Analytical Evaporators - Lasalle Scientific Inc.
Analytical Evaporators
Analytical Evaporators The FlexiVap™ Work Station is a new line of analytical nitrogen/air evaporators developed by Yongsong Huang of Brown University and licensed/manufactured by Glas-Col, LLC. The key advantages are:
One manifold suits all standard size vials
Easy closure of any manifold position
Reduced nitrogen consumption
Complete even flow rates in all ports
Cost effective compared with existing models on the market.
They are low cost, small footprint instruments used to concentrate chemical and biochemical solutions for further analysis, or evaporate to dryness for further reactions. What makes these systems unique is the ability to open or close each position by turning the knobs on the manifold and the rack and pinion precision lab stand. Digital temperature control to 100o C is available on certain models. Product Weight (lbs)
Voltage
Max PSI
109A YH-1*
FlexiVap Work Station, no heating for small insert, 24 positions with flowmeter.
N/A
50
15
109A YH-2*
FlexiVap Work Station, no heating for larger insert, 48 positions with flowmeter.
N/A
50
15
109A YH-1-12*
FlexiVap Work Station with heating for small insert, 24 positions with flowmeter.
120
50
20
109A YH-2-12*
FlexiVap Work Station with heating for larger insert, 48 positions with flowmeter.
120
50
25
109A YH-1-24*
FlexiVap Work Station with heating for small insert, 24 positions with flowmeter.
240
50
20
109A YH-2-24*
FlexiVap Work Station with heating for larger insert, 48 positions with flowmeter.
240
50
25
109A YH-4812
Aluminum Insert Block with 48 positions for up to 12 mm vials (Use with large system)
N/A
N/A
3
109A YH-4815
Aluminum Insert Block with 48 positions for 15 mm to 16mm vials (Use with large system)
N/A
N/A
3
109A YH-4816-15
Aluminum Insert Block with 48 positions for 15ml Centrifuge tubes (Use with large system)
N/A
N/A
3
109A YH-4828
Aluminum Insert Block with 24 positions for up to 28mm vials, EPA (Use with large system)
N/A
N/A
3
Aluminum Insert Block with 24 positions for 50ml Centrifuge tubes 109A YH-4829-50 (Use with large system)
N/A
N/A
3
109A YH-2412
Aluminum Insert Block with 24 positions for up to 12mm vials (Use with small system)
N/A
N/A
2
109A YH-2416
Aluminum Insert Block with 24 positions for 15mm to 16mm vials (Use with small system)
N/A
N/A
2
N/A
N/A
4
N/A
N/A
2
N/A
N/A
4
Catalog Number Description
Aluminum Insert Block with 24 positions for 15ml Centrifuge tubes 109A YH-2416-15 (Use with small system) 109A YH-2428
Aluminum Insert Block with 12 positions for up to 28mm vials, EPA (Use with small system)
Aluminum Insert Block with 12 positions for 50ml Centrifuge tubes 109A YH-2429-50 (Use with small system) 109A YH12
Bottom Heat plate only with digital control, 100oC Max
120
N/A
4
109A YH24
Bottom Heat plate only with digital control, 100oC Max, supplied with CEE/7 power cord
240
N/A
4
* does not include insert for vials, must be ordered separately Contact Glas-Col for other block sizes
Analytical Evaporators
Knobs to turn flow on/off for each posi‐ Rack & Pinion Drive
Metal luer locks and
Flow meter
Op onal heat source for samples
FlexiVap If your laboratory conducts research in any of the following areas, environmental organic analysis, organic analytical chemistry, petroleum analysis, food chemistry, forensic organic analysis, organic geochemistry, and any scientific research that requires solvent reduction. FlexiVap can greatly increase your lab productivity, especially if your research requires processing large numbers of samples. You or your students will never again have the mess of setting and dragging the pipettes or needles around in a nitrogen manifold, with just one FlexiVap in your lab.
