700-101464/1
Method Blank
Total/NA
Water
SM 4500 Cl G
LCS 700-101464/2
Lab Control Sample
Total/NA
Water
SM 4500 Cl G
LCSD 700-101464/3
Lab Control Sample Dup
Total/NA
Water
SM 4500 Cl G
640-33835-4
OWCB-P
Total/NA
Water
SM 4500 Cl G
640-33835-4 DU
OWCB-P
Total/NA
Solid
SM 4500 Cl G
640-33835-4 MS
OWCB-P
Total/NA
Solid
SM 4500 Cl G
640-33835-4 MSD
OWCB-P
Total/NA
Solid
SM 4500 Cl G
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
LCS 700-101470/1
Lab Control Sample
Total/NA
Water
SM 2710F
LCSD 700-101470/2
Lab Control Sample Dup
Total/NA
Water
SM 2710F
640-33835-4
OWCB-P
Total/NA
Water
SM 2710F
640-33835-4 DU
OWCB-P
Total/NA
Solid
SM 2710F
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 700-101773/1-A
Method Blank
Total/NA
Water
1664A
LCS 700-101773/2-A
Lab Control Sample
Total/NA
Water
1664A
LCSD 700-101773/3-A
Lab Control Sample Dup
Total/NA
Water
1664A
640-33835-4
OWCB-P
Total/NA
Water
1664A
Prep Batch
Analysis Batch: 101464 Prep Batch
Analysis Batch: 101470 Prep Batch
Prep Batch: 101773 Prep Batch
TestAmerica Tallahassee
Page 25 of 32
06/15/2011
QC Association Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
General Chemistry (Continued)
3
Analysis Batch: 101774 Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
MB 700-101773/1-A
Method Blank
Total/NA
Water
1664A
Prep Batch
101773
LCS 700-101773/2-A
Lab Control Sample
Total/NA
Water
1664A
101773
LCSD 700-101773/3-A
Lab Control Sample Dup
Total/NA
Water
1664A
101773
640-33835-4
OWCB-P
Total/NA
Water
1664A
101773
4 5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 26 of 32
06/15/2011
Lab Chronicle Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
Client Sample ID: MCWB-W
Lab Sample ID: 640-33835-1
2
Date Collected: 06/03/11 13:30 Date Received: 06/04/11 10:05
Matrix: Solid
Batch
Batch
Prep Type
Type
Method
TCLP
Leach
1311
TCLP
Analysis
8260C
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010C
Run
Batch
Factor
Number
Or Analyzed
Analyst
Lab
101440
06/07/11 17:10
MEB
TAL MOB
101524
06/09/11 16:24
JB
TAL MOB
101438
06/07/11 17:04
MEB
TAL MOB
101541
06/09/11 12:05
MEB
TAL MOB
101639
06/10/11 10:45
ZST
TAL MOB
100
1
Prepared
Lab Sample ID: 640-33835-2
Date Collected: 06/03/11 13:50 Date Received: 06/04/11 10:05
Matrix: Solid
Batch
Batch
Type
Method
TCLP
Leach
1311
TCLP
Analysis
8260C
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010C
Run
Dilution
Batch
Factor
Number
Or Analyzed
101440 101524
100
1
Analyst
Lab
06/07/11 17:10
MEB
TAL MOB
06/09/11 16:48
JB
TAL MOB
101438
06/07/11 17:04
MEB
TAL MOB
101541
06/09/11 12:05
MEB
TAL MOB
101639
06/10/11 10:52
ZST
TAL MOB
Lab Sample ID: 640-33835-3
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Solid
Batch
Batch
Prep Type
Type
Method
Dilution
Batch
Factor
Number
Or Analyzed
TCLP
Leach
1311
Analyst
Lab
101440
06/07/11 17:10
MEB
TCLP
Analysis
8260C
TAL MOB
101524
06/09/11 17:13
JB
TAL MOB
TCLP
Leach
TCLP
Prep
1311
101438
06/07/11 17:04
MEB
TAL MOB
3010A
101541
06/09/11 12:05
MEB
TCLP
Analysis
6010C
TAL MOB
101639
06/10/11 11:00
ZST
TAL MOB
Run
100
1
Prepared
Client Sample ID: OWCB-P
Lab Sample ID: 640-33835-4
Date Collected: 06/03/11 14:15 Date Received: 06/04/11 10:05
Matrix: Water
Batch
Batch
Prep Type
Type
Method
Dilution
Batch
Factor
Number
Total/NA
Analysis
180.1
Analyst
Lab
16
81587
06/05/11 12:45
JS
TAL TAL
Total/NA
Analysis
SM 4500 H+ B
1
81609
06/06/11 14:00
JS
TAL TAL
Total/NA
Analysis
SM 2540D
1
81644
DA
TAL TAL
DA
TAL TAL
Run
Prepared Or Analyzed
(Start): 06/07/11 10:09 (End): 06/08/11 09:03 Total/NA
Analysis
SM 2540C
1
