30345 TRC P689450
Certificate of Analysis 2 Brisbane Road, Toronto, ON. M3J 2J8 Canada Tel: (416) 665-9696 Fax: (416) 665-4439 E-mail: [email protected] Website: www.trc-canada.com
1. Identification CAS Number: 801-52-5
Catalogue Number: P689450
Product: Porfiromycin Synonyms: (1aS,8S,8aR,8bS)-6-Amino-8-[[(aminocarbonyl)oxy]methyl]-1,1a,2,8,8a,8b-hexahydro-8a-methoxy-1,5dimethylazirino[2',3':3,4]pyrrolo[1,2-a]indole-4,7-dione; ENT 50825; Methyl Mitomycin C; Methylmitomycin; NMethylmitomycin C; NCI 56410; NSC 56410; Porfiromycine; Regamycin; U 14743; ! Structure: Molecular Formula: C16H20N4O5 Molecular Weight: 348.35 Source of Product: Synthetic
2. Analytical Information Lot Number: 13-MAR-23-3 Melting Point: N/A
Boiling Point: N/A
Atmosphere: Inert Gas
Appearance of Product: Dark Purple Solid
Solubility Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
Method for Determining Identity: 1 H NMR (DMSO-d6) and MS
Stability Light Sensitive
Purity: 97%
Long Term Storage Condition: Amber Vial, -20˚C Freezer, Under Inert Atmosphere
Additional Information: TLC Conditions: SiO2; Dichloromethane : Methanol = 9 : 1; Visualized with UV, AMCS, and Naked Eye; Single Spot, Rf = 0.45. 1 H NMR and MS conform to structure. Elemental Analysis: (Found) %C: 53.14, %H: 5.84, %N: 15.33; (Calculated) %C: 55.17, %H: 5.79, %N: 16.08 Specific Rotation: +135.5° (c = 0.04, Methanol) Contains: 1.3% Dichloromethane
QC Test Date
March 18, 2016 Philip Chan, Quality Control Supervisor
Retest Date
March 16, 2019
Certificate of Analysis 2 Brisbane Road, Toronto, ON. M3J 2J8 Canada Tel: (416) 665-9696 Fax: (416) 665-4439 E-mail: [email protected] Website: www.trc-canada.com
1. Identification CAS Number: 801-52-5
Catalogue Number: P689450
Product: Porfiromycin Synonyms: (1aS,8S,8aR,8bS)-6-Amino-8-[[(aminocarbonyl)oxy]methyl]-1,1a,2,8,8a,8b-hexahydro-8a-methoxy-1,5dimethylazirino[2',3':3,4]pyrrolo[1,2-a]indole-4,7-dione; ENT 50825; Methyl Mitomycin C; Methylmitomycin; NMethylmitomycin C; NCI 56410; NSC 56410; Porfiromycine; Regamycin; U 14743; ! Structure: Molecular Formula: C16H20N4O5 Molecular Weight: 348.35 Source of Product: Synthetic
2. Analytical Information Lot Number: 13-MAR-23-3 Melting Point: N/A
Boiling Point: N/A
Atmosphere: Inert Gas
Appearance of Product: Dark Purple Solid
Solubility Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
Method for Determining Identity: 1 H NMR (DMSO-d6) and MS
Stability Light Sensitive
Purity: 97%
Long Term Storage Condition: Amber Vial, -20˚C Freezer, Under Inert Atmosphere
Additional Information: TLC Conditions: SiO2; Dichloromethane : Methanol = 9 : 1; Visualized with UV, AMCS, and Naked Eye; Single Spot, Rf = 0.45. 1 H NMR and MS conform to structure. Elemental Analysis: (Found) %C: 53.14, %H: 5.84, %N: 15.33; (Calculated) %C: 55.17, %H: 5.79, %N: 16.08 Specific Rotation: +135.5° (c = 0.04, Methanol) Contains: 1.3% Dichloromethane
QC Test Date
March 18, 2016 Philip Chan, Quality Control Supervisor
Retest Date
March 16, 2019
Certificate of Analysis 2 Brisbane Road, Toronto, ON. M3J 2J8 Canada Tel: (416) 665-9696 Fax: (416) 665-4439 E-mail: [email protected] Website: www.trc-canada.com