The main advantages of the device relative to those currently on the market are: - Fully flexible with all vial sizes used in a lab, with just one manifold. Vial sizes can range from the standard EPA 40 ml and 20 ml vials (e.g., those used in Dionex ASE) to 4 ml and 2 ml vials. There are two model sizes, one model can simultaneously evaporate solvent from 24 EPA (40 ml) vials or 48 (4 ml) vials, another model can deal with half the number of vials simultaneously. You will only need one system in your lab to meet all solvent evaporation needs from all different vial sizes. The larger size model will handle 24 large vials from ASE simultaneously - same as TurboVap®, but the FlexiVap is far more flexible (see below).
- Easy open and close of any individual gas port and allows individual flow adjustments. If you do not need to use any gas ports, shut down the specific ports easily: you will save nitrogen gas and avoid contamination from dust stirred up by unused ports. - Complete equal flow rates from all ports (regardless how many ports are open or closed), so all your samples are blown down simultaneously and avoid overheating of sensitive compounds in early-dried up samples. - Automatic holding of needle positions with a high quality jacking stand. Easily adjust the height of needle positions. Easy cleaning of needles, no chance of blowing away your samples due to nitrogen outbursts. - Much lower cost than other evaporators on the market.
Analytical Evaporators Our ZipVap ™ line of evaporators are low cost, small footprint instruments used for solvent and water removal. These units concentrate chemical and biochemical solutions for further analysis, or evaporate to dryness for further reactions. Different Zipvap™ evaporators are available for small 12 mm auto sampler vials to 62 mm dia. bottles. Number of positions range from 2, 8, 12, 24, 28, 48 and 96. Temperature set-points to 100o C.
Catalog Number Description Zipvap 2, 2-position evaporator for 61mm flasks, insert 109A 11-80021 heated only, gas inlet not heated, with flowmeter. Zipvap 2, 2-position evaporator for 61mm flasks, insert and 109A 11-80025 gas inlet heated, with flowmeter. Zipvap 8, 8-position evaporator for 28mm vials, insert heat109A 11-80081 ed only, gas inlet not heated, with flowmeter. Zipvap 8, 8-position evaporator for 28mm flasks, insert and 109A 11-80085 gas inlet heated, with flowmeter. Zipvap 12, 12-position evaporator for 18mm vials, insert 109A 11-80121 heated only, gas inlet not heated, with flowmeter. Zipvap 12, 12-position evaporator for 18mm vials, insert 109A 11-80125 and gas inlet heated, with flowmeter. Zipvap 18, 18-position evaporator for tubes up to 25mm, 109A 11-80185 insert heated only, gas inlet not heated, no flowmeter. Zipvap 20, 20-position evaporator for 15mm vials, insert 109A 11-80201 heated only, gas inlet not heated, with flowmeter. Zipvap 20, 20-position evaporator for 15mm vials, insert 109A 11-80205 and gas inlet heated, with flowmeter. Zipvap 24, 24-position evaporator for 15mm vials, insert 109A 11-80241 heated only, gas inlet not heated, with flowmeter. Zipvap 24, 24-position evaporator for 15mm vials, insert 109A 11-80245 and gas inlet heated, with flowmeter. Zipvap 48, 48-position evaporator for 12mm auto sampler vials, insert heated only, gas inlet not heated, with flowme109A 11-80481 ter. Zipvap 48, 48-position evaporator for 12mm auto sampler 109A 11-80485 vials, insert and gas inlet heated, with flowmeter. Zipvap 96, 96-position unheated evaporator for 96 well 109A 11-80960 plate, with flowmeter. Zipvap 96, 96-position evaporator for 96 well plate, gas 109A 11-80961 inlet not heated, with flowmeter. Zipvap 96, 96-position evaporator for 96 well plate, gas 109A 11-80965 inlet heated, with flowmeter. Zipvap 96, Triple position evaporator for (3) 96 deep well 109A 11-80333 plates, gas heater and flow meters with on/off switches.