81646 (Start): 06/07/11 10:15 (End): 06/08/11 12:44
Total/NA
Analysis
SM 4500 Cl G
1
101464
06/07/11 10:00
JDP
TAL MOB
Total/NA
Analysis
SM 2710F
1
101470
06/08/11 12:10
TKN
TAL MOB
Total/NA
Analysis
1664A
1
101774
06/14/11 08:30
HPG
TAL MOB
Total/NA
Prep
1664A
101773
06/14/11 08:30
HPG
TAL MOB
TestAmerica Tallahassee
Page 27 of 32
5 6 7 8 9 10
Prepared
Client Sample ID: OWCB-P
3 4
Dilution
Client Sample ID: MCWB-E
Prep Type
1
06/15/2011
11 12 13
Lab Chronicle Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2 3
Laboratory References:
TAL MOB = TestAmerica Mobile, 900 Lakeside Drive, Mobile, AL 36693, TEL (251)666-6633 TAL TAL = TestAmerica Tallahassee, 2846 Industrial Plaza Drive, Tallahassee, FL 32301, TEL (850)878-3994
4 5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 28 of 32
06/15/2011
Certification Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Laboratory
Authority
Program
EPA Region
Certification ID
TestAmerica Tallahassee
Florida
NELAC
4
E81005
TestAmerica Tallahassee
Louisiana
NELAC
6
30663
TestAmerica Tallahassee
New Jersey
NELAC
2
FL012
TestAmerica Tallahassee
Oklahoma
State Program
6
9986
TestAmerica Tallahassee
Texas
NELAC
6
T104704459-11-2
TestAmerica Tallahassee
USDA
USDA
0
P330-08-00158
TestAmerica Mobile
Alabama
State Program
4
40030
TestAmerica Mobile
Arkansas
State Program
6
88-0765
TestAmerica Mobile
Florida
NELAC
4
E87089
TestAmerica Mobile
Georgia
State Program
4
952
TestAmerica Mobile
Louisiana
NELAC
6
LA0900026
TestAmerica Mobile
Louisiana
NELAC
6
30673
TestAmerica Mobile
Mississippi
State Program
4
N/A
TestAmerica Mobile
North Carolina
North Carolina DENR
4
395
TestAmerica Mobile
South Carolina
State Program
4
75002
TestAmerica Mobile
Tennessee
State Program
4
2979
TestAmerica Mobile
Texas
NELAC
6
T104704460-09A-TX
TestAmerica Mobile
USDA
USDA
0
P330-08-00039
TestAmerica Mobile
Washington
State Program
10
C1918
4 5 6 7 8 9 10 11 12 13
Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s current list of certified methods and analytes.
TestAmerica Tallahassee
Page 29 of 32
3
06/15/2011
Method Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Method
Method Description
Protocol
Laboratory
8260C
Volatile Organic Compounds by GC/MS
SW846
TAL MOB
6010C
Metals (ICP)
SW846
TAL MOB
1664A
HEM and SGT-HEM
1664A
TAL MOB
180.1
Turbidity, Nephelometric
MCAWW
TAL TAL
SM 2540C
Solids, Total Dissolved (TDS)
SM
TAL TAL
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL TAL
SM 2710F
Specific Gravity, Density
SM
TAL MOB
SM 4500 Cl G
Chlorine, Residual
SM
TAL MOB
SM 4500 H+ B
pH
SM
TAL TAL
3 4 5 6 7 8
Protocol References:
1664A = EPA-821-98-002
9
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater",
10
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
11
Laboratory References:
TAL MOB = TestAmerica Mobile, 900 Lakeside Drive, Mobile, AL 36693, TEL (251)666-6633
12
TAL TAL = TestAmerica Tallahassee, 2846 Industrial Plaza Drive, Tallahassee, FL 32301, TEL (850)878-3994
13
TestAmerica Tallahassee
Page 30 of 32
06/15/2011
Sample Summary Client: Golder Associates Inc. Project/Site: St. Johns Power Park
TestAmerica Job ID: 640-33835-1
1 2
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
640-33835-1
MCWB-W
Solid
06/03/11 13:30
06/04/11 10:05
640-33835-2
MCWB-E
Solid
06/03/11 13:50
06/04/11 10:05
640-33835-3
OWCB-P
Solid
06/03/11 14:15
06/04/11 10:05
640-33835-4
OWCB-P
Water
06/03/11 14:15
06/04/11 10:05
3 4 5 6 7 8 9 10 11 12 13
TestAmerica Tallahassee
Page 31 of 32
06/15/2011
1 2 3 4 5 6 7 8 9 10 11 12 13
Page 32 of 32
06/15/2011
