Supporting Information Oblongolides from the Endophytic Fungus ...

Supporting Information

Oblongolides from the Endophytic Fungus Phomopsis sp. BCC 9789 Taridaporn Bunyapaiboonsri,*,† Seangaroon Yoiprommarat,† Prasert Srikitikulchai,† Kitlada Srichomthong,† and Saisamorn Lumyong‡

National Center for Genetic Engineering and Biotechnology (BIOTEC), 113 Thailand Science Park, Phahonyothin Road, Klong 1, Klong Luang, Pathumthani 12120, Thailand, Department of Biology, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand

_________________________________ * To whom correspondence should be addressed. Tel.: +66-25646700 ext. 3553; fax: +6625646707. E-mail: [email protected]. †

National Center for Genetic Engineering and Biotechnology.

‡

Chiang Mai University.

Content S1

1

S2

13

S3

1

S4

13

S5

1

S6

13

S7

1

H NMR spectrum of oblongolide W1 (1) in acetone-d6 (500 MHz) C NMR spectrum of oblongolide W1 (1) in acetone-d6 (125 MHz)

H NMR spectrum of oblongolide W2 (2) in acetone-d6 (500 MHz) C NMR spectrum of oblongolide W2 (2) in acetone-d6 (125 MHz)

H NMR spectrum of oblongolide X (3) in CDCl3 (500 MHz) C NMR spectrum of oblongolide X (3) in CDCl3 (125 MHz)

H NMR spectrum of 2-deoxy-4α-hydroxyoblongolide X (4) in acetone-d6 (500

MHz) S8

13

C NMR spectrum of 2-deoxy-4α-hydroxyoblongolide X (4) in acetone-d6

(125MHz) S9

1

S10

13

S11

1

S12

13

H NMR spectrum of oblongolide Y (6) in acetone-d6 (500 MHz) C NMR spectrum of oblongolide Y (6) in acetone-d6 (125 MHz)

H NMR spectrum of oblongolide Z (7) in acetone-d6 (500 MHz) C NMR spectrum of oblongolide Z (7) in acetone-d6 (125 MHz)

S1

1

H NMR spectrum of oblongolide W1 (1) in acetone-d6 (500 MHz)

S2

13

C NMR spectrum of oblongolide W1 (1) in acetone-d6 (125 MHz)

S3

1

H NMR spectrum of oblongolide W2 (2) in acetone-d6 (500 MHz)

S4

13

C NMR spectrum of oblongolide W2 (2) in acetone-d6 (125 MHz)

S5

1

H NMR spectrum of oblongolide X (3) in CDCl3 (500 MHz)

S6

13

C NMR spectrum of oblongolide X (3) in CDCl3 (125 MHz)

S7

1

H NMR spectrum of 2-deoxy-4α-hydroxyoblongolide X (4) in acetone-d6 (500 MHz)

S8

13

C NMR spectrum of 2-deoxy-4α-hydroxyoblongolide X (4) in acetone-d6 (125 MHz)

S9

1

H NMR spectrum of oblongolide Y (6) in acetone-d6 (500 MHz)

S10

13

C NMR spectrum of oblongolide Y (6) in acetone-d6 (125 MHz)

S11

1

H NMR spectrum of oblongolide Z (7) in acetone-d6 (500 MHz)

S12

13

C NMR spectrum of oblongolide Z (7) in acetone-d6 (125 MHz)