Voltage
Max PSI
Product Weight (lbs)
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
N/A
N/A
4
120
20
8
120
20
8
120
50
12
Analytical Evaporators
Barvap
Catalog Number 109A 11-06000 109A 11-06001 109A 11-06005 109A 11-12000 109A 11-13001 109A 11-16001 109A 11-20001
Description Barvap 6, 6 position unheated bar evaporator, with six 4" bent needles, needle valve and 3' of 1/4" tubing 4" needles with plated metal hub, bent. Set of 6 1/4" OD x 1/8" ID silicone tubing - 3' piece Barvap 12, 12 position unheated bar evaporator, with 12 4" bent needles, 2 needle valves and 2 - 3' pieces of tubing Aluminum Barvap holder for six 13mm diameter vials (nickel plated) Aluminum Barvap holder for six 16mm diameter vials (nickel plated) Aluminum Barvap holder for six 20mm diameter vials (nickel plated)
Max PSI
Product Weight (lbs)
40
2 0.2 0.2
40
5
2
2
2
Accessory Blocks for ZipVaps
Catalog Number Description 109A 12-70022 Aluminum block holder for two 61mm flasks 109A 12-70082 Aluminum block holder for 8 vials up to 28mm diameter 109A 12-70122 Aluminum block holder for 12 vials up to 22mm diameter 109A 12-70202 Aluminum block holder for 20 vials up to 15mm diameter 109A 12-70242 Aluminum block holder for 24 vials up to 12mm diameter 109A 12-70243 Aluminum block holder for 24 vials up to 15mm diameter 109A 12Aluminum block for 24 vials, 8mm diameter, auto sampler 70248SP vials Aluminum block for 48 vials, 12mm diameter, auto sampler 109A 12-70482 vials Aluminum block for 48 vials, 8mm diameter, auto sampler 109A 12-70483 vials Aluminum block for 48 vials, 6mm diameter, auto sampler 109A 12-70484 vials
Product Weight (lbs) 1 1 1 1 1 1 1 1 1 1
Analytical Evaporators Glas-Col’s New Smaller Digital Pulse Mixer with Evaporator/Concentrator: This system is designed to rapidly evaporate/concentrate solvents by both heating the sample bottom and the incoming nitrogen. Each position is furnished with an individual needle for the best possible delivery of gas. The pulsing feature that is selectable allows a film of solvent to be thrown on the sidewall; then the vortex collapses. Next the vortex again is created and the process continues until the concentration level is achieved providing the quickest method of solvent evaporation. This unit takes up less bench space compared to other concentrators. The beauty of this system is the flexibility to change sample size. The system is furnished with the 2 heat block chambers and then you select the polypropylene manifold and aluminum block to fit your application. Changing to another size of vial takes only a few minutes.
The Digital Pulse Mixer/Evaporator has the following features:
Micro-processor based control technology Speed 150 to 1000 rpm, Speed Setting Increment: 10 RPM 4-line back-lit LCD display Built-in digital timer (seconds: 1-60, minutes: 1-60, hours: 1-24) User selectable pulse profile (Pulses-per-minute: 1-100), Ppm-duty-cycle: 1-99 % Timer and Pulse mode may be combined. Communication port (USB) Membrane switch user interface (4-button) Soft Start/Stop of motor Optional software for real time data acquisition Orbital offset .070” Set point temperature for Bottom Blocks (120oC Max) Flow meter located on left side of mixer A fine needle valve for flow control is provided on each manifold
Maximum psi: 20
Specifications: Size Platform size
12”w x 22”d x 8” H to drive plate 7” x 12”
Voltage
120 or 240 volt models
Mixer mounts
Vibration absorbing for minimum transfer to lab bench
On/Off switch
Located on front of unit
Finish
Light gray and black powder coat finish
Cord
3-wire 6’ long
Catalog No.
Description
Weight (lbs)
099A DPMES12
Evap system 2 block format, w/out manifold 120 Volts, 60hz.
55
099A DPMES24
Evap system 2 block format, w/out manifold 240 Volts, 50/60hz.
55
099A PMAN96
96 well polypropylene manifold w/needles
1
099A PMAN24
24 well polypropylene manifold w/needles
1
099A PMAN20
20 well polypropylene manifold w/needles
1
099A PMAN8
8 well polypropylene manifold w/needles
1
R34 562
24 well aluminum block 12mm vials
2
R34 561
24 well aluminum block 15mm vials
2
R34 563
20 well aluminum block 15 to 16mm vials
2
R34 516
8 well aluminum block for EPA vials
2
Analytical Evaporators Glas-Col’s Digital Pulse Mixer with Evaporator/ Concentrator: This larger system is designed to rapidly evaporate/concentrate solvents by both heating the sample bottom and the incoming nitrogen. Each position is furnished with an individual needle for the best possible delivery of gas. The pulsing feature that is selectable allows a film of solvent to be thrown on the sidewall; then the vortex collapses. Next the vortex again is created and the process continues until the concentration level is achieved providing the quickest method of solvent evaporation. This unit takes up little bench space compared to other concentrators.
The Digital Pulse Mixer/Evaporator has the following features:
Micro-processor based control technology
Speed 150 to 800 rpm, Speed Display Resolution: .1 RPM, Speed Setting Increment: 10 RPM
4-line back-lit LCD display
Built-in digital timer (seconds: 1-60, minutes: 1-60, hours: 1-24)
User selectable pulse profile (Pulses-per-minute: 1-100), Ppm-duty-cycle: 1-99 %
Timer and Pulse mode may be combined.
Communication port (USB)
Membrane switch user interface (4-button)
Soft Start/Stop of motor
Optional software for real time data acquisition
Orbital offset .070”
Max Set point temperature for Manifold (80oC) and Bottom Blocks (105oC Max)
Exhaust fan (Optional with Solvent Recovery Cabinet)
Specifications: Size Platform size
19-1/4”w x 23”d x 20” H 10” x 12”
Voltage
120
Mixer mounts
Vibration absorbing
On/Off switch
Located on front of unit
Finish
Light gray and black powder coat finish
Cord
3-wire 6’ long
Load
Up to 10 lbs Weight Catalog Number
Description
Voltage
(lbs)
099A DPM12E24
24-Place Evaporator for EPA vials
120
80
099A DPM12E6
6-Place Evaporator for 250ml bottle
120
80
099A DPM24E24
24-Place Evaporator for EPA vials
240
80
099A DPM24E6
6-Place Evaporator for 250ml bottle
240
80
Analytical Evaporators The optional bolt on cabinet will allow the capture of solvents
Other options include:
Multi-zone heating
Ni Flow control thru front panel
Over temperature limits
PC control thru Labnetix® software
Contact our sales team to review your requirements. DPM Shown with Op onal Cabinet and Blow Down for 96 Well Plates Catalog Number
Description
Weight (lbs)
099A SCR
Solvent Recovery Cabinet Assembly
10
099A LABNETIX
LABNETIX Automation Software
1
SOLVENT EVAPORATION TIMES FOR DPM TYPE MIXERS WITH HEATED MANIFOLD Solvent
Conditions
Starting Volume
Time to 1 mL
*acetone/DCM
40
50
26
*acetone/hexane
40
50
19
**water
40
50
120
*acetone/DCM
20
50
33
*acetone/hexane
20
50
21
**water
20
50
175
***Acetonitrile/Water
20
40 (50/50 mix)
180
****Acetonitrile/Water
20
20 (50/50 mix)
150
*****acetic acid 2ml per well in 48 well plate
20
2ml
>60
*Temperature of vortex block: 50 °C. Temperature of the manifold: 70 °C. Speed 800 rpm. Pulse 70 per min, duty: 90% **Temperature of vortex block: 90 °C. Temperature of the manifold: 80 °C. Speed 800 rpm. Pulse 70 per min, duty: 90% *** Temperature of vortex block: 70 °C. Temperature of the manifold: 70 °C. Speed 800 rpm. **** Temperature of vortex block: 50 °C. Temperature of the manifold: 50 °C. Speed 800 rpm. ***** Temperature of vortex block: 35 °C. Temperature of the manifold: 35 °C. Speed 300 rpm.
711 Hulman Street. P.O. Box 2128, Terre Haute, IN 47802-0128 USA Phone. (812) 235-6167, Fax. (812) 234-6975 E-mail: [email protected] www.glascol.com
2/12 Rev 0
Analytical Evaporators The FlexiVap™ Work Station is a new line of analytical nitrogen/air evaporators developed by Yongsong Huang of Brown University and licensed/manufactured by Glas-Col, LLC. The key advantages are:
One manifold suits all standard size vials
Easy closure of any manifold position
Reduced nitrogen consumption
Complete even flow rates in all ports
Cost effective compared with existing models on the market.
They are low cost, small footprint instruments used to concentrate chemical and biochemical solutions for further analysis, or evaporate to dryness for further reactions. What makes these systems unique is the ability to open or close each position by turning the knobs on the manifold and the rack and pinion precision lab stand. Digital temperature control to 100o C is available on certain models. Product Weight (lbs)
Voltage
Max PSI
109A YH-1*
FlexiVap Work Station, no heating for small insert, 24 positions with flowmeter.
N/A
50
15
109A YH-2*
FlexiVap Work Station, no heating for larger insert, 48 positions with flowmeter.
N/A
50
15
109A YH-1-12*
FlexiVap Work Station with heating for small insert, 24 positions with flowmeter.
120
50
20
109A YH-2-12*
FlexiVap Work Station with heating for larger insert, 48 positions with flowmeter.
120
50
25
109A YH-1-24*
FlexiVap Work Station with heating for small insert, 24 positions with flowmeter.
240
50
20
109A YH-2-24*
FlexiVap Work Station with heating for larger insert, 48 positions with flowmeter.
240
50
25
109A YH-4812
Aluminum Insert Block with 48 positions for up to 12 mm vials (Use with large system)
N/A
N/A
3
109A YH-4815
Aluminum Insert Block with 48 positions for 15 mm to 16mm vials (Use with large system)
N/A
N/A
3
109A YH-4816-15
Aluminum Insert Block with 48 positions for 15ml Centrifuge tubes (Use with large system)
N/A
N/A
3
109A YH-4828
Aluminum Insert Block with 24 positions for up to 28mm vials, EPA (Use with large system)
N/A
N/A
3
Aluminum Insert Block with 24 positions for 50ml Centrifuge tubes 109A YH-4829-50 (Use with large system)
N/A
N/A
3
109A YH-2412
Aluminum Insert Block with 24 positions for up to 12mm vials (Use with small system)
N/A
N/A
2
109A YH-2416
Aluminum Insert Block with 24 positions for 15mm to 16mm vials (Use with small system)
N/A
N/A
2
N/A
N/A
4
N/A
N/A
2
N/A
N/A
4
Catalog Number Description
Aluminum Insert Block with 24 positions for 15ml Centrifuge tubes 109A YH-2416-15 (Use with small system) 109A YH-2428
Aluminum Insert Block with 12 positions for up to 28mm vials, EPA (Use with small system)
Aluminum Insert Block with 12 positions for 50ml Centrifuge tubes 109A YH-2429-50 (Use with small system) 109A YH12
Bottom Heat plate only with digital control, 100oC Max
120
N/A
4
109A YH24
Bottom Heat plate only with digital control, 100oC Max, supplied with CEE/7 power cord
240
N/A
4
* does not include insert for vials, must be ordered separately Contact Glas-Col for other block sizes
Analytical Evaporators
Knobs to turn flow on/off for each posi‐ Rack & Pinion Drive
Metal luer locks and
Flow meter
Op onal heat source for samples
FlexiVap If your laboratory conducts research in any of the following areas, environmental organic analysis, organic analytical chemistry, petroleum analysis, food chemistry, forensic organic analysis, organic geochemistry, and any scientific research that requires solvent reduction. FlexiVap can greatly increase your lab productivity, especially if your research requires processing large numbers of samples. You or your students will never again have the mess of setting and dragging the pipettes or needles around in a nitrogen manifold, with just one FlexiVap in your lab.
The main advantages of the device relative to those currently on the market are: - Fully flexible with all vial sizes used in a lab, with just one manifold. Vial sizes can range from the standard EPA 40 ml and 20 ml vials (e.g., those used in Dionex ASE) to 4 ml and 2 ml vials. There are two model sizes, one model can simultaneously evaporate solvent from 24 EPA (40 ml) vials or 48 (4 ml) vials, another model can deal with half the number of vials simultaneously. You will only need one system in your lab to meet all solvent evaporation needs from all different vial sizes. The larger size model will handle 24 large vials from ASE simultaneously - same as TurboVap®, but the FlexiVap is far more flexible (see below).
- Easy open and close of any individual gas port and allows individual flow adjustments. If you do not need to use any gas ports, shut down the specific ports easily: you will save nitrogen gas and avoid contamination from dust stirred up by unused ports. - Complete equal flow rates from all ports (regardless how many ports are open or closed), so all your samples are blown down simultaneously and avoid overheating of sensitive compounds in early-dried up samples. - Automatic holding of needle positions with a high quality jacking stand. Easily adjust the height of needle positions. Easy cleaning of needles, no chance of blowing away your samples due to nitrogen outbursts. - Much lower cost than other evaporators on the market.
Analytical Evaporators Our ZipVap ™ line of evaporators are low cost, small footprint instruments used for solvent and water removal. These units concentrate chemical and biochemical solutions for further analysis, or evaporate to dryness for further reactions. Different Zipvap™ evaporators are available for small 12 mm auto sampler vials to 62 mm dia. bottles. Number of positions range from 2, 8, 12, 24, 28, 48 and 96. Temperature set-points to 100o C.
Catalog Number Description Zipvap 2, 2-position evaporator for 61mm flasks, insert 109A 11-80021 heated only, gas inlet not heated, with flowmeter. Zipvap 2, 2-position evaporator for 61mm flasks, insert and 109A 11-80025 gas inlet heated, with flowmeter. Zipvap 8, 8-position evaporator for 28mm vials, insert heat109A 11-80081 ed only, gas inlet not heated, with flowmeter. Zipvap 8, 8-position evaporator for 28mm flasks, insert and 109A 11-80085 gas inlet heated, with flowmeter. Zipvap 12, 12-position evaporator for 18mm vials, insert 109A 11-80121 heated only, gas inlet not heated, with flowmeter. Zipvap 12, 12-position evaporator for 18mm vials, insert 109A 11-80125 and gas inlet heated, with flowmeter. Zipvap 18, 18-position evaporator for tubes up to 25mm, 109A 11-80185 insert heated only, gas inlet not heated, no flowmeter. Zipvap 20, 20-position evaporator for 15mm vials, insert 109A 11-80201 heated only, gas inlet not heated, with flowmeter. Zipvap 20, 20-position evaporator for 15mm vials, insert 109A 11-80205 and gas inlet heated, with flowmeter. Zipvap 24, 24-position evaporator for 15mm vials, insert 109A 11-80241 heated only, gas inlet not heated, with flowmeter. Zipvap 24, 24-position evaporator for 15mm vials, insert 109A 11-80245 and gas inlet heated, with flowmeter. Zipvap 48, 48-position evaporator for 12mm auto sampler vials, insert heated only, gas inlet not heated, with flowme109A 11-80481 ter. Zipvap 48, 48-position evaporator for 12mm auto sampler 109A 11-80485 vials, insert and gas inlet heated, with flowmeter. Zipvap 96, 96-position unheated evaporator for 96 well 109A 11-80960 plate, with flowmeter. Zipvap 96, 96-position evaporator for 96 well plate, gas 109A 11-80961 inlet not heated, with flowmeter. Zipvap 96, 96-position evaporator for 96 well plate, gas 109A 11-80965 inlet heated, with flowmeter. Zipvap 96, Triple position evaporator for (3) 96 deep well 109A 11-80333 plates, gas heater and flow meters with on/off switches.
Voltage
Max PSI
Product Weight (lbs)
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
120
20
8
N/A
N/A
4
120
20
8
120
20
8
120
50
12
Analytical Evaporators
Barvap
Catalog Number 109A 11-06000 109A 11-06001 109A 11-06005 109A 11-12000 109A 11-13001 109A 11-16001 109A 11-20001
Description Barvap 6, 6 position unheated bar evaporator, with six 4" bent needles, needle valve and 3' of 1/4" tubing 4" needles with plated metal hub, bent. Set of 6 1/4" OD x 1/8" ID silicone tubing - 3' piece Barvap 12, 12 position unheated bar evaporator, with 12 4" bent needles, 2 needle valves and 2 - 3' pieces of tubing Aluminum Barvap holder for six 13mm diameter vials (nickel plated) Aluminum Barvap holder for six 16mm diameter vials (nickel plated) Aluminum Barvap holder for six 20mm diameter vials (nickel plated)
Max PSI
Product Weight (lbs)
40
2 0.2 0.2
40
5
2
2
2
Accessory Blocks for ZipVaps
Catalog Number Description 109A 12-70022 Aluminum block holder for two 61mm flasks 109A 12-70082 Aluminum block holder for 8 vials up to 28mm diameter 109A 12-70122 Aluminum block holder for 12 vials up to 22mm diameter 109A 12-70202 Aluminum block holder for 20 vials up to 15mm diameter 109A 12-70242 Aluminum block holder for 24 vials up to 12mm diameter 109A 12-70243 Aluminum block holder for 24 vials up to 15mm diameter 109A 12Aluminum block for 24 vials, 8mm diameter, auto sampler 70248SP vials Aluminum block for 48 vials, 12mm diameter, auto sampler 109A 12-70482 vials Aluminum block for 48 vials, 8mm diameter, auto sampler 109A 12-70483 vials Aluminum block for 48 vials, 6mm diameter, auto sampler 109A 12-70484 vials
Product Weight (lbs) 1 1 1 1 1 1 1 1 1 1
Analytical Evaporators Glas-Col’s New Smaller Digital Pulse Mixer with Evaporator/Concentrator: This system is designed to rapidly evaporate/concentrate solvents by both heating the sample bottom and the incoming nitrogen. Each position is furnished with an individual needle for the best possible delivery of gas. The pulsing feature that is selectable allows a film of solvent to be thrown on the sidewall; then the vortex collapses. Next the vortex again is created and the process continues until the concentration level is achieved providing the quickest method of solvent evaporation. This unit takes up less bench space compared to other concentrators. The beauty of this system is the flexibility to change sample size. The system is furnished with the 2 heat block chambers and then you select the polypropylene manifold and aluminum block to fit your application. Changing to another size of vial takes only a few minutes.
The Digital Pulse Mixer/Evaporator has the following features:
Micro-processor based control technology Speed 150 to 1000 rpm, Speed Setting Increment: 10 RPM 4-line back-lit LCD display Built-in digital timer (seconds: 1-60, minutes: 1-60, hours: 1-24) User selectable pulse profile (Pulses-per-minute: 1-100), Ppm-duty-cycle: 1-99 % Timer and Pulse mode may be combined. Communication port (USB) Membrane switch user interface (4-button) Soft Start/Stop of motor Optional software for real time data acquisition Orbital offset .070” Set point temperature for Bottom Blocks (120oC Max) Flow meter located on left side of mixer A fine needle valve for flow control is provided on each manifold
Maximum psi: 20
Specifications: Size Platform size
12”w x 22”d x 8” H to drive plate 7” x 12”
Voltage
120 or 240 volt models
Mixer mounts
Vibration absorbing for minimum transfer to lab bench
On/Off switch
Located on front of unit
Finish
Light gray and black powder coat finish
Cord
3-wire 6’ long
Catalog No.
Description
Weight (lbs)
099A DPMES12
Evap system 2 block format, w/out manifold 120 Volts, 60hz.
55
099A DPMES24
Evap system 2 block format, w/out manifold 240 Volts, 50/60hz.
55
099A PMAN96
96 well polypropylene manifold w/needles
1
099A PMAN24
24 well polypropylene manifold w/needles
1
099A PMAN20
20 well polypropylene manifold w/needles
1
099A PMAN8
8 well polypropylene manifold w/needles
1
R34 562
24 well aluminum block 12mm vials
2
R34 561
24 well aluminum block 15mm vials
2
R34 563
20 well aluminum block 15 to 16mm vials
2
R34 516
8 well aluminum block for EPA vials
2
Analytical Evaporators Glas-Col’s Digital Pulse Mixer with Evaporator/ Concentrator: This larger system is designed to rapidly evaporate/concentrate solvents by both heating the sample bottom and the incoming nitrogen. Each position is furnished with an individual needle for the best possible delivery of gas. The pulsing feature that is selectable allows a film of solvent to be thrown on the sidewall; then the vortex collapses. Next the vortex again is created and the process continues until the concentration level is achieved providing the quickest method of solvent evaporation. This unit takes up little bench space compared to other concentrators.
The Digital Pulse Mixer/Evaporator has the following features:
Micro-processor based control technology
Speed 150 to 800 rpm, Speed Display Resolution: .1 RPM, Speed Setting Increment: 10 RPM
4-line back-lit LCD display
Built-in digital timer (seconds: 1-60, minutes: 1-60, hours: 1-24)
User selectable pulse profile (Pulses-per-minute: 1-100), Ppm-duty-cycle: 1-99 %
Timer and Pulse mode may be combined.
Communication port (USB)
Membrane switch user interface (4-button)
Soft Start/Stop of motor
Optional software for real time data acquisition
Orbital offset .070”
Max Set point temperature for Manifold (80oC) and Bottom Blocks (105oC Max)
Exhaust fan (Optional with Solvent Recovery Cabinet)
Specifications: Size Platform size
19-1/4”w x 23”d x 20” H 10” x 12”
Voltage
120
Mixer mounts
Vibration absorbing
On/Off switch
Located on front of unit
Finish
Light gray and black powder coat finish
Cord
3-wire 6’ long
Load
Up to 10 lbs Weight Catalog Number
Description
Voltage
(lbs)
099A DPM12E24
24-Place Evaporator for EPA vials
120
80
099A DPM12E6
6-Place Evaporator for 250ml bottle
120
80
099A DPM24E24
24-Place Evaporator for EPA vials
240
80
099A DPM24E6
6-Place Evaporator for 250ml bottle
240
80
Analytical Evaporators The optional bolt on cabinet will allow the capture of solvents
Other options include:
Multi-zone heating
Ni Flow control thru front panel
Over temperature limits
PC control thru Labnetix® software
Contact our sales team to review your requirements. DPM Shown with Op onal Cabinet and Blow Down for 96 Well Plates Catalog Number
Description
Weight (lbs)
099A SCR
Solvent Recovery Cabinet Assembly
10
099A LABNETIX
LABNETIX Automation Software
1
SOLVENT EVAPORATION TIMES FOR DPM TYPE MIXERS WITH HEATED MANIFOLD Solvent
Conditions
Starting Volume
Time to 1 mL
*acetone/DCM
40
50
26
*acetone/hexane
40
50
19
**water
40
50
120
*acetone/DCM
20
50
33
*acetone/hexane
20
50
21
**water
20
50
175
***Acetonitrile/Water
20
40 (50/50 mix)
180
****Acetonitrile/Water
20
20 (50/50 mix)
150
*****acetic acid 2ml per well in 48 well plate
20
2ml
>60
*Temperature of vortex block: 50 °C. Temperature of the manifold: 70 °C. Speed 800 rpm. Pulse 70 per min, duty: 90% **Temperature of vortex block: 90 °C. Temperature of the manifold: 80 °C. Speed 800 rpm. Pulse 70 per min, duty: 90% *** Temperature of vortex block: 70 °C. Temperature of the manifold: 70 °C. Speed 800 rpm. **** Temperature of vortex block: 50 °C. Temperature of the manifold: 50 °C. Speed 800 rpm. ***** Temperature of vortex block: 35 °C. Temperature of the manifold: 35 °C. Speed 300 rpm.
711 Hulman Street. P.O. Box 2128, Terre Haute, IN 47802-0128 USA Phone. (812) 235-6167, Fax. (812) 234-6975 E-mail: [email protected] www.glascol.com
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